溶剂萃取原子吸收光谱法测定高纯石英砂中痕量铁

高纯石英砂用HF等溶剂溶解并蒸干后,在微酸性介质中用抗坏血酸还原Fe^3＋为Fe^2＋,与1,10-二氮杂菲形成Fe2＋3络合物,加入适量ClO4^-阴离子与之形成离子缔合物,用硝基苯萃取,原子吸收测定有机相,本法检出限1.1μg/g,样品分析结果的RSD%为：4.52～10.3.     

平原农区土地综合整治与乡村转型发展协同机制

平原农区是保障国家粮食安全的核心区,土地综合整治与乡村转型发展协同有利于缓解平原农区经济发展、耕地保护、生态保育等多重压力,保障乡村振兴政策落实。本文以“问题研判—策略梳理—机制构建—实证检验”为研究主线,探讨两者协同机制。研究表明：① 平原农区“三生”空间利用冲突显著,生产空间低值低效、生活空间无序空废、生态空间污损衰退共同制约乡村转型发展;② 面向土地价值提升、人居环境改善、产业融合发展的土地综合整治优化策略,有利于推动乡村转型发展;③ 新时期,土地综合整治由“以地为本”单要素调控转向“人、地、业、权”多要素协同综合整治,权利重组、空间重构、产业重塑是推动土地综合整治与乡村转型发展协同的核心机制;④ 平原农区典型地区禹城市,聚焦土地权属调整、空心村整治和现代产业培育,实现土地综合整治与乡村转型发展的协同推进。本文有利于深化平原农区人地系统科学新认知,为构建现代化国土空间治理体系和全面推进乡村振兴提供实践参考。     

耕地粮食生产潜力及人口承载力研究——以长清县为例

以长清县为例 ,利用 GIS技术和遥感数据 ,按照“机制法”原理计算耕地资源粮食生产潜力。重点是因地制宜、科学确定并计算土壤有效系数和社会有效系数 ,从而得到耕地生产潜力和社会生产潜力像元分布数据。在此基础上 ,进行粮食增产潜力计算 ,并预测未来人口数量发展趋势 ,探讨未来的人口承载力问题。结果表明 :该县粮食增产潜力巨大 ,但是粮食问题仍不容乐观。     

“一国两制”下香港居民跨境消费行为特征和影响因素研究

深港边界是全球跨境活动最频繁的地区之一。以通过深圳湾口岸前往蛇口消费的香港居民为研究对象,采用定性、定量和空间计量相结合的方法分析香港居民来往深圳的消费模式和行为影响因素,发现在蛇口的跨境港人多来自“新界西”的屯门、元朗、荃湾三地,呈现以公交出行为主、出行频率高、消费低、时间短、老龄化、女性多的特点,其跨境行为主要受到个人年龄及收入、出行距离、区位等因素影响;港人在深港边界的跨境活动开始出现与收入、年龄相关的空间分异现象,呼吁展开针对不同过境群体的进一步研究,厘清其行为特点和影响因素,这将有助于建构粤港“优质生活圈”、促进粤港两地间更便利的跨境活动和更深层次的协作。     

科学大洋钻探中的新技术

大洋钻探诸多科学目标的实现与包括钻探、取芯、测试和海底观测技术在内的各种新技术的开发和革新密不可分。即将开展的IODP计划,将对各种技术提出新的要求。在钻探技术上,将联合使用多平台,以实现区域更广深度更大的钻探作业;在取芯技术上,取样范围更广,从各种岩石取样到地下流体的取样,并要求样品保持原始状态,同时确保获得更高的岩芯采收率;在测试上,要求采用随钻测试技术,以适时地获得地下真实信息;在观测技术上,要求开发各种工具,去除由于钻探造成的扰动,使得各种观测仪器能够进行长期的跟踪观测。     

A multi‐proxy sediment record of late Holocene and recent climate change from a lake near Ny‐Ålesund,Svalbard

Jiang, S., Liu, X., Sun, J., Yuan, L., Sun, L. & Wang, Y. 2011: A multi‐proxy sediment record of late Holocene and recent climate change from a lake near Ny‐Ålesund, Svalbard. Boreas, Vol. 40, pp. 468–480. 10.1111/j.1502‐3885.2010.00198.x. ISSN 0300‐9483 The Arctic constitutes a unique and important environment with a significant role in the dynamics and evolution of the earth system. Arctic lake sediments, which accumulate slowly over time, contain abundant information about the biological communities that lived within the water body, as well as in the surrounding catchment. In this study, we collected a sediment core from Ny‐Ålesund, Svalbard, performed multi‐proxy analyses on sediment pigments, mineral magnetic susceptibility, various sediment quality (i. e. organic matter content, CaCO₃ content, carbon and nitrogen isotope), and diatom composition, and reconstructed the history of ecosystem responses to environmental variations, especially regarding aquatic productivity and lake catchment surface processes. Ny‐Ålesund has undergone distinct ecological and climatic changes. During the Little Ice Age, the cold climate was unfavourable for the growth of lake algae, and therefore the lake primary productivity declined. After about AD 1890 and during the 20th century, the warming climate and reduced ice cover led to rapid lithological change and growth of lake algae, enhanced lake primary productivity, and increased input of nutrients derived from increased chemical weathering into the lake. The lake ecosystem on Ny‐Ålesund has had rapid responses to climatic and environmental changes in the Arctic.     

信息安全实验管理系统的实现及其系统中安全问题的解决

B／S模式的应用系统都要面对安全的问题，身份认证和访问控制是实现计算机安全的主要手段。介绍了基于Web的信息安全实验管理系统，分析了系统的体系架构和功能，针对B／S模式的安全威胁，采用了两个方案实现身份认证和访问控制。     

The impacts of urbanization on soil erosion in the Loess Plateau region

The accelerated urbanization has resulted in new soil erosion in the Loess Plateau region since the 1980s. A concept of urban erosion and its impacts on environment are discussed. The experimental studies and field investigations show that those loose silt and earth piles formed by urban construction can be eroded seriously: Under stormy rain, the amount of sediment from steep man-dumped slope is 10.8-12.2 times that of from uncovered slope land; the result of experiments with the wind tunnel also shows that the damage to the surface structure of dry loess can cause serious soil erosion by wind in some cities of the region. Even if in the urban built-up area, there are many loose sandy soil, mud and silt, which are washed into rivers by city’s ground flow in the rainy season. So, anthropogenically induced soil erosion has made soil erosion more serious around the urban areas. And the urban eroded environment has several characteristics such as fragility, complexity, seasonality and quick variability. Urban areas witness a quick economic growth and have more construction projects than rural areas, which brings more intensive changes of environments during a short period of time or adds some new elements to the erosion system. Therefore erosion has experienced more intensive impact by human activities. So, the possible impact of urbanization on erosion environment must be taken into consideration when designing or planning to exploit natural resources or to develop urban areas in the Loess Plateau.     

低碳盐湖提锂:高渗透选择性纳滤膜和正渗透膜材料

报道了联合基金项目“面向青海盐湖卤水锂提取过程强化的高性能中空纤维正渗透膜材料的设计研究”的最新进展。研究从吸附/解吸或稀释盐湖卤水出发,采用“纳滤－正渗透膜”耦合工艺纯化和浓缩Li+浓度至3 wt.%用于碳酸锂沉淀。研究重点是制备高渗透分离性能的层层自组装中空纤维纳滤膜和正渗透膜材料。通过基膜孔结构和物化性能与层层自组装纳滤膜性能和界面聚合正渗透膜性能之间的关系研究及系列技术攻关,已完成四寸中空纤维纳滤膜和正渗透膜的制备,技术指标达到项目指标。项目研究为青海盐湖锂提取提供了核心的分离和浓缩膜材料。     

ECOLOGICAL SERIES OF SOIL ANIMALS IN DARLIDAI MOUNTAIN

The ecological series of soil animals under the broad-leaved and pine mixed forest in Darlidai Mountainwas studied. Seven sample plots were selected according to different altitude gradients, which belong to different vegeta-tion types. By investigating and analyzing soil animals in every sample plot it is found that there are 45 groups and 1956individuals, which axe involved in 3 phylums, 7 classes, 16 orders, respectively. The altitude is a key factor which af-fects ecological series of soil animals. Both the groups and individuals of soil animals increase with altitude increasingunder certain conditions, which contrastes with ordinary cases, resulting from special micro-climate in studied area. Thegroups and individuls of soil animals are the most under the broad-leaved and pine forest on the top of the mountain, andthe least under Picea-Abies forest in the foot of the mountain.