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121.
122.
THREE-WAY METHODS FOR THE CALIBRATION OF CHROMATOGRAPHIC SYSTEMS:COMPARING PARAFAC AND THREE-WAY PLS
For the calibration of chromatographic systems,different methods can be used.One class of methodsutilizes three-way approaches.The calibration problem is stated in such a way that the decompositionof a three-way array can serve for the prediction of retention on new stationary phases.Two three-way approaches are presented:the Unfold-PCA and PARAFAC models.The theory ofboth methods is presented and the differences are highlighted,the main difference being that PARAFACis a trilinear decomposition whereas Unfold-PCA is not.Both three-way methods are evaluated on asmall data set consisting of retention measurements of eight solutes at six mobile phase compositions onsix stationary phases.The differences in performance of the two models are minor,For calibration purposes,two variants of the methods are discussed:three-way PLS and an extensionof PARAFAC.Again the theory and differences between the two methods are explained.The predictiveperformance of the two methods is compared using the same data set as earlier.The differences inpredictive performance,however,are minor.Both methods are capable of predicting 98% of thevariation in the test sets.Yet,there are other considerations when comparing methods than predictiveperformance,e.g.the quality of the predictions. 相似文献
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Denis Hatzfeld Vassilis Karakostas Maria Ziazia Iannis Kassaras Elephteria Papadimitriou Kostas Makropoulos Nikos Voulgaris and Christos Papaioannou 《Geophysical Journal International》2000,141(2):438-456
During the summer of 1993, a network of seismological stations was installed over a period of 7 weeks around the eastern Gulf of Corinth where a sequence of strong earthquakes occurred during 1981. Seismicity lies between the Alepohori fault dipping north and the Kaparelli fault dipping south and is related to both of these antithetic faults. Focal mechanisms show normal faulting with the active fault plane dipping at about 45° for both faults. The aftershocks of the 1981 earthquake sequence recorded by King et al . (1985 ) were processed again and show similar results. In contrast, the observations collected near the western end of the Gulf of Corinth during an experiment conducted in 1991 ( Rigo et al . 1996 ), and during the aftershock studies of the 1992 Galaxidi and the 1995 Aigion earthquakes ( Hatzfeld et al . 1996 ; Bernard et al . 1997 ) show seismicity dipping at a very low angle (about 15°) northwards and normal faulting mechanisms with the active fault plane dipping northwards at about 30°. We suggest that the 8–12 km deep seismicity in the west is probably related to the seismic–aseismic transition and not to a possible almost horizontal active fault dipping north as previously proposed. The difference in the seismicity and focal mechanisms between east and west of the Gulf could be related to the difference in the recent extension rate between the western Gulf of Corinth and the eastern Gulf of Corinth, which rotated the faults dipping originally at 45° (as in the east of the Gulf) to 30° (as in the west of the Gulf). 相似文献
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????CNES???????????????????λ???????д?????????????????о????????????????????????????????????????????????CNES??????????????????SuomiNet????????????????IGS??????????????????????????????????????????????????к??????? 相似文献
128.
东南极格罗夫山存在一套经历了峰期麻粒岩相变质作用的镁铁质麻粒岩和斜长角闪岩。对含石榴石的镁铁质麻粒岩的详细研究则显示了近等温降压 (ITD)的顺时针PT演化轨迹 ,与拉斯曼丘陵有相似的演化历史。岩石的主量元素组成和玄武岩一致 ,并且具有拉斑玄武岩演化趋势。进一步的地球化学研究表明 ,这套玄武岩为洋岛型玄武岩 (OIB)和洋中脊型玄武岩(MORB)的组合。OIB型具有大体类似的地球化学性质 ,它们均富集Ti(TiO2 =2 .68% )、REE( =2 0 2 μg/g)、LREE[(La/Yb) N=4.8]、Ti/Y( =343)、Zr/Y( =3.1 ) ,具洋岛玄武岩的特征 ,推测岩浆来源于富集地幔源区 (EM)。而MORB型以低Ti (TiO2 =1 .1 %— 1 .31 % ) ,明显低于OIB的P的含量 (P2 O5=0 .1 %— 0 .2 % ) ,低REE ( 4 7— 93μg/g)、LREE/HREE( 2 .2 7— 2 .5 4 )、(La/Yb) N( =1 .30— 1 .62 )为特征 ,具洋中脊玄武岩的特征。MORB和OIB组合的出现说明在泛非期该区可能存在过洋盆。 相似文献
129.
This paper aims to determine the optimal fines content of coarse-grained soil required to simultaneously achieve weaker frost susceptibility and better bearing capacity. We studied the frost susceptibility and strength properties of coarse-grained soil by means of frost heaving tests and static triaxial tests, and the results are as follows:(1) the freezing temperature of coarse-grained soil decreased gradually and then leveled off with incremental increases in the percent content of fines; (2) the fines content proved to be an important factor influencing the frost heave susceptibility and strength properties of coarse-grained soil. With incremental increases in the percent content of fines, the frost heave ratio increased gradually and the cohesion function of fines effectively enhanced the shear strength of coarse-grained soil before freeze-thaw, but the frost susceptibility of fines weakened the shear strength of coarse-grained soil after freeze-thaw; (3) with increasing numbers of freeze-thaw cycles,the shear strength of coarse-grained soil decreased and then stabilized after the ninth freeze-thaw cycle, and therefore the mechanical indexes of the ninth freeze-thaw cycle are recommended for the engineering design values; and (4) considering frost susceptibility and strength properties as a whole, the optimal fines content of 5% is recommended for railway subgrade coarse-grained soil fillings in frozen regions. 相似文献
130.
Water is a necessary element during gas hydrate formations. Therefore, by analyzing water depletion changes in media, the reaction characteristics of methane hydrate in media can be studied. In this study, two water sources supplying some liquid water which may be consumed by the methane hydrate formation reactions were designed and assembled. Using them, the full formation processes of methane hydrate was studied. Experimental results show the following: If heat released from nucleation reaction of methane hydrate is diffused rapidly, the nucleation ratios will be enhanced discernibly. While the hydrate is formed, a force is generated that sucks fresh water from the source into the vicinity of the hydrate, slowing down the cementation process and causing some hydrate grain dissociation. As a result of cementation differences, the hydrate reaction processes with different water sources present linear or quadratic equation characteristics. After a few repeated dissociation and formation processes of some hydrate grains caused by the fresh water, the gas amounts contained in hydrate will be significantly enhanced. 相似文献