Platinum-Group Element Geochemical Certified Reference Materials (GPt1-7)

Unlike the situation for other elements, few reference materials certified for the platinum-group elements are currently available. Therefore, the GPt1-7 series of PGE geochemical CRMs, prepared by the IGGE, represent an important addition and comprise a range of matrix types, including a soil, stream sediment, Mg-rich ultramafic rock, Fe-rich ultramafic rock, platinoid ore depleted in Cu, Ni and Fe, and a chromitite. The concentration of PGE in these samples ranges over 4-5 orders of magnitude and the samples were shown to have good homogeneity as assessed by a variance test. Analytical methods based on different principles were used in sample certification, including several fire assay and wet chemical procedures used for decomposition and preconcentration. Certified values for the elements Pt, Pd, Os, Ru, Ir, Rh and Au were determined by AAS, catalytic colourimetry (COL), catalytic polarography (POL), atomic emission spectrometry (AES), ICP-MS and NAA. Recently, the GPt1-7 samples were approved as national primary CRMs by the State Bureau of Technical Supervision of China.     

国内外海洋资料浮标技术现状与发展

海洋资料浮标是长期连续进行海洋监测的主要手段之一。本文简单介绍了国内外海洋资料浮标技术的现状与发展及浮标在我国海洋监测中的应用情况,提出了我国资料浮标技术的研究与发展设想。     

Empirical Formula of Shear Strength of Rock Fractures Based on 3D Morphology Parameters

The prime objective of this work is to provide a reference to predict the peak shear strength of rock fractures. The paper studied some shear properties of rock fractures and proposed an empirical formula for the peak shear strength of rock fractures based on 3D morphology parameters. The rock fractures were induced in cylindrical sandstone and marble specimens by means of indirect tension. A rock direct shear apparatus (RDS-200) was adopted to conduct direct shear tests on five groups of rock fractures under different levels of normal load. Before the direct shear test, 3D morphology parameters of rock fracture surfaces were obtained using a 3D optical scanner. By analyses of direct shear test data, the relationships between peak shear strength, peak shear displacement, peak dilatancy angle, residual friction coefficient and peak normal stress were found. According to the evolution trends of peak shear strength and peak dilatancy angle along with the normal stress, an empirical formula was proposed to predict the peak shear strength of rock fractures in both sliding and cutting failure modes considering the 3D morphology parameters of rock fracture surfaces. The empirical formula could be commonly used for different types (sandstone and marble) and grain sizes (powder-grained, fine-grained, medium-grained and coarse-grained) of rock fractures.     

The null distribution of sample serial correlation coefficient

 The null distribution of the lag-k sample serial correlation coefficient (r _k , k=1,2,3) was investigated by Monte Carlo simulation. For a time series with normal, exponential, Pearson 3, EV1 (Gumbel), or generalized Pareto (GP) distribution type, the null distribution of its r _k can be approximated by the normal distribution with mean −1/(n−k) and variance 1/(n−1). But for a time series with the lognormal, EV2 or EV3 (Weibull) distribution type, the null distribution of r _k is skewed distributed. In such cases, a simulation technique is suggested to construct percentile confidence intervals at a given significance level.     

陕西二台子铜金床钠长石碳酸（角砾）岩类特征及形成构造背景分析

从岩石学、矿物学、岩石化学、地球化学、稀土元素等方面研究了二台子铜金矿内长石炭酸（角砾）岩类地质地球化学特征。晚泥盆世－石炭纪,在区域幔羽构造作用下,深部热流体沿先存在构造通道上升进入镇安二台子三级热水沉积盆地之中,形成了石英重晶石炭酸角砾岩、碳酸角砾岩、复成分角砾岩、钠长岩、钠长石碳酸岩,受同性断裂及层位控制明显,并构成了金的矿源层及普遍金矿化。燕山期,具有幔源特征的深部含矿热流体在北东、北西向     

华南阿伦尼格世几丁虫生物地层与古生物地理

本文系统介绍了湖北宜昌黄花场及浙江常山黄泥塘剖面Ａｒｅｎｉｇ统几丁虫分布发育规律，指出华南地区Ａｒｅｎｉｎｇ统的几丁虫自下向上可划分为Ｃｏｎｏｃｈｉｔｉｎａｓｙｍｍｅｔｒｉｃａ，Ｅｒｅｍｏｃｈｉｔｉｎａｂａｃｕｌａｔａ，Ｅｒｅｍｏｃｈｉｔｉｎａｂｒｅｖｉｓ－Ｃｏｎｏｃｈｉｔｉｎａｌａｎｇｅｉ，Ｃｏｎｏｃｈｉｔｉｎａｐｉｒｕｍ，Ｒｈａｂｄｏｃｈｉｔｉｎａｔｕｒｇｉｄａ等生物带。讨论了华南地区这一时期     

显式完全平方守恒差分格式在近岸海流数值模拟中的应用

用显式完全平方守恒差分格式及其改进分解算法对南海月平均流和海面起伏进行了数值模拟，与隐式完全平方守恒差分格式相比，计算时间可省３—５倍，具有良好的时间效益，而且，其计算效果不比隐式完全平方守恒差分格式差。因此，显式完全平方守恒差分格式及其改进分解算法具有良好的实用价值。     

中国雨季的气候学特征

利用全国740站日降水资料,采用多种统计学方法,对两湖流域雨季降水特征进行了分析。结果表明：(1)两湖流域年降水序列可分为5个阶段,其中主雨季从4月的第2候开始,持续到7月的第1候。两湖流域雨季较江淮梅雨来得早,持续的时间长。(2)雨季内以出现2个和3个主雨期模态的可能性较大。其中2个主雨期一般出现在5月上、中旬及6月中、下旬,这种模态在上世纪60年代、90年代表现明显;3个主雨期一般出现在4月中旬、5月中下旬到6月初与6月下旬至7月初,该模态在20世纪60年代后期至70年初、80年代中后期表现明显。(3)两湖流域雨季内降水的准双周(10~20 d)、30~60 d低频振荡现象明显。准双周振动在雨季中表现为5个波动,30~60 d振荡表现为3个完整的波动,波峰分别出现4月上旬、5月上旬及6月中旬,与其降水主模态有较好的对应关系。