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441.
石英岩化学成分分析标准物质研制 总被引:4,自引:4,他引:0
目前巴西、英国、日本、南非等国研制有一些石英岩类标准物质,SiO2含量均在96%以上,含量范围较窄,定值元素较少。我国尚无石英岩类的标准物质,无法满足石英岩勘查和实际应用的需要。本文研制了3个石英岩化学成分分析标准物质,样品采自我国具有代表性的安徽省凤阳县大庙镇老青山、青海省大通县景阳镇和湖北省蕲春县灵虬山三个石英矿区,利用流化床式气流粉碎机将样品细碎至-45 μm,解决了纯度较高的石英岩粉碎加工易受污染的难题。因石英岩样品难以压制成型,均匀性检验未采用压片制样X射线荧光光谱法,而是采用以电感耦合等离子体发射光谱法和电感耦合等离子体质谱法为主的检验方法。结果表明,方差检验的F值均小于临界值,证明其均匀性符合要求。为期两年的长期稳定性8次检验中未发现统计学意义上的明显变化,在颠震和极端温度条件下所检验的短期稳定性良好。经我国十家实验室使用多种分析方法联合定值,同时探索采用类似元素比较法获取未进行均匀性和稳定性检验的成分的相应不确定度分量,给出了36个成分的认定值(或参考值)和相应的不确定度。3个标准物质现已被批准为国家一级标准物质(编号GBW 07835、GBW 07836、GBW 07837),其主要成分SiO2的含量相应为92.93%、95.97%、99.18%,呈梯度分布。此系列标准物质具有样品粒度均匀、粒度分布范围窄(D25~D75在4~16 μm之间),定值元素种类多,SiO2含量分布广泛的特点,可以满足石英岩样品化学成分分析过程中监控的需要。 相似文献
442.
为研究一种有效、合理的测定路基动模量的方法,在分析便携式地震波地质分析仪的工作原理和测试特点的基础上,根据弹性动力学和表面波谱分析理论,阐述了便携式地震波地质分析仪的测试原理,并推导了测试路基动模量计算公式。结合路基测试实际工作要求,提出了便携式地震波地质分析仪器的测试步骤及技术要点。通过在路基进行大量点点对应的便携式地震波地质分析仪、便携式落锤弯沉仪和承载板回弹模量测试以及动态圆锥贯入仪贯入测试和灌砂法压实度测试,建立了便携式地震波地质分析仪动模量与其他各指标之间的相关关系。结果表明,便携式地震波地质分析仪与其他检测方法具有很好的相关性,相关系数均大于0.8。结果表明,应用便携式地震波地质分析仪快速检测路基动模量是合理、可行的,可以用于路基施工过程的质量控制,为路面结构设计提供参数和依据。 相似文献
443.
444.
Global air-sea surface carbon-dioxide transfer velocity and flux estimated using ERS-2 data and a new parametric formula 总被引:1,自引:1,他引:0
Using data from the European remote sensing scatterometer(ERS-2) from July 1997 to August 1998,global distributions of the air-sea CO2 transfer velocity and flux are retrieved.A new model of the air-sea CO2 transfer velocity with surface wind speed and wave steepness is proposed.The wave steepness(5) is retrieved using a neural network(NN) model from ERS-2 scatterometer data,while the wind speed is directly derived by the ERS-2 scatterometer.The new model agrees well with the formulations based on the wind speed and the variation in the wind speed dependent relationships presented in many previous studies can be explained by this proposed relation with variation in wave steepness effect.Seasonally global maps of gas transfer velocity and llux are shown on the basis of the new model and the seasonal variations of the transfer velocity and llux during the 1 a period.The global mean gas transfer velocity is 30 cm/h after area-weighting and Schmidt number correction and its accuracy remains calculation with in situ data.The highest transfer velocity occurs around 60°N and 60°S,while the lowest on the equator.The total air to sea CO2 llux(calculated by carbon) in that year is 1.77 Pg.The strongest source of CO2 is in the equatorial east Pacific Ocean, while the strongest sink is in the 68°N.Full exploration of the uncertainty of this estimate awaits further data.An effectual method is provided to calculate the effect of waves on the determination of air-sea CO2 transfer velocity and fluxes with ERS-2 scatterometer data. 相似文献
445.
非开挖技术在市政工程管网建设中已得到成功广泛的应用。传统非开挖定向拉管技术主要针对抗拉强度较好的钢管、PE管施工,且多为电力、电信套管或压力管等,标高要求不严,但在非压力污(雨)水管铺设时,除标高控制严格外,污水管网的材质也是多样化的设计,给传统非开挖施工提出了难题。针对PE管柔性好,HDPE管抗拉、抗压强度差,小口径砼管不适用顶管施工等特点,采用非开挖定向技术新工艺施工,取得了很好的效果。 相似文献
446.
Changes in terrestrial near-surface wind speed(NSWS) are indicative of the concentrated net effect of climate change and anthropogenic activities. Investigating change mechanisms of NSWS not only furthers the understanding of how the atmosphere changes and improves the climate analysis and projection, but also aids the evaluation and application of wind energy resources. Recent advances in studies of the changes and associated mechanisms of the NSWS over China are reviewed in this paper. Some new results have been achieved in understanding the behaviors of the NSWS changes. The NSWS over China has experienced a decrease in the past 40 years and a recovery in the recent decade, exhibiting large regional and seasonal differences. Understanding of the mechanisms of the NSWS changes has been improved in several aspects; for example, it is found that the reduced NSWS over China is due to the weakening of the pressure-gradient force(PGF) attributed to variations in large-scale ocean–atmosphere circulations(LOACs) as well as the increase of surface roughness due to the land use and cover change(LUCC). The main methods used to analyze the NSWS changes and corresponding mechanisms are also elucidated and discussed.However, studies are still lacking on the mechanisms for multi-timescale(seasonal, interannual, decadal, multidecadal) variations in the NSWS over China, and it remains unknown about the contributions of different forcing factors to the NSWS changes. Finally, key scientific issues regarding our understanding of the NSWS changes are proposed for future investigation. 相似文献