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111.
112.
Gianfranco?Di VincenzoEmail author Cecilia?Viti Sergio?Rocchi 《Contributions to Mineralogy and Petrology》2003,145(6):643-658
Biotite is one of the most common minerals dated by the 40Ar–39Ar method. It frequently shows K contents below the expected stoichiometric value, suggesting the presence of low-K impurities. The most common low-K alteration product of biotite is chlorite. Therefore, it is important to understand the effects of chlorite interlayering on 40Ar–39Ar ages in order to correctly interpret 40Ar–39Ar data. This study examines the outcome of 40Ar–39Ar dating analyses on variably chloritised biotites from Ordovician intrusive rocks. The infrared (IR) laser-probe technique and different gas extraction methods were adopted. Incremental laser-heating data on bulk samples yielded hump-shaped age profiles with meaningless young and old age steps. Both the extent of anomalous old age steps and the degree of discordance of the age spectra were much more pronounced in the more chloritised biotite samples. In contrast, in situ data on rock chips and total-fusion ages on single biotite flakes yielded ages concordant with, or younger than, the inferred emplacement ages. Transmission electron microscopy (TEM) was used to texturally characterise biotite samples at the nanometre scale. It was also used to document the complex decomposition-transformation process affecting interlayered biotite–chlorite during in-vacuo IR-laser heating to temperatures ranging from ~600 to >1,000 °C. TEM results suggest that hump-shaped age profiles result from an interplay between 39ArK
redistribution by recoil during sample irradiation and differential release of argon isotopes hosted in three main reservoirs. These reservoirs are (from least to most retentive): extended defects, chlorite and biotite. The final descending age segment is attributed to the progressive release of argon with increasing temperature from large biotite domains for which 39ArK recoil loss was less important. 40Ar–39Ar data support previous findings, which suggest that 40Ar–39Ar ages when recoil effects are minimised, provide minimum estimates that approach the true biotite age, when the pristine domains are analysed. The most effective approach for obtaining meaningful 40Ar–39Ar ages was using individual total-fusion analyses on carefully selected, single flakes previously split along the basal cleavage by wet-grinding and corresponding to a sample mass of a few micrograms.Editorial responsibility: I Parsons 相似文献
113.
Characterisation of Soot Emitted by Domestic Heating,Aircraft and Cars Using Diesel or Biodiesel 总被引:1,自引:0,他引:1
Anne?Smekens Ricardo?Henrique?Moreton?Godoi Patrick?Berghmans René?Van?GriekenEmail author 《Journal of Atmospheric Chemistry》2005,52(1):45-62
The characterisation of aggregates, like soot, firstly requires the determination of the size distribution of the primary
particles. The primary particle size of combustion generated aggregates depends upon the combustion environment and the formation
conditions, such as temperature, pressure and fuel-to-air ratio, among others. Since the combustion characteristics are different
in the different types of burners, the characterisation of primary particles may offer the possibility to distinguish soot
from different sources. In this paper, we present the signature of the primary particles and the aggregates of soot emitted
by cars using diesel or biodiesel, by domestic heating, and by aircraft exhausts, which can be considered as the major sources
as derived from measurements on transmission electron micrographs. The size distributions of all aggregates types with different
aerodynamic diameter were log-normal and quasi-monodisperse. The size distribution of the primary particles for soot emitted
by different sources showed minor differences. However, a comparison between the diameter of the primary particles and those
obtained using a standard method for carbon black revealed discrepancies. The median diameter of the primary particles was
combined with the median number of primary particles in an aggregate to calculate the relative particle surface area available
for adsorption. In a similar way, the relative specific surface area was determined. The surface area was measured using the
Brunauer-Emmett-Teller (B.E.T.) nitrogen adsorption method and the relative surface area available for adsorption was calculated. 相似文献
114.
Metallothioneins (MTs) are small, cysteine-rich proteins which detoxify xenobiotic metals such as cadmium (Cd) and mercury (Hg). In crustaceans and mammals they consist of two independent domains which are folded around metal-thiolate clusters. MT clusters of different origins, exhibiting distinct, highly conserved cysteine positions on their sequences, show differences in metal-cysteine coordination and reactivity. Lobster-MT, containing two Cd3 beta domains, is an important model for structure-function relationships among the clusters. The influence of (1) the position of the cysteine residues and (2) steric and electrostatic effects of neighboring amino acids on the folding and stability of MT cluster were investigated. Thus, the native lobster beta C and beta N domains (each having nine cysteines and binding three M2+ ions) and a modified domain Cd3 beta C-->N, in which the cysteines of the C-terminal domain were relocated to match the positions of those in the N-terminal domain, were chemically prepared and characterized. The synthetic native domains (Cd3 beta C and Cd3 beta N) were found to exhibit spectroscopic properties, metal-binding affinities and kinetic reactivity similar to the holo-protein. However, the modified Cd3 beta C-->N domain was unusually reactive and in the presence of Chelex, metal chelation resin, aggregated to a Cd5(beta C-->N)2 dimer, which exhibited unusual structure as observed by its 113Cd-nuclear magnetic resonance. These differences in structure and reactivity demonstrated that the requirements for formation of a stable Cd3S9 beta-cluster are more stringent than simply the sequential positions of the cysteines along the peptide chain and must include interactions involving neighboring, noncysteine amino acids. 相似文献
115.
Seok-Gwan?Choi Eun-A?Yoon Doo-Hae?An Sangdeuk?Chung Jaebong?Lee Kyounghoon?LeeEmail author 《Ocean Science Journal》2018,53(4):667-677
In this study, the dB difference and characteristics of krill swarms inhabiting Subarea 48.1, which includes the west and south of the South Shetland Island and the Elephant Island peripheries, were estimated to distinguish Antarctic krill, using acoustics. From April 13 to 24, 2016, acoustic data were collected along 24 survey lines using the frequencies 38 and 120 kHz, and middle trawling was performed at 7 stations. Using the difference between the dB values of two volume backscattering strength (Sv) frequencies (38 and 120 kHz), a clear acoustic distinction could be made between Antarctic krill (4.9 to 12.0 dB) and fish (?4.0 to ?0.2 dB). The distributions and mean Sv of krill swarms in the Elephant Island peripheries and south of South Shetland Island were higher than those in the west of South Shetland Island. The mean length/ height ratio of krill swarms in the west of the South Shetland Island (64.5) was higher than that in the south (35.9) and the Elephant Island peripheries (33.8), with the length of the aggregations exceeding their height. Most krill swarms were distributed between the surface layer (less than 10 m below sea level) and within 200 m of water depth. These results are expected to serve as baseline data for evaluating krill density and biomass by distinguishing them from fish, using acoustics. 相似文献
116.
117.
Norihisa?UsuiEmail author Shiro?Ishizaki Yosuke?Fujii Masafumi?Kamachi 《Journal of Oceanography》2011,67(3):253-262
We assess validity of a Gaussian error assumption, the basic assumption in data assimilation theory, and propose two kinds
of constraints regarding non-Gaussian statistics. In the mixed water region (MWR) off the east coast of Japan exhibiting complicated
frontal structures, a probability density function (PDF) of subsurface temperature shows double peaks corresponding to the
Kuroshio and Oyashio waters. The complicated frontal structures characterized by the temperature PDF sometimes cause large
innovations, bringing about a non-Gaussianity of errors. It is also revealed that assimilated results with a standard three-dimensional
variational (3DVAR) scheme have some issues in MWR, arising from the non-Gaussianity of errors. The Oyashio water sometimes
becomes unrealistically cold. The double peaks seen in the observed temperature PDF are too smoothed. To improve the assimilated
field in MWR, we introduce two kinds of constraints, J
c1 and J
c2, which model the observed temperature PDF. The constraint J
c1 prevents the unrealistically cold Oyashio water, and J
c2 intends to reproduce the double peaks. The assimilated fields are significantly improved by using these constraints. The
constraint J
c1 effectively reduces the unrealistically cold Oyashio water. The double peaks in the observed temperature PDF are successfully
reproduced by J
c2. In addition, not only subsurface temperature but also whole level temperature and salinity (T–S) fields are improved by
adopting J
c1 and J
c2 to a multivariate 3DVAR scheme with vertical coupled T–S empirical orthogonal function modes. 相似文献
118.
Altimeter data and output from the HYbrid Coordinate Ocean Model global assimilation run are used to study the seasonal variation
of eddy shedding from the Kuroshio intrusion in the Luzon Strait. The results suggest that most eddy shedding events occur
from December through March, and no eddy shedding event occurs in June, September, or October. About a month before eddy shedding,
the Kuroshio intrusion extends into the South China Sea and a closed anticyclonic eddy appears inside the Kuroshio loop which
then detaches from the Kuroshio intrusion. Anticyclonic eddies detached from December through February move westward at a
speed of about 0.1 m s−1 after shedding, whereas eddies detached in other months either stay at the place of origin or move westward at a very slow
speed (less than 0.06 m s−1). The HYCOM outputs and QuikSCAT wind data clearly show that the seasonal variation of eddy shedding is influenced by the
monsoon winds. A comparison between eddy volume and integrated Ekman transport indicates that, once the integrated Ekman transport
exceeds 2 × 1012 m3 (which roughly corresponds to the volume of an eddy), the Kuroshio intrusion expands and an eddy shedding event occurs within
1 month. We infer that the Ekman drift of the northeasterly monsoon pushes the Kuroshio intrusion into the SCS, creates a
net westward transport into the Strait, and leads to an eddy detachment from the Kuroshio. 相似文献
119.
120.
Eitarou?OkaEmail author Bo?Qiu Shinya?Kouketsu Kazuyuki?Uehara Toshio?Suga 《Journal of Oceanography》2012,68(2):355-360
Available Argo profiling float data from 2002 to 2011 were analyzed to examine the effect of the Kuroshio Extension (KE) current
system variability on the formation of the Central Mode Water. Just north of the upstream portion of the KE at 140–152°E,
formation of a lighter variety of the Central Mode Water in winter was active during the unstable period of the upstream KE
in 2006–2009 and was reduced when the upstream KE was in the stable period of 2002–2005 and 2010–2011. This decadal formation
variability is out of phase with that of the Subtropical Mode Water just south of the KE. 相似文献