Simple determination of dimethylsulfide (DMS) and dimethylsulfoniopropionate (DMSP) using solid-phase microextraction and gas chromatography-mass spectrometry

Solid-phase microextraction (SPME) is a simple, sensitive and less destructive method for the determination of dimethylsulfide (DMS) in seawater. Combined with detection by gas chromatography-mass spectrometry (GC-MS), the method had sufficient sensitivity (minimum detectable concentration of DMS was 0.05 nM), and practical levels of reproducibility (relative standard deviation ≤7%) and linearity (r ² > 0.995) over a wide concentration range (0.5 to 910 nM). The protocol developed was applied to a Sagami Bay water sample to determine concentrations of DMS and DMSP, and in situ DMSP-lyase activity.     

Eddy Shedding from the Kuroshio Bend at Luzon Strait

TOPEX/POSEDIENT-ERS satellite altimeter data along with the mean state from the Parallel Ocean Climate Model result have been used to investigate the variation of Kuroshio intrusion and eddy shedding at Luzon Strait during 1992–2001. The Kuroshio penetrates into the South China Sea and forms a bend. The Kuroshio bend varies with time, periodically shedding anticyclonic eddies. Criteria of eddy shedding are identified: 1) When the shedding event occurs, there are usually two centers of high Sea Surface Height (SSH) together with negative geostrophic vorticity in the Kuroshio Bend (KB) area. 2) Between the two centers of high SSH there usually exists positive geostrophic vorticity. These criteria have been used to determine the eddy shedding times and locations. The most frequent eddy shedding intervals are 70, 80 and 90 days. In both the winter and summer monsoon period, the most frequent locations are 119.5°E and 120°E, which means that the seasonal variation of eddy shedding location is unclear.     

重金属锌,铅对菲律宾蛤仔的急性毒性试验

本文研究了必需元素Ｚｎ及非必需元素Ｐｂ对菲律宾蛤仔的急性毒性作用，得到Ｚｎ对其的４８ｈＬＤ５０和９６ｈＬＤ５０分别为１４７．９１、１６．４０ｍｇ／ｄｍ＾３；Ｐｂ对其的４８ｈＬＤ５０和９６ｈＬＤ５０分别为３１．６２、１４．２８ｍｇ／ｄｍ＾３。估算得到Ｚｎ、Ｐｂ对菲律宾蛤仔的安全浓度分别为０．８２、０．７１ｍｇ／ｄｍ＾３。     

Geodynamics of the deep sedimentary basin of the Caspian Sea region: paragenetic correlation of seismicity and mud volcanism

In this paper we analyze seismic regime and earthquake depth distribution and correlation of seismicity and mud volcanism in the Azerbaijan and the Caspian Sea region. For the present region we have calculated accurate source locations, seismic activity, earthquake repetition and released earthquake energy parameters. It is shown that the active tectonic processes in the region are concentrated within the thick sedimentary cover that we consider as a general source of contemporary stress and a main structural element responsible for the origin of regional earthquakes. The correlation of seismicity and mud volcanism is of paragenetic character.     

山东半岛东部诸岛水域叶绿素—a含量和初级生产力

据１９９０．１１－１９９１年８月期间，山东半岛东部诸岛水域调查资料，分析了该水域叶绿素－ａ含量的时空分布和初级生产力的分布与变化，此分布与该水域的温度和营养盐水含量密切相关。叶绿素－ａ含量的季节变化分三种类型，年变幅为０．１１－１２．８１ｍｇ／ｍ＾３，年平均值为１．１７ｍｇ／ｍ＾３。初级生产力夏季〉春季〉秋季〉冬季，年变幅为２３．００－７９１．６０ｍｇ．ｃ／ｍ＾２．ｄ年平均为１５２．０ｍｇ．ｃ／ｍ     

Chemistry of marine resources-ⅩⅨ. The molecule design and synthesis of crow-link type alkyd resin and its enrichment behaviour for potassium ion in sea water

This paper first presents the molecule design and synthesis of crown-link type alkyd resin,and its enrichment behaviour for potassium ion in low concentration solution and sea water.On the basis of some theory concepts of Host-Guest chemistry developed in recent years,we have designed and synthesized a new polymer enrichment agent of crow-link resin for potassiumion,i.e.,polymacrocyclic ether bislactone of diethylene glycolpyromyllitic acid(briefly called crown-link type alkyd resin or PBL resin).The yield was about 97.4%,almost quantitatively.     

GALILEO系统仿真与分析

本文着重阐述了GALILEO仿真系统星座和误差模型的构建过程,利用该系统进行DOP值分析并通过定位解算验证了GALILEO系统的性能指标。通过与GPS系统性能指标进行比较,得出GALILEO系统的星座设计具有较好的DOP值分布特性,定位精度优于GPS定位精度。在进行差分定位时,其误差贡献比较大的是接收机噪声和卫星钟差,因此提高差分定位的关键是降低接收机的噪声水平和提高卫星钟差预报精度。     

基于GIS的区域经济统计分析系统的设计与实现

随着经济的发展,区域间经济相互作用和影响的关系越来越密切,忽略空间相互作用的传统区域经济分析手段和方法开始显现出一些明显的不足。而GIS在处理和分析区域地理数据上具有强大的空间分析能力,为此我们引入GIS工具对区域经济进行分析,相较于传统的分析手法有了很大改善。本文以江西省区域经济数据为例,设计了一个基于GIS的区域经济统计分析系统,并利用Arcob-jects二次开发控件结合VB可视化编程语言,实现了大部分区域经济统计分析功能,最后并将结果进行网络发布。研究结果表明将GIS引入到区域经济统计分析中,更能正确、有效的揭示区域经济发展在空间上的联系,为区域经济研究决策提供服务。     

点质模型求定月球重力场及其特征分析

利用Lunar-Prospector扩展任务的视线加速度数据,根据点质模型恢复了月球近区的重力场,将其与LP165月球重力场模型进行了比较和分析,并利用恢复的重力场联合月球地形数据对Mas-con进行分析,总结了月球重力场的主要特征及其研究方向发展趋势,将重力场恢复技术与我国的探月计划-"嫦娥"工程结合起来,为建立高精度的月球重力场和地形模型提供了一种有效而实用的方法。     

Magnetite-Fluorite Rock: A New Rock Type of Hot Water Sedimentation

The new type hot water sedimentary rock - magnetite-fluorite rock occurs as quasi-layers inflat parts of contact zones between rock body and strata in Bamiaushan of Changshan County,Zhejiang Province, China. The main mineral assemblage is fluorite magnetite cassiterite. The rockshows typical laminated structure and obvious mosaic texture. Its formation temperature is between123℃-160℃, averaging at 142℃. The major chemical composition of the rock includes CaF2, SiO2,Al2O3, FeO, and Fe2O3; the high-content microelement association includes W, Sn, Be, Rb, Sr, S, andCl; and the total content of REE is low (∑REE between 35.34x10-6-38.35x10-6), showing LREEenrichment type of distribution pattern. Diagenesis: driven by the tectonic stress, the formation waterheated in the deep strata had moved along the fissures or fractures in strata and had extractedcomponents from the strata on the way, and finally stagnated in the flat parts of contact zones betweenrock body and strata. With drop in temperature, magnetite and fluorite were separated from the hotwater and precipitated alternately, forming this hot water sedimentary rock with new typemineralogical composition, typical laminated structure, obvious mosaic texture and sub-horizontaloccurrence. The characteristics of the new type mineralogical composition, sedimentary tectonicenvironment and chemical composition are different from that of the well-known traditionalhydrothermai sedimentary rocks.