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41.
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β-环糊精包合态三氟氯氰杀虫剂的制备 总被引:3,自引:0,他引:3
为了进一步提高三氟氯氰菊酯农药的防治效果。寻找适宜的农药新剂型,我们用液相法制备了三氟氯氰菊酯-β-环糊精包合物,并以水为基质进行了稳定性观察,同时又以差热分析法和气相色谱法确认了包合物的形成,以旋光度法证明两者间的包合比。结果表明,三氟氯氰菊酯与β-环糊精可形成1:1型包合物,该包合物稳定性高,具有一定的水溶性,而且在水中稳定,所以有望通过环糊 包合作用将三氟氯氰菊酯帛成水剂;当以气相法测试包合态三氟氯氰菊酯含量时,必须将其解络,使之成为游离状态,然后按常规方法进行含量测定。 相似文献
43.
本文对松辽盆地东南部后五家户气田划分出22种沉积微相,建立7种相层序,分析了扇三角洲及三角洲沉积环境对天然气成藏的控制作用。指出了扇三角洲前缘砂体和三角洲前缘砂体较为发育,沉积物源来自气田东北部和东南部两个方向。后五家户气田多为构造—岩性气藏和岩性气藏。 相似文献
44.
Introduction The Western Kunlun Mountain Pass M=8.1 earthquake occurred on November 14, 2001 is the other M=8 earthquake occurred 50 years after Dangxiong, Tibet M=8.0 earthquake in Chinese mainland. The earthquake has caused the attention of the seismologists in the following aspects: 1) The fracture length is more than 400 km, which is far away from the estimated length by the statistic empirical function between the magnitude and the fracture length (WANG, et al, 2002); 2) The aftersh… 相似文献
45.
Stanley N. Davis Stephen Moysey DeWayne L. Cecil Marek Zreda 《Hydrogeology Journal》2003,11(2):217-227
Natural production of the radionuclide chlorine-36 (36Cl) has provided a valuable tracer for groundwater studies. The nuclear industry, especially the testing of thermonuclear
weapons, has also produced large amounts of 36Cl that can be detected in many samples of groundwater. In order to be most useful in hydrologic studies, the natural production
prior to 1952 should be distinguished from more recent artificial sources. The object of this study was to reconstruct the
probable preanthropogenic levels of 36Cl in groundwater in the United States. Although significant local variations exist, they are superimposed on a broad regional
pattern of 36Cl/Cl ratios in the United States. Owing to the influence of atmospherically transported ocean salt, natural ratios of 36Cl/total Cl are lowest near the coast and increase to a maximum in the central Rocky Mountains of the United States.
Electronic Publication 相似文献
46.
Andesitic pillow lavas containing biogenic, solid bitumen (SB) are a constituent of a Neoproterozoic volcanosedimentary sequence (Teplá-Barrandian unit, Bohemian Massif) in the Mítov area of the Czech Republic. A black shale formation that is crosscut by these andesitic basalts is 565 Ma old. Carbon disulfide extracts of two powdered samples of SB contain 0.2 and 0.3 ppm of C60, respectively, as determined by high-pressure liquid chromatography. The peak assignment based on retention time is fully supported by high-resolution electron ionization mass spectrometry (EI-MS). No C70 was detected, nor was C60 found in two other SB samples from this locality. Other investigated carbonaceous samples from Bohemia (coals and anthracites of Upper Paleozoic age and anthraxolite, graphitoids, and graphite of Upper Proterozoic age) did not contain fullerenes at concentrations above the detection limit of 0.01 ppm. The absence of C60 in these samples was confirmed by EI-MS. The proposed mechanism of fullerene formation involves a primary algal phase, generation of a hydrocarbonaceous mixture in the course of thermal evolution of the sedimentary series, and their high-temperature transformation related to the extrusion of basalt. An important feature for fullerene conservation was the enclosure of fullerenes in SB with a structure similar to glasslike carbon, where the fullerene was protected against oxidation. 相似文献
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Simulation of multigaussian stochastic fields can be made after a Karhunen-Loéve expansion of a given covariance function.
This method is also called simulation by Empirical Orthogonal Functions. The simulations are made by drawing stochastic coefficients
from a random generator. These numbers are multiplied with eigenfunctions and eigenvalues derived from the predefined covariance
model. The number of eigenfunctions necessary to reproduce the stochastic process within a predefined variance error, turns
out to be a cardinal question. Some ordinary analytical covariance functions are used to evaluate how quickly the series of
eigenfunctions can be truncated. This analysis demonstrates extremely quick convergence to 99.5% of total variance for the
2nd order exponential (‘gaussian’) covariance function, while the opposite is true for the 1st order exponential covariance
function. Due to these convergence characteristics, the Karhunen-Loéve method is most suitable for simulating smooth fields
with ‘gaussian’ shaped covariance functions. Practical applications of Karhunen-Loéve simulations can be improved by spatial
interpolation of the eigenfunctions. In this paper, we suggest interpolation by kriging and limits for reproduction of the
predefined covariance functions are evaluated. 相似文献
50.