傅立叶红外光谱技术在翡翠研究中的应用

基于透射光谱的差异，用傅立叶红外光谱研究翡翠的矿物组成；分析硬玉、霓石、霓辉石和透辉石等主要矿物，以天然翡翠的特征红外光谱为依据，鉴别市售翡翠的真伪和类别（Ａ、Ｂ货）；利用红外显微镜作微区透射光谱，鉴别通常难以鉴别的有裂缝及裂缝填充物的翡翠（Ｂ货），提出了准确的无损鉴别翡翠的方法。     

Determination of the poroelasticity of shale

Shales play important roles in various civil, energy and environmental engineering applications. Shales are categorized as poroelastic materials due to their tight and very stiff structure, and reliable poroelastic properties are required when dealing with shales. This paper presents simple procedures to determine the poroelastic properties of rocks using oedometer and triaxial consolidation tests. The procedures, which avoid the difficulty to perform determination of the unjacketed bulk modulus of the rock minerals, are demonstrated on a North Sea shale. The experimentally obtained Biot coefficient α and the drained bulk modulus K of the shale range from 0.95 to 0.99, and from 0.17 to 2.00 GPa, respectively. The Biot coefficient α and the drained bulk modulus K values determined from the oedometer and triaxial tests are compared and show good agreement and consistency between the two test procedures. The Skempton’s coefficient B-value of the triaxial samples was also experimentally measured prior to the triaxial consolidation tests. The theoretically predicted B-value varies from 0.81 to 0.96 which is, on the average, only about 10% higher than the experimentally obtained B-value which range from 0.80 to 0.85.

     

Changes of visceral properties and digestive enzymes in the herbivorous marine teleost Siganus canaliculatus fed on different diets

The rabbitfish Siganus canaliculatus is one of the few cultured herbivorous marine teleosts. To better understand the digestive physiology of this fish and provide data for designing formulated feed using macroalgae as an ingredient, the changes of visceral properties and digestive enzyme activities were investigated after the juveniles were fed on different types of food including raw fish(RF), formulated diet(FD) or macroalgae Enteromorpha prolifra(EP) and Gracilaria lemaneiformis(GL) for eight weeks. The results showed that the hepatosomatic and viscerosomatic indices in the RF and FD groups, as well as the relative intestine length(RIL) in the EP and GL groups, were significantly higher than those in other groups. Additionally, differences in the histological structure of the liver and anterior intestine were also observed among different dietary groups. The hepatic nuclei were displaced to the periphery by lipid inclusions in fish fed RF. The highest levels of mucosal folds were found in the anterior intestines of fish fed macroalgae. Digestive enzyme activity profiles showed obvious fluctuations in the first three weeks, and then leveled off in the following weeks. The levels of protease, lipase and α-amylase in the alimentary tract showed changes related to the levels of dietary protein, lipid and carbohydrate, respectively.Although macroalgae significantly inhibited the activity of protease in the stomach, it increased RIL and the number of mucosal folds in the anterior intestine so as to compensate for the influences on protease activities in the stomach. This study suggests that the digestive tract of rabbitfish can well adapt to different diets, and needs about three weeks to physiologically acclimatize to the nutritional status, thus implying that rabbitfish are somewhat omnivorous.     

1∶50000空间数据缩编更新方案设计

现势性是地图的基本特性之一。为保持1：50000空间数据的现势性,国家实施了全国1：50000数据库的更新项目,以甘肃永昌测区为例阐述了利用1：10000DLG数据直接缩编更新1：50000空间数据的方法。     

农业干旱灾害风险模糊集对评价法及其应用

开展农业干旱灾害风险评估,有利于定量认识农业旱灾和科学指导防旱抗旱工作。基于集对分析原理和模糊理论建立的模糊集对评价法,兼顾了信息的多尺度特征和评价等级的模糊性,概念清晰,计算简洁。构建了由旱灾危险性子系统、旱灾暴露性子系统、灾损敏感性子系统和抗旱能力子系统组成的干旱灾害风险评估体系和评价指标。将模糊集对评价法应用于2012年安徽省亳州市农业干旱灾害风险评估,研究结果表明,建议方法是可靠的,为农业干旱灾害风险评估提供了一种新途径。     

广西佛子冲铅锌矿田火成岩的时空序列及其对成矿时限的约束

广西佛子冲铅锌矿田火成岩的主要岩石类型有花岗岩、花岗斑岩、花岗闪长岩（石英闪长岩）、花岗闪长斑岩、少斑花岗斑岩、英安斑岩和凝灰岩等。本文共进行了14件火成岩样品的LA-ICP-MS锆石U-Pb测年,其中大冲石英闪长岩侵位于海西期二叠纪（（256.8±2.0）Ma）,糯垌岩体（（152.6±1.2）Ma）和广平岩体（（152.9±2.9）Ma）形成于燕山早期晚侏罗世,花岗斑岩、少斑花岗斑岩、花岗闪长斑岩、英安斑岩和火山角砾凝灰岩形成于燕山晚期早白垩世（约100 Ma）。结合前人的研究成果及14件火成岩样品的测年结果,构建该区火成岩的年代学序列,确定其侵位时代主要集中在志留纪（约440 Ma）、二叠纪末期（约256 Ma）、晚侏罗世（约152 Ma）、早白垩世晚期（约100 Ma）。根据佛子冲铅锌矿的空间展布、矿体特征以及与火成岩的关系,确定花岗斑岩为成矿地质体,进而限定其成矿时代为早白垩世晚期（约100 Ma）。     

顺层岩质滑坡渐进破坏进入加速的能量学判据

顺层岩质滑坡是最常见的斜坡灾害,研究其渐进破坏过程、建立预报判据对于防灾减灾具有重要意义.以秭归杉树槽滑坡为例,在野外调查和室内岩石试验的基础上,利用JRC-JCS模型及GSI法估算得出滑坡基本力学参数;通过FLAC3D模拟滑坡渐进破坏过程,分析顺层岩质滑坡变形破坏的发展规律;基于能量守恒和虚功原理,提出了顺层岩质滑坡迈入加速变形的能量学判据.研究表明:杉树槽滑坡由后缘向前渐进破坏,后缘变形累积的总位移值不断增大,前缘切层段的锁固作用使变形迅速降低,当临近破坏时,前缘位移由前向后发展,滑面快速贯通;滑体沿滑动方向应变曲线可近似表示为"S"型曲线,随渐进破坏该曲线向坡下发展;以滑体动能增量大于0作为滑坡迈入加速变形的能量学判据,其结果符合滑坡地质演化观点,与FLAC3D模拟结果吻合.      

生物和环境样品中痕量溴碘的小体积交换分离与测定

针对微克量级卤素的分离问题,研究了不同形态卤素在７１７阴离子交换柱上的吸附特点。通过离子交换柱的改进和分离条件的选择,实现了卤素与基体以及卤素之间的有效分离。洗脱体积小,盐份浓度低,经水样、土壤和生物样品分析考查,方法可行。     

Preference of the herbivorous marine teleost Siganus canaliculatus for different macroalgae

The decomposition of a large amount of unexploited macroalgal resource along the coast of China often results in heavy environmental pollution. In order to pave a way of using macroalgae as the dietary ingredient of rabbitfish Siganus canaliculatus, one of a few farmed herbivorous marine teleosts in China, its preference （feeding selectivity） for different macroalgae was determined in this study. Seven seaweed species abundantly inhabiting the coast of east Guangdong Province were exposed simultaneously to rab-bitfish juveniles in laboratory （multiple-choice feeding） with their content and absolute intake assayed. It was found that the most preferred algae were Ulva prolifera, Gracilaria lemaneiformis and Chaetomorpha linum, less preferred algae were U. pertusa and Porphyra haitanensis, and least preferred ones were Sargassum fusiforme and Corallina sessilis. Such an order did not change when one to four relatively preferred seaweeds were removed. The preferred seaweeds were richer in protein and soluble sugar thus higher in energy than the least preferred. In addition, this fish was found to favor filamentous and flat algae rather than calcified ones. Ac-cordingly, the richness of nutrients and morphological characteristics determined the preference of S. canaliculatus for tested macro-algae.     

地籍调查中的监理工作

介绍了地籍调查中监理工作的组织程序和工作内容,提出了应建立测绘监理工程师细则规定.