刺参中皂苷组分蒸发光散射-高效液相特征图谱研究

采用高效液相色谱-蒸发光散射(HPLC-ELSD)法建立了刺参皂苷的特征图谱.方法:色谱柱为Symmetry C18(150 mm×4.6 mm,5 μm),采用0.2% 乙酸水溶液-乙腈进行梯度洗脱,流速1.0 mL/min;柱温30 ℃;漂移管温度70 ℃;载气压力25 psi.结论:方法具有良好的专属性,可以作为刺参类产品是否含有刺参皂苷的评价方法.     

台风影响期间的河道水位设防标准研究

针对台风影响期间的河道设防标准提出1种新的计算方法(三维复合极值分布模型),同时比较规范推荐的Pearson-Ⅲ方法以及其它几种适线方法的计算结果,在三维概率预测模型和单因素概率模型的比较过程中,阐述了三维复合极值分布模型在样本选取、多重致灾因素的选取、计算结果稳定性等多方面的先进性和合理性。     

Diel vertical migration of mesozooplankton in the northern Yellow Sea

The Yellow Sea Cold Water Mass (YSCWM), one of the most vital hydrological features of the Yellow Sea, causes a seasonal thermocline from spring to autumn. The ...     

Climatology and seasonal variability of satellite-derived chlorophyll a around the Shandong Peninsula

The chlorophyll a (Chl a ) is an important indicator of marine ecosystems. The spatiotemporal variation of the Chl a greatly affects the mariculture and marine ...     

浅谈两要素自动雨量监测站的检修

通过对两要素自动雨量监测站的多次检查维修经验教训的总结,摸索出一套检修方法和步骤,同时对自动雨量监测站提出了一些积极的建议和设想,对自动雨量监测站今后的建设和维护维修起到很好的借鉴作用。     

Simultaneous quantification of greenhouse gas and nitric oxide emissions from subtropical conventional vegetable systems: a 2-site field case study in Sichuan Basin

Quantification of greenhouse gases[nitrous oxide(N₂O)and methane(CH₄)]and nitric oxide(NO)emissions from subtropical conventional vegetable systems through multi-site field measurements are needed to obtain accurate regional and global estimates.N2 O,NO and CH4 emissions from subtropical conventional vegetable systems were simultaneously measured at two different sites with hilly topography in the Sichuan basin,southwest China by using the static chamber gas chromatography technique.Results showed that annual soil N₂O and NO fluxes for the treatment receiving N fertilizer ranged from 6.34-7.71 kg N ha^-1 yr^-1 and 0.69-0.85 kg N ha^-1 yr^-1,respectively,while decreased soil CH4 uptakes by 26.4%as compared with no N fertilizer addition across our two sites of experiment.Overall,the average direct N2 O and NO emission factor(EFd)were 0.71%and 0.12%,respectively,which were both lower than the available EFd for subtropical conventional vegetable systems.This finding indicates that current regional and global estimates of N₂O and NO emissions from vegetable fields are likely overestimated.Background N₂O emissions(3.42-3.62 kg N ha^-1 yr^-1)from the subtropical conventional vegetable systems were relatively high as compared with available field measurements worldwide,suggesting that background N₂O emissions cannot be ignored for regional estimate of N₂O emissions in subtropical region.Nevertheless,the significantly intra-and inter-annual variations in N₂O,CH₄ and NO emissions were also observed in the present study,which could be explained by temporal variations of environmental variables(i.e.soil temperature and moisture).The differences in N₂O and NO EFd and CH₄emissions between various vegetable systems in particular under subtropical conditions should be taken into account when compiling regional or global inventories and proposing mitigation practices.     

高温高压模拟实验气态产物碳同位素演化特征

对泥炭、褐煤样品进行了高压（０．１～２ＧＰａ）、高温（２００～８００℃）模拟实验,并用微量气体同位素测定系统（ＧＣ－Ｃ－ＭＳ）测定了气态产物的碳同位素值。在４００℃的温度条件下,乙烷、丙烷、正丁烷碳同位素值有随压力升高而变重的趋势,并出现了碳同位素局部反序的特征（δ＾１３Ｃ２〉δ＾１３Ｃ３）;在６００℃、１ＧＰａ和１．５ＧＰａ的温压条件下,甲烷和乙烷的δ＾１３（ＰＤＢ）值偏重,分别约为－１５．０‰     

冲绳海槽Jade热液活动区块状硫化物的铅同位素组成及其地质意义

新测行Ｊａｄｅ热液活动区中５件块状硫化物样品的铅同位素组成,具有较小的变化范围,表现出较均一的铅同位素组成特征。在Ｐｂ－Ｐｂ图解上,块状硫化物的铅同位素数据构成线形排列,与该区沉积物和蚀变火山岩的铅同位素组成一致,而与该区新鲜火山岩相比具较高的放射成因铅,证实了该区海底块状硫化物中的铅是由沉积物长英质火山岩来源铅共同构成的混合铅。不同热液活动区铅同位素组成对比研究表明,地质－构造环境的不同是导致各     

空间GPS无线电掩星反演大气参数方法及其应用

给出了空间无线电掩星反演大气参数的原理及其误差估计方法,介绍了国内外在该领域的研究进展。并针对该技术的一些特点,指出了若干尚需解决的问题。     

京郊门城镇地面塌陷危险性研究

采空地面塌陷是门城镇地区危害性最严重的地质灾害类型。根椐实地勘察资料 ,论述了地面塌陷的分布特征和形成条件 ;选取与塌陷密切相关的 1 1个因素 ,采用二级模糊综合评判法对地面塌陷的危险度进行了分区预测。