Determination of the thicknesses of oil films in micro- and nano-pores in tight oil sands: an example from the southern Songliao Basin,NE China

An experimental method of field-emission environmental scanning electron microscope (ESEM) coupled with the energy dispersive spectrum (EDS) to determine the thickness of oil films in the micro- and nano-pores of tight oil sands was proposed to overcome the limitations of current methods. First, we got the data of the detection range volumes, elemental mass percentages, and elemental atomic percentages using the EDS, and then calculated the volumes of oil films in the detection range according to the elemental mass percentages and the elemental atomic percentages of carbon. After that, we calculated the surface areas of oil films using the pore size data (lengths, widths, and depths) detected by ESEM. The thicknesses of oil films in the pores equaled the volumes divided by the surface areas. An analysis of tight oil samples from the Quan 4 Segment of in the southern Songliao Basin, NE China confirmed that the oil in the micro- and nano-pores had two main forms: oil films and oil droplets. The thicknesses of the oil films ranged from about 400 nm to 2 μm, while the thicknesses of the oil droplets ranged from about 200 to 700 nm.     

Characterization of the mechanical properties of a claystone by nano-indentation and homogenization

Based on the analyses of mineralogical compositions by X-ray diffraction and microstructure by optical microscopy, the Young’ modulus and hardness of a claystone were characterized by the nano-indentation technique and homogenization method. Three distinct microstructural zones are identified in the claystone: clay matrix, a composite matrix of clay and small mineral grains and imbedded quartz grains. The elastic modulus and hardness of different zones were determined by nano-indentation testing. Based on the statistical analysis of nano-indentation results, the spatial mappings and frequency distributions of elastic modulus and hardness of the different zones were obtained. The elastic moduli of main constituent phases of the claystone are then estimated from the nano-indentation tests. These values were further used for the determination of the macroscopic elastic modulus of the claystone using two different homogenization schemes: the dilute scheme and Mori–Tanaka scheme. The predicted values by the homogenization schemes are compared with experimental data obtained from conventional uniaxial compression tests.     

Periodical mixing of MORB magmas near East Pacific Rise 13°N: Evidence from modeling and zoned plagioclase phenocrysts

Thirty-six basalt samples from near East Pacific Rise 13°N are analyzed for major and trace elements. Different types of zoned plagioclase phenocrysts in basalts are also backscatter imaged, and major element profiles scanned and analyzed for microprobe. Basalts dredged from a restricted area have evolved to different extents (MgO=9.38wt%—6.76wt%). High MgO basalts are modeled for crystalliza-tion to MgO of about 7wt%, and resulted in the Ni contents (≈28 ppm) that are generally lower than that in observed basalts (>60 ppm). It suggests that low MgO basalts may have experienced more intensive magma mixing. High MgO (9.38wt%) basalt is modeled for self-"mixing-crystallization", and the high Ni contents in low MgO basalts can be generated in small scale and periodical self-mixing of new magma (high MgO). "Mixing-crystallization" processes that low MgO magmas experienced accord with recent 226Ra/230Th disequilibria studies for magma residence time, in which low MgO magmas have experi-enced more circles of "mixing-crystallization" in relatively longer residence time. Magma mixing is not homogeneous in magma chamber, however, low MgO magmas are closer to stable composition pro-duced by periodical "mixing-crystallization", which is also an important reason for magma diversity in East Pacific Rise. Zoned plagioclase phenocrysts can be divided into two types: with and without high An# cores, both of which have multiple reversed An# zones, suggesting periodical mixing of their host magmas. Cores of zoned plagioclase in low MgO (7.45wt%) basalt differ significantly with their mantle in An#, but are similar in An# with microlite cores (products of equilibrium crystallization) in high MgO (9.38wt%) basalt, which further shows that plagioclase phenocryst cores in low MgO basalts may have formed in their parental magmas before entering into the magma chamber.     

Sedimentary Deposits from the 17 July 2006 Western Java Tsunami,Indonesia: Use of Grain Size Analyses to Assess Tsunami Flow Depth,Speed, and Traction Carpet Characteristics

The 2006 western Java tsunami deposited a discontinuous sheet of sand up to 20 cm thick, flooded coastal southern Java to a depth of at least 8 m and inundated up to 1 km inland. In most places the primarily heavy mineral sand sheet is normally graded, and in some it contains complex internal stratigraphy. Structures within the sand sheet probably record the passage of up to two individual waves, a point noted in eyewitness accounts. We studied the 2006 tsunami deposits in detail along a flow parallel transect about 750 m long, 15 km east of Cilacap. The tsunami deposit first becomes discernable from the underlying sediment 70 m from the shoreline. From 75 to 300 m inland the deposit has been laid down in rice paddies, and maintains a thickness of 10–20 cm. Landward of 300 m the deposit thins dramatically, reaching 1 mm by 450 m inland. From 450 m to the edge of deposition (around 700 m inland) the deposit remains <1 mm thick. Deposition generally attended inundation—along the transect, the tsunami deposited sand to within about 40 m of the inundation limit. The thicker part of the deposit contains primarily sand indistinguishable from that found on the beach 3 weeks after the event, but after about 450 m (and roughly coinciding with the decrease in thickness) the tsunami sediment shifts to become more like the underlying paddy soil than the beach sand. Grain sizes within the deposit tend to fine upward and landward, although overall upward fining takes place in two discrete pulses, with an initial section of inverse grading followed by a section of normal grading. The two inversely graded sections are also density graded, with denser grains at the base, and less dense grains at the top. The two normally graded sections show no trends in density. The inversely graded sections show high density sediment to the base and become less dense upward and represents traction carpet flows at the base of the tsunami. These are suggestive of high shear rates in the flow. Because of the grain sorting in the traction carpet, the landward-fining trends usually seen in tsunami deposits are masked, although lateral changes of mean sediment grain size along the transect do show overall landward fining, with more variation as the deposit tapers off. The deposit is also thicker in the more seaward portions than would be produced by tsunamis lacking traction carpets.     

基于GPRS的监控软件和网站的设计与实现

针对野外恶劣自然环境条件制约冻土温度现场采集和远程监控的问题,本文设计和开发基于通用分组无线业务(GPRS)的冻土实时监控软件和监控中心网站。冻土远程实时监控软件实现野外冻土温度数据的自动采集、实时显示、数据存储和远程控制等功能,降低数据采集的成本,提高数据采集的效率,已经成功应用于野外现场监控。配套开发的监控中心网站将冻土温度数据发布至Internet网络,解决冻土数据共享问题,扩大冻土温度监控的范围,实现多用户的实时数据远程监控。     

Seismic evaluation of an existing complex RC building

The seismic evaluation of existing buildings is a more difficult task than the seismic design of new buildings. Non-linear methods are needed if realistic results are to be obtained. However, the application to real complex structures of various evaluation procedures, which have usually been tested on highly idealized structural models, is by no means straightforward. In the paper, a practice-oriented procedure for the seismic evaluation of building structures, based on the N2 method, is presented, together with the application of this method to an existing multi-storey reinforced concrete building. This building, which is asymmetric in plan and irregular in elevation, consists of structural walls and frames. It was designed in 1962 for gravity loads and a minimum horizontal loading (2% of the total weight). The main results presented in terms of the global and local seismic demands are compared with the results of non-linear dynamic response-history analyses. As expected, the structure would fail if subjected to the design seismic action according to Eurocode 8. The shear capacity of the structural walls is the most critical. If the shear capacity of these elements was adequate, the structure would be able to survive the design ground motion according to Eurocode 8, in spite of the very low level of design horizontal forces. The applied approach proved to be a feasible tool for the seismic evaluation of complex structures. However, due to the large randomness and uncertainty which are involved in the determination of both the seismic demand and the seismic capacity, only rough estimates of the seismic behaviour of such structures can be obtained.     

Results from the Big Spring basin water quality monitoring and demonstration projects,Iowa, USA

Agricultural practices, hydrology, and water quality of the 267-km² Big Spring groundwater drainage basin in Clayton County, Iowa, have been monitored since 1981. Land use is agricultural; nitrate-nitrogen (-N) and herbicides are the resulting contaminants in groundwater and surface water. Ordovician Galena Group carbonate rocks comprise the main aquifer in the basin. Recharge to this karstic aquifer is by infiltration, augmented by sinkhole-captured runoff. Groundwater is discharged at Big Spring, where quantity and quality of the discharge are monitored. Monitoring has shown a threefold increase in groundwater nitrate-N concentrations from the 1960s to the early 1980s. The nitrate-N discharged from the basin typically is equivalent to over one-third of the nitrogen fertilizer applied, with larger losses during wetter years. Atrazine is present in groundwater all year; however, contaminant concentrations in the groundwater respond directly to recharge events, and unique chemical signatures of infiltration versus runoff recharge are detectable in the discharge from Big Spring. Education and demonstration efforts have reduced nitrogen fertilizer application rates by one-third since 1981. Relating declines in nitrate and pesticide concentrations to inputs of nitrogen fertilizer and pesticides at Big Spring is problematic. Annual recharge has varied five-fold during monitoring, overshadowing any water-quality improvements resulting from incrementally decreased inputs. Electronic Publication     

一种用于海底类型聚类的新方法

By using sonar imaging, this paper presents a new algorithm for the clustering of seabed types based on the self-organizing feature maps （SOFM） neural network. The theory as well as data processing is studied in detail. Some valuable conclusions and suggestions are given     

A Directed-Line-Segment-Based Photogrammetry Method to Survey the Tunneling Working Surface of Mine Roadway

Absolute orientation is a basic technical work in digital image geologic logging of underground coal mine. Traditional control-point-based absolute orientation method requires setting object space control points of the known three-dimensional coordinates, which may lead to low efficiency. Therefore, this paper proposed a point-free close-range photogrammetry absolute orientation algorithm, which utilized direction line segments including plumb line segments and line segments with known directions and lengths to identify the dimensional orientation of a stereoscopic model. Experiment results show that the precision of the orientation results is favorable. σ _X and σ _Y are as high as 0.5 mm, and σ _Z is 0.3 mm. Finally, this paper introduced the application of the proposed algorithm in rapid geological logging of coal mine roadway, which was fast and reliable, convenient and feasible.     

珠海年降雨量的多时间尺度变化

利用Morlet小波分析方法,对珠海市40年（1961—2000年）的年降雨量和气温资料进行计算和分析,得出：珠海的年降雨量存在比较完整的明显准22年的周期振荡,它有两个降雨偏少中心（1960—1970年和1980—1990年）和两个降雨偏多中心（1970—1980年和1990—2000年）,历经40年的全过程,因而具有长期预测意义。还有其它22年以下的较短周期振荡,但多不具全局性变化特征。从对28、12和4年周期的小波方差随时间变化来看,28年周期存在两个突变点（1974年和1987年）,而且降水和气温的变化趋势是一致的。从12年和4年周期看,降雨和气温的变化趋势是相反的。