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181.
Etienne Balan Marc Blanchard Michele Lazzeri Jannick Ingrin 《Physics and Chemistry of Minerals》2014,41(2):105-114
Water incorporation in forsterite samples synthesized under low to medium silica-activity conditions mostly occurs via a substitutional mechanism in which a Si vacancy is compensated by four protons. Corresponding IR absorption spectra display a cluster of narrow and weakly anharmonic OH-stretching bands at wavenumbers above 3,500 cm?1. However, this diagnostic spectrum is often superimposed to one broader absorption band, rarely two, displaying pronounced temperature-dependent properties and tentatively assigned to H atoms in interstitial position (Ingrin et al. in Phys Chem Miner 40:499–510, 2013). Here, we investigate the structural and vibrational properties of selected interstitial H-bearing defects in forsterite using a first-principles modeling approach. We show that the broad bands discussed by Ingrin et al. (Phys Chem Miner 40:499–510, 2013) are most likely related to interstitial OH groups in the vacant octahedral sites alternating with the M2 sites along the c axis of the forsterite structure. The corresponding OH defects lead to the formation of fivefold coordinated Si species. Their peculiar thermal properties stem from the vibrational phase relaxation due to the anharmonic coupling of the high-energy local OH-stretching mode with a low-energy vibrational mode. This “exchange mode” corresponds to the hindered longitudinal translation of the OH group. These results suggest that at high pressure, hydrogen incorporation in forsterite is dominated by coexisting interstitial OH groups and (4H)Si defects. 相似文献
182.
François Guillot Urs Schaltegger Jean-Michel Bertrand Étienne Deloule Thierry Baudin 《International Journal of Earth Sciences》2002,91(6):964-978
Among the Middle Penninic basements of the Internal NW-Alps, the Ruitor massif shows the best preserved remnants of pre-Permian metamorphic rocks. Their Barrovian-type mineral associations are somewhat masked by the greenschist to blueschist Alpine metamorphism of Tertiary age. Four Ruitor gneisses have been analysed, showing geochemical characters of granitoids from orogenic zones. Zircon morphology also suggests magmatic protoliths and a crustal source; some of the morphological zircon types suggest anatectic granites. The first U-Pb ages on zircon for this massif have been obtained concurrently through conventional multigrain and ion microprobe dating. Two metavolcanic rocks at 471LJ and 468ᆪ Ma could be slightly older than the porphyritic augen gneisses at 465ᆟ and 460lj Ma. Regional data from the other Internal basement massifs suggest that the Variscan event is poorly recorded, except in Ruitor-type units. Ruitor and Sapey gneisses belonged to the same unit (Nappe des Pontis), which was affected by a 480-450-Ma event including volcanism and anatexis and ended with a late calc-alkaline granite emplacement at 460-450 Ma. The distribution of Variscan basement units roughly parallels Alpine zonation. 相似文献
183.
184.
汉诺坝幔源单斜辉石巨晶氢同位素组成的离子探针分析:微尺度不均一性 总被引:3,自引:0,他引:3
运用离子探针技术测定了河北汉诺坝新生代玄武岩中3个单斜辉石巨晶的氢同位素组成,结果显示同一颗粒内部表现出微尺度的不均一性,2mm范围内δD的变化达到60‰。δD和氢含量之间不存在同步的变化,巨晶内部的化学成分均一,因此我们认为巨晶的氢同位素不均一性继承自母岩浆。母岩浆的氢同位素变化可能是去气过程中气相与熔体之间的分馏引起的。单斜辉石巨晶形成后很短的时间内即被寄主岩浆带至地表并经历了快速淬火。 相似文献