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121.
122.
Axel K. Schmitt Kevin R. Chamberlain Susan M. Swapp T. Mark Harrison 《Chemical Geology》2010,269(3-4):386-395
We introduce a technique for U–Pb dating of baddeleyite using secondary ion mass spectrometry (SIMS) in situ analysis of ng-mass crystals that cannot be efficiently extracted by conventional mineral separation techniques. Average 207Pb/206Pb ages for Precambrian baddeleyite crystals are within < 0.3% of the respective isotope dilution thermal ionization mass spectrometry (ID-TIMS) ages. 206Pb/238U ratios are corrected for instrumental fractionation calibrated through linear regression in a Pb/U relative sensitivity vs. UO2+/U+ calibration plot. Calibration is performed on separated baddeleyite crystals (~ 100–200 μm in maximum dimension) mounted in random crystallographic orientation. 206Pb/238U ages for baddeleyite from Duluth gabbro (FC4b) and Kovdor are accurate within 1–2% when averaging 15–30 individual spot analyses and relative sensitivities calibrated on Phalaborwa baddeleyite. The relative difference of 206Pb/238U between large crystals and micro-baddeleyite from FC4b is within ~ 1%. Comparison between silicate glass and baddeleyite, as well as replicate analysis of the same grains in different orientations relative to the incidence direction of the primary beam support previous evidence for bias in Pb/U sensitivity in baddeleyite due to variable crystal orientations. We successfully utilized oxygen flooding and a UO2+/U+-based calibration to significantly reduce orientation dependent bias. 相似文献
123.
Direct measurements of calcite faces were performed using in situ atomic force microscopy (AFM) to reveal the dissolution processes as a function of solution saturation state and temperature. Time-sequential AFM images demonstrated that step velocities at constant temperature increased with increasing undersaturation. The anisotropy of obtuse and acute step velocities appeared to become more significant as solutions approached equilibrium and temperature increased. At saturation state Ω > 0.02, a curvilinear boundary was formed at the intersection of two acute steps and the initially rhombohedral etch pit exhibited a nearly triangular shape. This suggests that the and steps may not belong to the calcite-aqueous solution equilibrium system. Further increase in the saturation state (Ω ? 0.3) led to a lack of etch pit formation and dissolution primarily occurred at existing steps, in accordance with Teng (2004). Analysis of step kinetics at different temperatures yielded activation energies of 25 ± 6 kJ/mol and 14 ± 13 kJ/mol for obtuse and acute steps, respectively. The inconsistencies in etch pit morphology, step anisotropy, and step activation energies from the present study with those of studies far-from-equilibrium can be explained by increased influence of the backward reaction, or growth, near-equilibrium. We propose that the backward reaction occurs preferentially at the acute-acute kink sites. The kinetics and effective activation energies of near-equilibrium calcite dissolution presented in this work provide accurate experimental data under likely CO2 sequestration conditions, and thus are crucial to the development of robust geochemical models that predict the long-term performance of mineral-trapped CO2. 相似文献
124.
Kevin R. Chamberlain Axel K. Schmitt Susan M. Swapp T. Mark Harrison Norbert Swoboda-Colberg Wouter Bleeker Tony D. Peterson Charles W. Jefferson Andrei K. Khudoley 《Precambrian Research》2010
An in situ U–Pb SIMS (IN-SIMS) method to date micro-baddeleyite crystals as small as 3 μm is presented with results from three samples that span a variety of ages and geologic settings. The method complements ID-TIMS geochronology by extending the range of dateable crystals to sizes smaller than can be recovered by physical separation. X-ray mapping and BSE imaging are used to locate target grains in thin section, followed by SIMS analysis on a CAMECA ims 1270, using the field aperture in the transfer column to screen out ions from host phases. Internal age precisions for the method are anticipated to range from 0.1% for Precambrian rocks to 3–7% for Phanerozoic rocks. Results establish a 2689 ± 5 Ma age for mafic dikes in the Wyoming craton, USA, a 1540 ± 30 Ma age for a subaerial lava flow from the Thelon Basin of northern Canada, and a 457 ± 34 Ma age for mafic dikes in the platform sequence of southeastern Siberia. The method is ideal for relatively non-destructive dating of small samples such as extraterrestrial rocks and precious terrestrial samples. 相似文献
125.
Kevin S. Knight 《Physics and Chemistry of Minerals》2010,37(8):529-533
Expressions are presented to allow the simple determination of the magnitudes and directions of the principal axes for the
isothermal compressibility tensor and the isobaric thermal expansion tensor for monoclinic crystals. The method is applied
to re-evaluate the apparently contradictory results that have recently been obtained for the direction of maximum compressibility
in jadeite. The term ‘unit strain’ to describe these second rank tensors is discouraged and the use of the representation
quadric for visualisation of second rank tensors is recommended. 相似文献
126.
Multi-zone fusion crust formation and classification of the 2004 Auckland meteorite (L6, S5, and W0)
James M. Scott Marianne Negrini Kevin Faure Marshall C. Palmer Derek R. Knaack Matthew I. Leybourne 《Meteoritics & planetary science》2023,58(3):328-340
On June 12, 2004, a meteorite passed through Earth's atmosphere and landed under the television in the living room of a house in Auckland, New Zealand. Textural characteristics, the chemistry of olivine (Fa23–24) and orthopyroxene (Fs20.7), and the bulk rock triple oxygen isotopes (δ17O + 3.1; δ18O + 4.2‰) from the interior of the completely unweathered (W0) 1.3 kg meteorite, hereafter referred to as Auckland, suggest it to be a strongly metamorphosed fragment from the interior of a low iron ordinary chondrite (L6) parent asteroid. The occurrence of maskelynite but shock fracturing of olivine and pyroxene indicates Auckland experienced extreme shock metamorphism (S5), likely during Ordovician fragmentation of the asteroid parent. The fusion crust consists of three zones: (1) an innermost zone containing narrow Fe-Ni-S-bearing veins that migrated along pre-existing shock fractures in olivine and pyroxene; (2) a middle zone in which the meteorite partially melted to form a silicate glass and immiscible blebs of metal and troilite, and is accompanied by unmelted silicate minerals; and (3) an approximately 0.1 mm wide vesicular-rich outermost layer that largely melted, volatilizing sulfides, before quenching to form glass and olivine. Oxygen isotope values of the bulk rock and/or maskelynite of melted rim and modified substrate are 2–3‰ greater than the meteorite interior and indicate that up to 19% of terrestrial atmospheric O2 was incorporated into the fusion crust during the formation. The fusion crust migrated inwards as ablation occurred, enabling melting, migration, and re-precipitation ± loss of sulfide and metal components, with the prominent glassy rim therefore forming from an already chemically modified zone. 相似文献
127.
Andrea Pieroni Anely Nedelcheva Avni Hajdari Behxhet Mustafa Bruno Scaltriti Kevin Cianfaglione Cassandra L. Quave 《山地科学学报》2014,11(1):180-193
Ethnobotanical studies in the Balkans are crucial for fostering sustainable rural development in the region and also for investigating the dynamics of change of Traditional Ecological Knowledge (TEK), which has broad-sweeping implications for future biodiversity conservation efforts. A survey of local botanical and medical knowledge and practices was conducted in four mountainous villages of the Peshkopia region in northeast Albania, near the Macedonian border. Snowball sampling techniques were employed to recruit 32 informants for participation in semi-structured interviews regarding the use of the local flora for food, medicinal, veterinary and ritual purposes. The uses of 84 botanical taxa were recorded as well as a number of other folk remedies for the treatment of both humans and livestock. Comparison of the collected data with another ethnobotanical field study recently conducted among Albanians living on the Macedonian side of Mount Korab shows a remarkable divergence in medicinal plant uses, thus confirming the crucial role played by the history of the last century in transforming TEK. Most noteworthy, as a legacy of the Communist period, a relevant number of wild medicinal taxa are still gathered only for trade rather than personal/familial use. This may lead to unsustainable exploitation of certain taxa (i.e. Orchis and Gentiana spp.) and presents some important conservation challenges. Appropriate development and environmental educational frameworks should aim to reconnect local people to the perception of limitation and renewability of botanical resources. 相似文献
128.
Maya P. Bhatt William H. McDowell Kevin H. Gardner Jens Hartmann 《Environmental Earth Sciences》2014,71(2):911-922
Water quality in less-developed countries is often subject to substantial degradation, but is rarely studied in a systematic way. The concentration and flux of major ions, carbon, nitrogen, silicon, and trace metals in the heavily urbanized Bagmati River within Kathmandu Valley, Nepal, are reported. The concentrations of all chemical species increased with distance downstream with the exceptions of protons and nitrate, and showed strong relationships with population density adjacent to the river. Total dissolved nitrogen (TDN), dominated by NH4, was found in high concentrations along the Bagmati drainage system. The export of dissolved organic carbon (DOC) and TDN were 23 and 33 tons km?2 year?1, respectively, at the outlet point of the Kathmandu Valley, much higher than in relatively undeveloped watersheds. The cationic and silica fluxes were 106 and 18 tons km?2 year?1 at the outlet of the Bagmati within Kathmandu Valley, and 36 and 32 tons km?2 year?1 from the relatively pristine headwater area. The difference between headwaters and the urban site suggests that the apparent weathering flux is three times higher than the actual weathering rate in the heavily urbanized Bagmati basin. Fluxes of cations and silica are above the world average, as well as fluxes from densely populated North American and European watersheds. End-member composition of anthropogenic sources like sewage or agricultural runoff is needed to understand the drivers of this high rate of apparent weathering. 相似文献
129.
Roger H. Mitchell Peter C. Burns Kevin S. Knight Christopher J. Howard Anton R. Chakhmouradian 《Physics and Chemistry of Minerals》2014,41(6):393-401
Laboratory powder XRD patterns of the perovskite-group mineral lueshite from the type locality (Lueshe, Kivu, DRC) and pure NaNbO3 demonstrate that lueshite does not adopt the same space group (Pbma; #57) as the synthetic compound. The crystal structures of lueshite (2 samples) from Lueshe, Mont Saint-Hilaire (Quebec, Canada) and Sallanlatvi (Kola, Russia) have been determined by single-crystal CCD X-ray diffraction. These room temperature X-ray data for all single-crystal samples can be satisfactorily refined in the orthorhombic space group Pbnm (#62). Cell dimensions, atomic coordinates of the atoms, bond lengths and octahedron tilt angles are given for four crystals. Conventional neutron diffraction patterns for Lueshe lueshite recorded over the temperature range 11–1,000 K confirm that lueshite does not adopt space group Pbma within these temperatures. Neutron diffraction indicates no phase changes on cooling from room temperature to 11 K. None of these neutron diffraction data give satisfactorily refinements but suggest that this is the space group Pbnm. Time-of-flight neutron diffraction patterns for Lueshe lueshite recorded from room temperature to 700 °C demonstrate phase transitions above 550 °C from Cmcm through P4/mbm to \(Pm\overline{3} m\) above 650 °C. Cell dimensions and atomic coordinates of the atoms are given for the three high-temperature phases. The room temperature to 400 °C structures cannot be satisfactorily resolved, and it is suggested that the lueshite at room temperature consists of domains of pinned metastable phases with orthorhombic and/or monoclinic structures. However, the sequence of high-temperature phase transitions observed is similar to those determined for synthetic NaTaO3, suggesting that the equilibrated room temperature structure of lueshite is orthorhombic Pbnm. 相似文献
130.
Anastasia Petrenko Anton Sizo Winchel Qian A. Dylan Knowles Amin Tavassolian Kevin Stanley Scott Bell 《Transactions in GIS》2014,18(3):351-369
The popularization of tracking devices, such as GPS, accelerometers and smartphones, have made it possible to detect, record, and analyze new patterns of human movement and behavior. However, employing GPS alone for indoor localization is not always possible due to the system's inability to determine location inside buildings or in places of signal occlusion. In this context, the application of local wireless networks for determining position is a promising alternative solution, although they still suffer from a number of limitations due to energy and IT‐resources. Our research outlines the potential for employing indoor wireless network positioning and sensor‐based systems to improve the collection of tracking data indoors. By applying various methods of GIScience we developed a methodology that can be applicable for diverse human indoor mobility analysis. To show the advantage of the proposed method, we present the result of an experiment that included mobility analysis of 37 participants. We tracked their movements on a university campus over the course of 41 days and demonstrated that their movement behavior can be successfully studied with our proposed method. 相似文献