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Daniela Comelli Massimo D'orazio Luigi Folco Mahmud El‐Halwagy Tommaso Frizzi Roberto Alberti Valentina Capogrosso Abdelrazek Elnaggar Hala Hassan Austin Nevin Franco Porcelli Mohamed G. Rashed Gianluca Valentini 《Meteoritics & planetary science》2016,51(7):1301-1309
Scholars have long discussed the introduction and spread of iron metallurgy in different civilizations. The sporadic use of iron has been reported in the Eastern Mediterranean area from the late Neolithic period to the Bronze Age. Despite the rare existence of smelted iron, it is generally assumed that early iron objects were produced from meteoritic iron. Nevertheless, the methods of working the metal, its use, and diffusion are contentious issues compromised by lack of detailed analysis. Since its discovery in 1925, the meteoritic origin of the iron dagger blade from the sarcophagus of the ancient Egyptian King Tutankhamun (14th C. BCE) has been the subject of debate and previous analyses yielded controversial results. We show that the composition of the blade (Fe plus 10.8 wt% Ni and 0.58 wt% Co), accurately determined through portable x‐ray fluorescence spectrometry, strongly supports its meteoritic origin. In agreement with recent results of metallographic analysis of ancient iron artifacts from Gerzeh, our study confirms that ancient Egyptians attributed great value to meteoritic iron for the production of precious objects. Moreover, the high manufacturing quality of Tutankhamun's dagger blade, in comparison with other simple‐shaped meteoritic iron artifacts, suggests a significant mastery of ironworking in Tutankhamun's time. 相似文献
34.
Enrico Costa Ronaldo Bellazzini Gianpiero Tagliaferri Giorgio Matt Andrea Argan Primo Attinà Luca Baldini Stefano Basso Alessandro Brez Oberto Citterio Sergio Di Cosimo Vincenzo Cotroneo Sergio Fabiani Marco Feroci Antonella Ferri Luca Latronico Francesco Lazzarotto Massimo Minuti Ennio Morelli Fabio Muleri Lucio Nicolini Giovanni Pareschi Giuseppe Di Persio Michele Pinchera Massimiliano Razzano Luigia Reboa Alda Rubini Antonio Maria Salonico Carmelo Sgro’ Paolo Soffitta Gloria Spandre Daniele Spiga Alessio Trois 《Experimental Astronomy》2010,28(2-3):137-183
Since the birth of X-ray astronomy, spectral, spatial and timing observation improved dramatically, procuring a wealth of information on the majority of the classes of the celestial sources. Polarimetry, instead, remained basically unprobed. X-ray polarimetry promises to provide additional information procuring two new observable quantities, the degree and the angle of polarization. Polarization from celestial X-ray sources may derive from emission mechanisms themselves such as cyclotron, synchrotron and non-thermal bremsstrahlung, from scattering in aspheric accreting plasmas, such as disks, blobs and columns and from the presence of extreme magnetic field by means of vacuum polarization and birefringence. Matter in strong gravity fields and Quantum Gravity effects can be studied by X-ray polarimetry, too. POLARIX is a mission dedicated to X-ray polarimetry. It exploits the polarimetric response of a Gas Pixel Detector, combined with position sensitivity, that, at the focus of a telescope, results in a huge increase of sensitivity. The heart of the detector is an Application-Specific Integrated Circuit (ASIC) chip with 105,600 pixels each one containing a full complete electronic chain to image the track produced by the photoelectron. Three Gas Pixel Detectors are coupled with three X-ray optics which are the heritage of JET-X mission. A filter wheel hosting calibration sources unpolarized and polarized is dedicated to each detector for periodic on-ground and in-flight calibration. POLARIX will measure time resolved X-ray polarization with an angular resolution of about 20 arcsec in a field of view of 15 × 15 arcmin and with an energy resolution of 20% at 6 keV. The Minimum Detectable Polarization is 12% for a source having a flux of 1 mCrab and 105 s of observing time. The satellite will be placed in an equatorial orbit of 505 km of altitude by a Vega launcher. The telemetry down-link station will be Malindi. The pointing of POLARIX satellite will be gyroless and it will perform a double pointing during the earth occultation of one source, so maximizing the scientific return. POLARIX data are for 75% open to the community while 25% + SVP (Science Verification Phase, 1 month of operation) is dedicated to a core program activity open to the contribution of associated scientists. The planned duration of the mission is one year plus three months of commissioning and SVP, suitable to perform most of the basic science within the reach of this instrument. A nice to have idea is to use the same existing mandrels to build two additional telescopes of iridium with carbon coating plus two more detectors. The effective area in this case would be almost doubled. 相似文献
35.
Francesco Di Benedetto Francesco D’Acapito Gabriele Fornaciai Massimo Innocenti Giordano Montegrossi Luca A. Pardi Silvia Tesi Maurizio Romanelli 《Physics and Chemistry of Minerals》2010,37(5):283-289
An X-ray absorption spectroscopy (XAS) study of the Fe local environment in natural amethyst (a variety of α-quartz, SiO2) has been carried out. Room temperature measurements were performed at the Fe K-edge (7,112 eV), at both the X-ray absorption near-edge structure (XANES) and extended X-ray absorption fine structure (EXAFS) regions. Experimental results were then compared with DFT calculations. XANES experimental spectra suggest Fe to occur mainly in the trivalent state, although a fraction of Fe2+ is identified. EXAFS spectra, on the other hand, reveal an unusual short distance for the first coordination shell: = 1.78(2) Å, the coordination number being 2.7(5). These results allow to establish that Fe replaces Si in its tetrahedral site, and that numerous local distortions are occurring as a consequence of the presence of Fe3+ variably compensated by protons and/or alkaline ions, or uncompensated. The formal valence of Fe, on the basis of both experimental and DFT structural features, can be either 4+ or 3+. Taking into account the XANES evidences, we suggest that Fe mainly occurs in the trivalent state, compensated by protons, and that a minor fraction of Fe4+ is stabilised by the favourable local structural arrangement. 相似文献
36.
Jérôme Gattacceca Francis M. McCubbin Jeffrey N. Grossman Devin L. Schrader Nancy L. Chabot Massimo D'Orazio Cyrena Goodrich Ansgar Greshake Juliane Gross Katherine Helen Joy Mutsumi Komatsu Bingkui Miao 《Meteoritics & planetary science》2023,58(6):901-904
Meteoritical Bulletin 111 contains the 3094 meteorites approved by the Nomenclature Committee of the Meteoritical Society in 2022. It includes 11 falls (Antonin, Botohilitano, Cranfield, Golden, Great Salt Lake, Longde, Msied, Ponggo, Qiquanhu, Tiglit, Traspena), with 2533 ordinary chondrites, 165 HED, 123 carbonaceous chondrites (including 4 ungrouped), 82 lunar meteorites, 28 Rumuruti chondrites, 27 iron meteorites, 23 ureilites, 22 mesosiderites, 22 Martian meteorites, 21 primitive achondrites (one ungrouped), 17 ungrouped achondrites, 13 pallasites, 7 enstatite achondrites, 6 enstatite chondrites, and 5 angrites. Of the meteorites classified in 2022, 1787 were from Antarctica, 1078 from Africa, 180 from South America, 34 from Asia, 6 from North America, 4 from Europe, and 1 from Oceania. 相似文献
37.
Silvia Ceramicola Daniel Praeg Andrea Cova Daniela Accettella Massimo Zecchin 《Geo-Marine Letters》2014,34(2-3):111-129
Mud volcanoes (MVs) are abundant along the eastern Mediterranean subduction zones, recording mud breccia extrusion over long timescales (106 years), but to date relatively few have been recognised in the northern Ionian Sea on the Calabrian accretionary prism (CAP). In the present study, the seafloor distribution and recent activity of MVs is investigated across a 35,600 km2 sector of the CAP using a regional acoustic dataset (multibeam bathymetric and backscatter imagery, integrated with subbottom profiles) locally ground-truthed by sediment cores. A total of 54 MVs are identified across water depths of 150–2,750 m using up to four geophysical criteria: distinctive morphology, high backscatter, unstratified subbottom facies and, in one case, a hydroacoustic flare. Fourteen MVs are identified from 3–4 criteria, of which five have been previously proven by cores containing mud breccia beneath up to 1.6 m of hemipelagic sediments (Madonna dello Ionio MVs 1–3, Pythagoras MV and the newly named Sartori MV), while nine others are identified for the first time (Athena, Catanzaro, Cerere, Diana, Giunone, Minerva, ‘right foot’, Venere 1 and 2). Forty other as yet unnamed MVs are inferred from 1–2 geophysical criteria (three from distinctive morphology alone). All but one possible MV lie on the inner plateau of the CAP, landwards of the Calabrian Escarpment in a zone up to 120 km wide that includes the inner pre-Messinian wedge and the fore-arc basins, where they are interpreted to record the ascent from depth of overpressured fluids that interacted with tectonic structures and with evaporitic or shale seals within the fore-arc basins. The rise of fluids may have been triggered by post-Messinian out-of-sequence tectonism that affected the entire pre-Messinian prism, but Plio-Quaternary sedimentation rates and depositional styles support the inference that significant mud volcanism has taken place only on the inner plateau. Sedimentation rates across the CAP applied to a 12 khz sonar detection depth of 225 cm imply that all MVs with backscatter signatures (50 of 54) have erupted mud breccias within the last 56 ka, and within the last 12.5 ka in the fore-arc basins. Ages of eruption estimated from the depth of cored mud breccias at five MVs, and a seismo-stratigraphic relationship at a sixth, indicate episodes at the last glacial maximum ca. 20 ka BP and during the postglacial period. Eruptive episodes within the Calabrian MV province constitute recurrent geohazards, separated by longer periods of quiescent (subdued) fluid seepage that are likely to support gas hydrate formation and chemosynthetic ecosystems. 相似文献
38.
Tunnelling and Hydrogeological Issues: A Short Review of the Current State of the Art 总被引:1,自引:1,他引:0
Since the 1960s, there has been an increasing interest in the understanding of the hydraulic flow inside a hard rock mass, since water inflow into deep tunnels constitute a hazard, in addition to being an important factor in controlling the advancement of excavation. The characterisation of fluid flow through hard rock masses is still one of the most challenging problems faced by geologists and engineers. A rock mass is characterised by networks of discrete and ubiquitous discontinuities that strongly affect its hydraulic properties, but detailed knowledge of the discontinuity properties allows for the evaluation of the hydraulic flow in the rock mass affected by the excavation of a tunnel. A geostructural field survey is fundamental in order to correctly define the discontinuity types, settings and networks. Numerous approaches have been proposed to estimate the water inflow based on empirical relations supported by field experience and case studies, as well as analytical solutions. Often, however, these approaches are not easily applicable in standard practice and in complex scenarios. The most appropriate approach to characterising the hydraulic flow of the rock mass and to predicting in the most effective way the expected water inflow during the excavation of a tunnel is based on a detailed geological model and geostructural analysis as described in this paper. 相似文献
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Maurizio Gemelli Massimo D'Orazio Luigi Folco 《Geostandards and Geoanalytical Research》2015,39(1):55-69
We evaluate the performance of a hand‐held XRF (HHXRF) spectrometer for the bulk analysis of iron meteorites. Analytical precision and accuracy were tested on metal alloy certified reference materials and iron meteorites of known chemical composition. With minimal sample preparation (i.e., flat or roughly polished surfaces) HHXRF allowed the precise and accurate determination of most elements heavier than Mg, with concentrations > 0.01% m/m in metal alloy CRMs, and of major elements Fe and Ni and minor elements Co, P and S (generally ranging from 0.1 to 1% m/m) in iron meteorites. In addition, multiple HHXRF spot analyses could be used to determine the bulk chemical composition of iron meteorites, which are often characterised by sulfide and phosphide accessory minerals. In particular, it was possible to estimate the P and S bulk contents, which are of critical importance for the petrogenesis and evolution of Fe‐Ni‐rich liquids and iron meteorites. This study thus validates HHXRF as a valuable tool for use in meteoritics, allowing the rapid, non‐destructive (a) identification of the extraterrestrial origin of metallic objects (i.e., archaeological artefacts); (b) preliminary chemical classification of iron meteorites; (c) identification of mislabelled/unlabelled specimens in museums and private collections and (d) bulk analysis of iron meteorites. 相似文献