反相流动注射催化光度法测定废水中的亚硝酸根

采用反相流动注射技术与催化光度法相结合，用微机化流动注射分析仪准确控制反应时间，优化了实验条件，克服了催化光度法反应时间难以控制引起的方法精密度、准确度不高的弱点，拟定了测定痕量亚硝酸根的流动注射催化光度方法。分析速度第小时20次，NO2^- 质量浓度在0．00－2．00mg/L，回归方程斜率为0．155。方法直接测定电厂测水中NO2^-的结果与Griess法相符合，RSD＜5．0％（n=5）。     

云南澜沧江以西的白垩系

云南白垩系分布在滇中、滇西和澜沧江以西三个地域，彼此之间被深断裂所，它们的地质历程、构造特征各不相同。不能将澜沧江以西勐海、潞西地区的白垩系解体归属不同地层区。澜沧江以西的白垩系，分布于冈瓦纳古陆和古特提斯造带的小型山间盆地，地层层序齐全，岩性、厚度稳定，今古生物化石。有两套岩石序列，三个沉积旋回。     

含油气性物化探信息双子波群灰色关联滤波提取

构建了一个考虑两个子波群，增加信息约束条件对研究区物化探信息进行滤波的新模型－双子波关联滤波模型。对模型的分析研究与应用表明，新模型对物化探油气性信息的识别、提取具有更强的能力。     

地震勘探方法在江西九江-瑞昌地区寻找隐伏岩(矿)体的应用及效果

提供了地震勘探方法在金属矿区寻找隐伏火成岩(矿)体的应用技术和地质成果。通过钻探工程验证,其结果与地震解释推断的结论有较好的吻合。这种尝试对拓宽地震勘探服务领域有重大意义。     

Physical structure features of the crust at southeast region of Tibetan Plateau

Chemical reactions of plagioclase, biotite and their single minerals, as well as a mineral mixture of (plagioclase+biotite+quartz), with KCl and (KCl+KHCO₃) solutions were carried out at 150–400°C and 50–80 MPa. Experiments show that alkaline fluid promotes plagioclase’s changing into potash feldspar, while acid fluid helps plagioclase, potash feldspar and biotite alteration form chlorite and sericite. After chemical reaction the acidity-alkalinity of solutions often changes reversely. It was observed that gold dissolved from the tube wall and recrystallized on the surfaces of biotite and pyrite. Therefore the transportation and enrichment of gold are related to the elementary effect of the fluid-mineral interfaces. Fe³⁺-Fe²⁺, as an oxidition-reduction agent, and volatile components Cl^- and CO₂ play important roles in the reaction process     

Magnetotelluric sounding results in eastern Tibetan Plateau

The results of Zayü-Qingshuihe MT sounding profile carried out in eastern Tibetan Plateau are presented in this paper. Using 2-D RRI method, the resistivity distribution with depth is obtained along the profile. It is featured by the resistivity zones in the horizontal direction and layers in the vertical direction. The Bangong-Nujiang suture zone and Jinshajiang suture zone are both important electrical conductivity-separating zones in the plateau, and the former is a zone with relatively low resistivity while the latter is an electrical conductivity gradient zone. The highly electrical conductive bodies in the mid and lower crust of northern Qiangtang and Bayan Har Terrain might be caused by regional melting due to shear heating during the process of subduction in tectonic evolution.     

Preparation and Certification of High-Grade Gold Ore Reference Materials (GAu 19-22)

Two types of gold deposit with both good homogeneity and a high-grade of gold were selected to prepare four gold ore reference materials (GAu-19,GAu-20,GAu-21 and GAu-22) by the Institute of Geophysical and Geochemical Exploration (IGGE),China.Seven laboratories participated in the certification programme. Volumetric methods for GAu19-21 and atomic absorption spectrometry for GAu-22 were used for the homogeneity testing,the coefficient of variation being found to be less than 3%.After sample digestion and preconcentration,the samples were analysed by flame atomic absorption spectrometry (AAS),colorimetry,neutron activation analysis (NAA)and volumetric analysis. The certified values for the gold concentration in GAu19-22 are 18.3 μg g -1, 32.3 μg g -1, 53.0 μg g -1 and 5.72 μg g -1,respectively.     

喜马拉雅构造-成矿域及其成矿效应初步分析

通过近年来的研究 ,提出了全新的喜马拉雅构造 -成矿域概念。从大喜马拉雅构造域及其成矿效应出发 ,通过构造域对矿集区的控制作用、成矿时代、成矿物质来源、深部过程与成矿效应的分析 ,从而较全面地评价了青藏高原及邻区的资源潜力和需要进一步工作的重要成矿带或矿集区。通过分析认为喜马拉雅构造 -成矿域内强烈的壳幔物质交换 ,下地壳翻天覆地的物质和流体交换 ,导致了在同一构造地质单元内可以有一个或多个超大型矿床的存在。并对多个重要矿床类型提出了更切合实际的观点 ,如西藏甲马铜钼银铅锌金多金属矿床属于矽卡岩 -斑岩复合型 ,云南羊拉铜钼金多金属矿床也属于矽卡岩 -斑岩复合型矿床等。在喜马拉雅构造域内形成的燕山晚期或喜马拉雅期矿床大多和大陆地壳深部复杂的动力学过程有关 ,所形成的矿床矿物组合及成矿元素组合复杂 ,特别是矿石中钴、银元素含量较高 ,许多矿床中银、钴已经作为主要成矿元素。最后明确提出了青藏高原主体及东缘重要矿集区的资源潜力     

Trace Elements Analysis of Geological Samples by Laser Ablation Inductively Coupled Plasma Mass Spectrometry

ＩＮＴＲＯＤＵＣＴＩＯＮＬａｓｅｒａｂｌａｔｉｏｎｉｎｄｕｃｔｉｖｅｌｙｃｏｕｐｌｅｄｐｌａｓｍａｍａｓｓｓｐｅｃｔｒｏｍｅ ｔｒｙｉｓａｎｉｎｃｒｅａｓｉｎｇｌｙｄｅｖｅｌｏｐｅｄａｎａｌｙｔｉｃａｌｔｅｃｈｎｉｑｕｅｆｏｒｓｏｌｉｄｓａｍｐｌｅａｎａｌｙｓｉｓ.ＬＡ ＩＣＰ ＭＳｏｆｆｅｒｓａｔｔｒａｃｔｉｖｅｃｈａｒａｃｔｅｒｉｓｔｉｃｓｏｆｈｉｇｈｓｅｎｓｉｔｉｖｉｔｙ ,ｌｏｗｄｅｔｅｃｔｉｏｎｌｉｍｉｔｓ,ｍｉｎｉｍａｌｓａｍｐｌｅｐｒｅｐａｒａ ｔｉｏｎ ,ｌｅｓｓｏｘｉｄｅｓｉｎｔｅｒｆｅ…     

理查逊数和晴空颠簸的关系

对切变气流中重力内波的稳定性进行了数值计算，结果表明，判别晴空颠是否发生的临界Ｒｉ数随波长，层结稳定度和基本气流变强度的不同而有所变化，预报业务中用Ｒｉ〈０．２５作为预报晴空的指标易出现空报。