山东省临沂市归来庄金矿国家矿山公园矿业遗迹类型与评价

归来庄金矿国家矿山公园的矿业遗迹主要包括:矿产地质遗迹、矿业生产活动遗迹、矿业制品遗存、矿业开发文献史籍和矿业社会生活遗迹五大类。公园内矿业遗迹丰富,类型齐全,组合较好,具有稀有性、典型性、观赏性和科学价值,与自然、人文旅游资源相得益彰,具有较强的外在吸引力和独特的文化内涵。     

Diethylstilbestrol in fish tissue determined through subcritical fluid extraction and with GC-MS

As the key point in sex hormone analysis, sample pre-treatment technology has attracted scientists' attention all over the world, and the development trend of sample preparation forwarded to faster and more efficient technologies. Taking economic and environmental concerns into account, subcritical fluid extraction as a faster and more efficient method has stood out as a sample pre-treatment technology. This new extraction technology can overcome the shortcomings of supercritical fluid and achieve higher extraction efficiency at relatively low pressures and temperatures. In this experiment, a simple, sensitive and efficient method has been developed for the determination of diethylstilbestrol(DES) in fish tissue using subcritical 1,1,1,2-tetrafluoroethane(R134a) extraction in combination with gas chromatography-mass spectrometry(GC-MS). After extraction, freezing-lipid filtration was utilized to remove fatty co-extract. Further purification steps were performed with C_(18) and NH_2 solid phase extraction(SPE). Finally, the analyte was derived by heptafluorobutyric anhydride(HFBA), followed by GC-MS analysis. Response surface methodology(RSM) was employed to optimizing the extraction condition, and the optimized was as follows: extraction pressure, 4.3 MPa; extraction temperature, 26℃; amount of co-solvent volume, 4.7 m L. Under this condition, at a spiked level of 1, 5, 10 μg kg~(-1), the mean recovery of DES was more than 90% with relative standard deviations(RSDs) less than 10%. Finally, the developed method has been successfully used to analyzing the real samples.     

Experimental study of dissolved oxygen transport by regular waves through a perforated breakwater

The perforated breakwater is an environmentally friendly coastal structure,and dissolved oxygen concentration levels are an important index to denote water quality.In this paper,oxygen transport experiments with regular waves through a vertical perforated breakwater were conducted.The oxygen scavenger method was used to reduce the dissolved oxygen concentration of inner water body with the chemicals Na_2SO_3 and Co Cl_2.The dissolved oxygen concentration and wave parameters of 36 experimental scenarios were measured with different perforated arrangements and wave conditions.It was found that the oxygen transfer coefficient through wave surface,K_1a_1,is much lower than the oxygen transport coefficient through the perforated breakwater,K_2a_2.If the effect of K_1a_1 is not considered,the dissolved oxygen concentration computation for inner water body will not be greatly affected.Considering the effect of a permeable area ratio α,relative location parameter of perforations δ and wave period T,the aforementioned data of 30 experimental scenarios,the dimensional analysis and the least squares method were used to derive an equation of K_2a_2(K_2a_2=0.0042α~(0.5)δ~(0.2)T~(-1)).It was validated with 6 other experimental scenarios data,which indicates an approximate agreement.Therefore,this equation can be used to compute the DO concentration caused by the water transport through perforated breakwater.     

FY3地面业务系统关键信息短信报警平台的设计及实现

FY3卫星地面业务系统关键信息短信报警平台为高可靠极轨业务系统运行提供了保障。从报警监视关键监视点的选取、轨道接收圈的智能判别,平台报警信息的处理以及保证软件的高时效性出发,讨论了FY3卫星轨道可能出现的情况,提出了两种判别算法并进行了取舍。针对平台报警信息处理以及保证软件高时效性,对FY3卫星的接收时间特性进行了分析并基于此设计报警短信过滤逻辑及基本软件结构。该平台已在实际工程中应用并取得了良好效果,本文最后给出了运行统计数据。     

Research Progress on Electrical Properties and Conductivity Measurement Technology of Ice Core

Ice core is an important object of the global climate change research, and can extract paleoclimate information by physical and chemical methods. As one of the major physical analysis technology, conductivity measurement technology mainly contains two methods and has been applied to many drilling project. The technology reflects the ice core electrical properties influenced by factors such as temperature, pressure, impurities and changes, and the cause of these changes can be explained from the aspects of macroscopic and microscopic. What obtained from measurement can be used to the research of dating, volcanic events, accumulation rate, biomass burning, ion concentration recovery, which systematically help us to understand the quaternary evolution of Antarctic climate since late pleistocene. This paper summarized in detail the main research achievements on electrical properties and dielectric measurement technology of ice core, and also discussed the prospect of the technology in China deep ice core project further.