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221.
An Investigation of Digestion Methods for Trace Elements in Bauxite and Their Determination in Ten Bauxite Reference Materials Using Inductively Coupled Plasma‐Mass Spectrometry
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Wen Zhang Liang Qi Zhaochu Hu Cunjiang Zheng Yongsheng Liu Haihong Chen Shan Gao Shenghong Hu 《Geostandards and Geoanalytical Research》2016,40(2):195-216
Trace elements from samples of bauxite deposits can provide useful information relevant to the exploration of the ore‐forming process. Sample digestion is a fundamental and critical stage in the process of geochemical analysis, which enables the acquisition of accurate trace element data by ICP‐MS. However, the conventional bomb digestion method with HF/HNO3 results in a significant loss of rare earth elements (REEs) due to the formation of insoluble AlF3 precipitates during the digestion of bauxite samples. In this study, the digestion capability of the following methods was investigated: (a) ‘Mg‐addition’ bomb digestion, (b) NH4HF2 open vessel digestion and (c) NH4F open vessel digestion. ‘Mg‐addition’ bomb digestion can effectively suppress the formation of AlF3 and simultaneously ensure the complete decomposition of resistant minerals in bauxite samples. The addition of MgO to the bauxite samples resulted in (Mg + Ca)/Al ratios ≥ 1. However, adding a large amount of MgO leads to significant blank contamination for some transition elements (V, Cr, Ni and Zn). The NH4HF2 or NH4F open vessel digestion methods can also completely digest resistant minerals in bauxite samples in a short period of time (5 hr). Unlike conventional bomb digestion with HF/HNO3, the white precipitates and the semi‐transparent gels present in the NH4HF2 and NH4F digestion methods could be efficiently dissolved by evaporation with HClO4. Based on these three optimised digestion methods, thirty‐seven trace elements including REEs in ten bauxite reference materials (RMs) were determined by ICP‐MS. The data obtained showed excellent inter‐method reproducibility (agreement within 5% for REEs). The relative standard deviation (% RSD) for most elements was < 6%. The concentrations of trace elements in the ten bauxite RMs showed agreement with the limited certified (Li, V, Cr, Cu, Zn, Ga, Sr, Zr and Pb) and information values (Co, Ba, Ce and Hf) available. New trace element data for the ten RMs are provided, some of which for the first time. 相似文献
222.
在内蒙古大青山地区逆冲推覆构造所截切的英安岩中获得锆石~(207)Pb/~(206)Pb表面年龄加权平均值为1870±19Ma,认为英安岩为华北克拉通古元古代末—新元古代一次裂解事件的产物.同时,据安山岩锆石U-Pb年龄谐和度(102)较好的锆石~(206)Pb/~(238)U表面年龄436±4Ma及英安岩锆石U-Pb年龄谐和度(104)较好的锆石~(206)Pb/~(238)U表面年龄153±2Ma和160±2Ma,表明大青山地区逆冲推覆构造存在构造复活或构造追踪现象。这一认识为大青山地区逆冲推覆构造的研究积累了新的资料,提供了新的研究思路。 相似文献
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Characteristics of groundwater flow field after land creation engineering in the hilly and gully area of the Loess Plateau 总被引:1,自引:0,他引:1
Xiaoxi Yin Luwang Chen Jiandong He Xiaoqing Feng Wen Zeng 《Arabian Journal of Geosciences》2016,9(14):646
In order to study the degree of influence and control mechanism to groundwater flow field caused by land creation engineering in the hilly and gully area of the Loess Plateau, based on the geological and engineering conditions of the first stage project of Yan’an new district in China, numerical simulation of groundwater flow is carried out by the Feflow and GIS technologies. From the simulation, punning measure relatively reduces infiltration recharge and artificial gravel drain increases groundwater seepage. The basic characteristics of groundwater flow field is controlled by the old and new topographies in the whole study area, and artificial gravel drain plays an auxiliary role in accelerating groundwater drawdown upstream and promotes groundwater rise downstream. According to differences of groundwater level and declining percentages of hydraulic gradient in the main and secondary gullies, dewatering of artificial gravel drain in the secondary gully is more effective than that in the main gully, which will yet play an important role in the future. The study results will make contributions to understand groundwater response to land creation engineering and will be beneficial to take necessary measures to prevent collapse of loess and failure of building foundation in the hilly and gully area of the Loess Plateau. 相似文献
230.
The Three Gorges are considered to be critical to understand the formation of Yangtze River. Recent research results suggest that the Yangtze Three Gorges was created during the Quaternary but the exact time is debatable. Fe–Ti oxide minerals are seldom used to study sediment provenance, expecially using scanning electron microscopy(SEM), and energy dispersive spectrometer(EDS). In this study, the provenance of Quaternary sediments in Yichang area, which is located to the east of the Yangtze Three Gorges, was investigated by using SEM and EDS to research Fe–Ti oxides. The Panzhihua vanadium titanomagnetite and Emeishan basalt outcrop are located to the west of the Three Gorges. Further, the materials from them are observed in the Quaternary sediments of Yichang area. Fe–Ti oxide minerals from the Huangling granite are observed in the Yunchi and Shanxiyao Formations, which were formed before 0.75 Ma B.P., whereas Fe–Ti oxide minerals from the Huangling granite, Panzhihua vanadium titanomagnetite, and Emeishan basalt are observed in the riverbed and fifth-terrace sediments of the Yangtze River, which were formed after 0.73 Ma B.P.. Thus, we can infer that the Three Gorges formed after the deposition of the Shanxi Formation and before the fifth-terrace; i.e., 0.75–0.73 Ma B.P.. 相似文献