单柱离子色谱测定二氧化锰产品中无机阴离子杂质

采用了单柱离子色谱法测ＭｎＯ２产品中无机离子杂质；提出了消除干扰的可行途径，将Ｌａ（ＯＨ）３加入后能同时消除进样峰的干扰和溶剂峰的出现。选用１．７５ｍｍｏｌ／Ｌ邻苯二甲酸１．７５ｍｍｏｌ／Ｌ三羟甲基氨基甲烷为混合淋洗剂测定Ｆ＾－，Ｃｌ＾－，ＮＯ３＾和ＳＯ＾２－４，其标准加入回收率为９５％－１０５％；ＲＳＤ（ｎ＝７）为２．４７％－８．０８％。     

台风移动规律的研究 Ⅱ．小地形与边界层的动力作用

从支配台风中心移动的基本方程出发，着重分析了小地形（地形高度与台风系统的垂直厚度相比为小量）的抬升作用和边界层的摩擦作用对台风移动影响的定性特征。结果表明，较高地势对台风有“吸引”作用；边界层摩擦辐合引起的艾克曼抽吸有利于台风产生沿局地流场引导速度方向的加速度。     

Predicting lake water quality responses to load reduction: a three-dimensional modeling approach for total maximum daily load

Water quality restoration efforts often suffer the risk of ineffectiveness and failure due to lack of quantitative decision supports. During the past two decades, the restoration of one of China’s most heavily polluted lakes, Lake Dianchi, has experienced costly decision ineffectiveness with no detectable water quality improvement. The governments are planning to invest tremendous amount of funds in the next 5 years to continue the lake restoration process; however, without a quantitative understanding between the load reduction and the response in lake water quality, it is highly possible that these planned efforts would suffer the similar ineffectiveness as before. To provide scientifically sound decision support for guiding future load reduction efforts in Lake Dianchi Watershed, a sophisticated quantitative cause-and-effect response system was developed using a three-dimensional modeling approach. It incorporates the complex three dimensional hydrodynamics, fate and transport of nutrients, as well as nutrient-algae interactions into one holistic framework. The model results show that the model performs well in reproducing the observed spatial pattern and temporal trends in water quality. The model was then applied to three total maximum daily load scenarios and two refined restoration scheme scenarios to quantify phytoplankton responses to various external load reduction intensities. The results show that the algal bloom in Lake Dianchi responds to load reduction in a complex and nonlinear way, therefore, it is necessary to apply the developed system for future load reduction and lake restoration schemes for more informed decision making and effective management.     

Preliminary investigation of mercury in bone tissues of skua and penguin in Antarctica using AFS and Synchrotron Radiation X-ray Fluorescence （SR-XRF）

Mercury （Hg） was investigated in bone tissues of skua （ Catharacta maccormick） and penguin （Pygoscelis adeliae） collected in the maritime Antarctic using atomic fluorescence spectrometry （AFS） and synchrotron radiation X-ray fluorescence （SR-XRF） method. The total levels of mercury in bone tissues of penguin and skua are much lower than those in other organs （e. g. , kidney, liver）. The toxic effects of mercury in bone tissues of seabirds in polar region are not known. We have used SR- XRF method to map the distribution of trace levels of mercury in bones. The levels of mercury are found to be enriched somewhere near the periosteal surface and/or endosteal surface. The distribution of mercury shows strongly correlation with that of some essential elements and probably poses negative effect on the bone metabolism inferring from the relationship of mercury with the other elements. These studies represent a first step toward understanding the toxic effects of mercury on bone of polar animals by suggesting the possible microscopic investigation.     

贻贝育苗中不同饵料的饲养效果比较

培育双壳类软体动物幼苗所需的饵料，是指池内培育阶段适合于幼虫和幼苗(壳长一般在1mm以下)的饵料。育苗成功的关键问题之一为是否已经选择到这样的饵料。自40年代找到适宜的饵料生物以后，双壳类幼虫的培养才取得较明显的成效。以往利用过的一些饵料生物巳有文献系统记载。我国贻贝人工育苗是在分离与培养出扁藻以后才获得成功的。随着研究工作的深入以及适应各种不同情况的需要，采用的饵料种类越来越多样化。从生产性育苗特别是多茬育苗考虑，必须因地制宜地筛选出一定种数的饵料，以便在不同培养条件下有机动选择的余地。同一时还应找出适宜的投饵数量，以求取得较好的育苗效果。为此目的，我们于1975-1978年结合生产性育苗的需要进行了一些饵料饲养实验。本文根据实验结果以及多年来生产性育苗的实践，对贻贝育苗的饵料问题进行总结，侧重于不同饵料的饲养效果比较。     

塔克拉玛干荒漠-绿洲过渡带尘卷风活动特征——以肖塘为例

利用1992—2011年塔克拉玛干沙漠北缘荒漠-绿洲过渡带肖塘气象站的观测资料,分析了该地区尘卷风的年、月变化规律及其与气象因子的关系。结果表明:(1) 1992—2011年尘卷风发生日数总体呈波动递减趋势;尘卷风主要发生在3—9月,占全年总日数的90.9%,其中4—7月占全年总日数的70%左右。(2)尘卷风月发生日数随月平均地表与1.5 m高处温差的增大而线性增加(r=0.875,P<0.01)。(3)尘卷风月发生日数随着月平均风速的增大而幂函数增加(r=0.89,P<0.01)。(4)尘卷风月发生日数随月平均相对湿度的增大而线性减少(r=-0.869,P<0.01)。     

降雨入渗补给地下水数值模拟研究

针对在地下水资源评价中入渗补给量采用经验估算存在较大误差的问题,以神东矿区为例,在广泛调查矿区包气带岩性结构并结合野外取样、室内参数测定的基础上,采用数值模拟的方法建立包气带水分运移数值模拟模型,定量模拟矿区内不同地段降雨入渗强度,探讨影响降雨入渗强度的主要因素,计算得出研究区降雨入渗系数大致在0.18~0.27,分析认为影响降雨入渗强度的因素有降雨量、潜水埋深、包气带岩性等。其中在研究区广泛分布的风积沙对地下水资源起到了一定的保护作用。     

Petrogenesis of I-type granites from Yuqikapa granite pluton of the western Kunlun orogen: Deformation-driven filter-pressing differentiation

<正>1 Introduction The western Kunlun orogen,located in the northwest Tibet Plateau,and is a conjunction between the Pan-Asian and the Tethys tectonic domains.From north to south,the Western Kunlun orogen includes four     

Thermal conductivity measurements of road construction materials in frozen and unfrozen state

A series of thermal conductivity measurements for various materials was performed in a large climate chamber. The size of the chamber allowed the preparation of relatively large samples in a controlled thermal environment. Three types of thermal sensors were used: (1) two needle probes; (2) a grid of temperature sensors, evenly distributed inside the sample; (3) two additional thermal probes, which were simplified versions of an instrument originally developed for measuring thermal properties of the ice/dust mixture expected to exist at the surface of a comet nucleus. They consist of a series of individual temperature sensors integrated into a glass fibre rod. Each of these sensors can be operated in an active (heated) or passive (only temperature sensing) mode. The following sample materials were used: fine-grained reddish sand, coarse-grained moist sand, gravels with various grain size distributions from < 1 cm up to about 6 cm, and for comparison and calibration pure water (with convection suppressed by adding agar-agar), compact ice, and compact granite. Of particular interest are the measurements with composite samples, like stones embedded in an agar-agar matrix. We describe the evaluation methods and present the results of the thermal conductivity measurements.     

甘肃北山野马大泉志留纪花岗岩的成因和构造意义

马鬃山地体是北山造山带的主要构造单元之一,其广泛出露的花岗岩对于认识和完善北山古生代构造格架具有重要意义.对野马大泉一带的花岗岩进行LA-ICP-MS锆石U-Pb定年,获得了早-中志留世(441±4 Ma和425±2 Ma)的年龄.岩石地球化学显示它们均富钠、钙碱性和镁质花岗岩的特征,小于A型花岗岩的Ga/Al×10⁴值和Zr+Nb+Ce+Y值,且含角闪石二长花岗岩出现标志性矿物角闪石,属于Ⅰ型花岗岩.它们具有正的ε_Hf(t)值(-0.1～+7.6),两阶段Hf模式年龄集中于1.42～0.94 Ga,反映花岗质岩浆可能起源于中元古代(～1.4 Ga)地壳的部分熔融,并伴有幔源岩浆的参与.马鬃山地体志留纪花岗岩的地球化学显示形成于大陆弧的构造环境,且结合区域古生代花岗岩的时空分布指示相关的俯冲带在早石炭世发生北向后撤.