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221.
Zusammenfassung Die massenspektrometrische Analyse kleinster Gasmengen von H2, O2, CO, CO2, CH4 und H2O ist infolge der Beeinflussung durch das Meßsystem mit beachtlichen Schwierigkeiten verbunden. Die Beeinflussung erfolgt einerseits durch Reaktionen der Gase mit heißen Metalloberflächen und andererseits durch im System vorhandene Glasoberflächen. Bei einer entprechenden apparativen Anordnung, Erhitzen der Proben und Trennung der Gase durch Kühlfallen, können Gasmengen in und auf Mineralen bis zu 0,005 mm3/NDT quantitativ bestimmt werden. Die Apparatur ist durch thermische Zersetzung von Muskovit-, Calcitkristallen usw. geeicht. Die Anwendung dieser Methode auf das Gebiet der Chemie und Mineralogie sowie die Grenzen und Möglichkeiten einer quantitativen Analyse von Restgasen wird gezeigt.
Mit 5 Abbildungen 相似文献
Mass-spectrometric analysis of gases of the system C-H-O in minerals
Summary The analysis by mass-spectrometer of smallest amounts of gases H2, O2, CO, CO2, CH4 and H2O, respectively, meets with considerable difficulties, because of the influence by the measuring system. The influence is caused by interactions of the gases with hot metal surfaces on one hand, and glass surfaces on the other hand. By a suitable arrangement of apparatus and procedures, such as heating the samples and separating the gases by cooling traps, the gas amounts in and on minerals can be quantitatively determined up to 0.005 mm3/SPT. The apparatus is calibrated by thermal dissociation of crystals like muscovite, calcite etc. The application of this method in chemistry and mineralogy is treated as well as the limits and the possibility of the quantitative analysis of residual gas.
Mit 5 Abbildungen 相似文献
222.
B. Panteleit K. Hamer R. Kringel W. Kessels H. D. Schulz 《Environmental Earth Sciences》2011,62(1):77-91
Geochemical processes, occurring in a stable transition zone between saltwater and freshwater, were simulated in a 2D, multi-layer
flow chamber experiment. Mixing, calcite dissolution, and oxidative degradation of organic matter were identified as the main
controlling factors. The results of the chamber experiment were compared to field data and verified by thermodynamic modeling.
Similarity in most ion distributions suggests the general applicability of the experimental method. Differences in the redox
conditions between field and experiment were reflected by the oxidants involved in the mineralization of organic carbon; while
field data show evidence of sulfate reduction, the presence of oxygen in the laboratory experiment resulted in the reoxidation
of sulfides. 相似文献
223.
Gas emission prediction and recovery in underground coal mines 总被引:2,自引:0,他引:2
Strata gas can be released and captured from non-active and active gas resources either from virgin or relaxed strata, both prior to and when mining activities take place. The high and irregular gas emissions associated with high production longwall mining have provided a need to optimise the methods used to predict these gas levels and the ventilation requirements for gas dilution. A forecast of gas emissions during development drivage and longwall mining indicated possible gas and ventilation problems requiring the introduction of various gas drainage techniques and in maintaining the necessary air quantities in ventilation systems to satisfy the statutory gas limitations for various coal production rates. Although there are sound principles used in world-recognised methods of gas emission prediction, a new approach developed from long-term practical experience in underground gassy coal mine practices and gas-rock mechanics studies appear most suitable for local conditions and mining systems in use. The Lunagas ‘Floorgas' and ‘Roofgas' geomechanical and gas emission models offer an effective solution to these problems. Both programs are the most advanced engineering, numerical tools available to calculate gas source contributions to total gassiness and improve the accuracy and quality of gas control, gas capture technologies and ventilation system design. 相似文献
224.
The Shamrocke ore body is a stratiform deposit of disseminated copper-iron sulphides found within lenses of calcareous meta-arkose occurring in Lomagundi Group graphitic schist (Late Precambrian) at Karoi, Rhodesia. Both sulphides and sediments were subjected to high grades of regional metamorphism. Argon/argon isochron ages indicate a major metamorphic event at 550 m. y. (Damaran orogeny) with later minor argon losses. Ore sulphide 34S values range from +3.0 to +14.8 CDT and a general decrease from footwall to hanging-wall reflects an original sedimentary environment where sulphides formed about the sea bed from hydrothermal fluids progressively mixing with sea water. Isotopically lighter sulphides formed syngenetically in the host rocks from bacterial reduction of sulphate. The pyrrhotite was probably formed from pyrite during metamorphism, and owing to reducing conditions maintained similar 34S values to the original pyrite. Oxygen and carbon isotopic analyses of mineralised and unmineralised carbonate lenses are consistent with deposition as marine limestones in an evaporitic environment and/or near hot spring vents.I. N. S. Contribution No 734 相似文献
225.
Kenneth D. Adams Ted Goebel Kelly Graf Geoffrey M. Smith Anna J. Camp Richard W. Briggs David Rhode 《Geoarchaeology》2008,23(5):608-643
The Great Basin of the western U.S. contains a rich record of Late Pleistocene and Holocene lake‐level fluctuations as well as an extensive record of human occupation during the same time frame. We compare spatial‐temporal relationships between these records in the Lahontan basin to consider whether lake‐level fluctuations across the Pleistocene‐Holocene transition controlled distribution of archaeological sites. We use the reasonably well‐dated archaeological record from caves and rockshelters as well as results from new pedestrian surveys to investigate this problem. Although lake levels probably reached maximum elevations of about 1230–1235 m in the different subbasins of Lahontan during the Younger Dryas (YD) period, the duration that the lakes occupied the highest levels was brief. Paleoindian and Early Archaic archaeological sites are concentrated on somewhat lower and slightly younger shorelines (_1220–1225 m) that also date from the Younger Dryas period. This study suggests that Paleoindians often concentrated their activities adjacent to large lakes and wetland resources soon after they first entered the Great Basin. © 2008 Wiley Periodicals, Inc. 相似文献
226.
227.
Cordieritites and highly peraluminous granites within the ElPilón granite complex, Sierras Pampeanas, Argentina,were emplaced during a medium-P, high-T metamorphic event duringthe initial decompression of a Cambrian orogen along the southwesternmargin of Gondwana. Very fresh orbicular and massive cordierititebodies with up to 90% cordieritite are genetically associatedwith a cordierite monzogranite pluton and a larger body of porphyriticgranodiorite. The petrogenesis of this association has beenstudied using petrographical, mineralogical, thermobarometric,geochemical, geochronological and isotope methods. The graniticmagmas were formed by anatexis of mid-crustal metamorphic rocksformed earlier in the Pampean orogeny. The cordieritites appearat the top of feeder conduits that connected the source regionlocated at 相似文献
228.
J. M. Charnock C. M. B. Henderson J. F. W. Mosselmans R. A. D. Pattrick 《Physics and Chemistry of Minerals》1996,23(7):403-408
The X-ray absorption spectra of the transition metal L3,2-edges of the dichalcogenides FeS2 (pyrite), FeSe2, FeTe2, CoS2, CoSe2, CoTe2, NiS2, NiSe2 and NiTe2 have been studied. These spectra are compared with theoretical simulations make using the atomic multiplet approach assuming on octahedral site for the metal atoms. The Ni spectra can be closely simulated using this approach but the Fe and Co spectra show less good fits to the experimental data. The reasons for this and its implications for the use of L-edge spectra in the study of such minerals are discussed in terms of the covalency and the ground states of the compounds; these results indicate the mixing of the ground states increases in the order Ni<Co<Fe. 相似文献
229.
R. W. John 《Astronomische Nachrichten》1986,307(5):303-305
In the vacuum case, Einstein's equations generalized by additive terms containing derivatives of the metric up to the 4th order are applied to cosmological Bianchi-type I model space-times. 相似文献
230.
On 11 September 1973 a peculiar prominence was observed. The prominence displayed strong ( 50km s–1) systematic motions toward and away from the observer. The unusual spectrographic appearance of the prominence might have been due to downflowing material lifted into the corona during an earlier coronal transient.The National Center for Atmospheric Research is sponsored by the National Science Foundation.Operated by the Association of Universities for Research in Astronomy, Inc., under contract with the National Science Foundation. 相似文献