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731.
本文以 1条简单有效的新路线合成了莫达非尼 ,总收率为 6 1.6 %。首先在 Fe(NO3 ) 3 ·9H2 O催化下以二苯甲醇和巯基乙酸合成二苯甲基巯基乙酸 ,进而进行酰胺化反应 ,生成相应的酰胺化合物在双氧水作用下将硫醚氧化为亚枫得到目标化合物。产物用 IR,NMR确证其结构。 相似文献
732.
1 .IntroductionIntheexploitationofoceanresourcesandintheutilizationofoceanspaces,verylargefloatingstructures (VLFS)suchasMega FloatinJapan (Isobe ,1 999)andMobileOffshoreBase (MOB)inUSA (Remmers ,1 999)playasignificantrole .However,owingtotheirlargesizesandrelativelylowbendingrigidities ,theirhydroelasticresponsesinwavesareofthemostconcern .ManystudieshavebeencarriedoutforthepredictionofthehydroelasticresponsesofVLFS′s (Kashiwagi,2 0 0 0 ;Cui,2 0 0 2 ) .However,inalmostallofthesestu… 相似文献
733.
为查明内蒙古克鲁伦凹陷伊敏组下段砂岩铀成矿规律和成因,系统总结了内外部铀源、构造环境、岩性-岩相特征、后生氧化作用等关键控矿条件以及铀成矿特征,较精准厘定了目的层时代及其铀成矿年龄,进而构建了砂岩铀成矿模式。结果表明:克鲁伦凹陷的主攻找矿目的层为伊敏组下段,侏罗纪中酸性火山岩、海西期花岗岩、下白垩统伊敏组和地下水的U含量高,指示了内外部铀源十分丰富;目的层形成于断-坳转换期,发育扇三角洲相—滨浅湖相沉积体系,(水下)分流河道微相灰色砂体发育,岩性以含砾粗砂岩、砂砾岩为主,结构疏松,透水性好;原生砂体中富含碳屑及植物茎干,自身还原容量较高,是一套良好的含矿建造;该砂体普遍发育强烈的褐黄色面状古潜水(局部古潜水-层间)后生氧化作用,进而控制了矿体的形成和形态;矿体埋深一般小于150 m,每平方米U质量为0.46~1.00 kg,主要呈透镜状和似层状;铀矿化砂岩全岩U-Pb定年获得了(67.1±5.9)Ma和(63.7±5.2)Ma的等时线成矿年龄;结合凹陷构造演化史,建立了伊敏组下段4个阶段的古潜水-层间氧化铀成矿模式,即早白垩世早期成矿前富铀建造准备阶段、早白垩世中晚期含矿目的层形成阶段、古近纪主成矿阶段和新近纪成矿停滞保存阶段,并指出区内深部(500 m以浅)仍具有较好的古潜水-层间氧化带型铀矿成矿潜力。 相似文献
734.
The role of non‐coaxiality in the simulation of strain localization based on classical and Cosserat continua
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It is normally accepted that materials inside the shear band undergo severe rotation of the principal stress direction, which causes non‐coaxiality between the principal stress and principal plastic strain rate. However, classical plasticity flow theory implicitly assumes that the principal stress and the principal plastic strain rate are coaxial; thus, it may not correctly predict the onset of the shear band. In addition, classical continuum does not contain any internal length scales; as a result, it cannot provide a reasonable shear band thickness. In this study, the original vertex non‐coaxial plastic model based on the classical continuum is extended to the Cosserat continuum. The corresponding codes are implemented via the interface of the user defined element subroutine in ABAQUS. Through a simple shear test, the effectiveness of the user's codes is verified. Through a uniaxial compression test, the influence of non‐coaxiality on the onset, the orientation, and the thickness of the shear band is investigated. Results show that the onset of the shear localization is delayed, and the thickness of the shear band is widened when the non‐coaxial degree increases, while the orientation of the shear band is little affected by the non‐coaxial degree. In addition, it is found that the non‐coaxiality can weaken the micro‐polar effect to some extent; nonetheless, the Cosserat non‐coaxial model still has its advantage over the classical non‐coaxial model in capturing the pre‐bifurcation as well as the post‐bifurcation behaviors of strain localization. Copyright © 2016 John Wiley & Sons, Ltd. 相似文献
735.
An ensemble Kalman filter (EnKF) is developed to identify a hydraulic conductivity distribution in a heterogeneous medium by assimilating solute concentration measurements of solute transport in the field with a steady‐state flow. A synthetic case with the mixed Neumann/Dirichlet boundary conditions is designed to investigate the capacity of the data assimilation methods to identify a conductivity distribution. The developed method is demonstrated in 2‐D transient solute transport with two different initial instant solute injection areas. The influences of the observation error and model error on the updated results are considered in this study. The study results indicate that the EnKF method will significantly improve the estimation of the hydraulic conductivity field by assimilating solute concentration measurements. The larger area of the initial distribution and the more observed data obtained, the better the calculation results. When the standard deviation of the observation error varies from 1% to 30% of the solute concentration measurements, the simulated results by the data assimilation method do not change much, which indicates that assimilation results are not very sensitive to the standard deviation of the observation error in this study. When the inflation factor is more than 1.0 to enlarge the model error by increasing the forecast error covariance matrix, the updated results of the hydraulic conductivity by the data assimilation method are not good at all. Copyright © 2012 John Wiley & Sons, Ltd. 相似文献
736.
In northern regions, river ice‐ jam flooding can be more severe than open‐water flooding causing property and infrastructure damages, loss of human life and adverse impacts on aquatic ecosystems. Very little has been performed to assess the risk induced by ice‐related floods because most risk assessments are limited to open‐water floods. The specific objective of this study is to incorporate ice‐jam numerical modelling tools (e.g. RIVICE, Monte‐Carlo simulation) into flood hazard and risk assessment along the Peace River at the Town of Peace River (TPR) in Alberta, Canada. Adequate historical data for different ice‐jam and open‐water flooding events were available for this study site and were useful in developing ice‐affected stage‐frequency curves. These curves were then applied to calibrate a numerical hydraulic model, which simulated different ice jams and flood scenarios along the Peace River at the TPR. A Monte‐Carlo analysis was then carried out to acquire an ensemble of water level profiles to determine the 1 : 100‐year and 1 : 200‐year annual exceedance probability flood stages for the TPR. These flood stages were then used to map flood hazard and vulnerability of the TPR. Finally, the flood risk for a 200‐year return period was calculated to be an average of $32/m2/a ($/m2/a corresponds to a unit of annual expected damages or risk). Copyright © 2016 John Wiley & Sons, Ltd. 相似文献
737.
This study presents a novel hysteresis model based on van Genuchten's soil‐moisture relationships. The proposed model yields a series of closed‐form relationships in which two shape factors α and η are determined from the main drying and wetting curves. Experimental and literature‐cited data were used to assess model accuracy. The proposed model was also compared with the Scott and KP models. Analytical results indicate that the present model is simple, accurate and effective in constructing the series of wetting and drying scanning curves. Notably, the proposed model outperforms the Scott and KP models in terms of model accuracy. Moreover, the novel model eliminates the pumping effect and has perfect closure at scanning curve reversal points. Copyright © 2004 John Wiley & Sons, Ltd. 相似文献
738.
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???????????????????????????жΣ?????????????????????й?????????Ч???????????????????????????????????????????????????????????????????????????????????????????????????????????????????????????????????????????????????????? 相似文献
739.
介绍基于C8051F330单片机的地震观测系统中故障报警子系统的工作原理,并对温度报警设计中的问题进行分析。 相似文献
740.
Chu P.C. Mancini S. Gottshall E.L. Cwalina D.S. Barron C.N. 《Oceanic Engineering, IEEE Journal of》2007,32(2):453-468
The purpose of this research is to assess the benefit of assimilating satellite altimeter data for naval undersea warfare. To accomplish this, sensitivity of the weapon acoustic preset program (WAPP) for the Mk 48 variant torpedo to changes in the sound-speed profile (SSP) is analyzed with SSP derived from the modular ocean data assimilation system (MODAS). The MODAS fields differ in that one uses altimeter data assimilated from three satellites while the other uses no altimeter data. The metric used to compare the two sets of outputs is the relative difference in acoustic coverage area generated by WAPP. Output presets are created for five different scenarios, two anti surface warfare (ASTJW) scenarios, and three antisubmarine warfare (ASW) scenarios, in each of three regions: the East China Sea, Sea of Japan, and an area south of Japan that includes the Kuroshio currents. Analysis of the output reveals that, in some situations, WAPP output is very sensitive to the inclusion of the altimeter data because of the resulting differences in the subsurface predictions. The change in weapon presets can be so large that the effectiveness of the weapon may be affected. 相似文献