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71.
Ingrid Raczek Brigitte Stoll Albrecht W. Hofmann Klaus Peter Jochum 《Geostandards and Geoanalytical Research》2001,25(1):77-86
Different batches of the new US Geological Survey (USGS) reference materials (RMs) BCR-2, BHVO-2, AGV-2, DTS-2 and GSP-2 and the original USGS RMs BCR-1, BHVO-1, AGV-1, DTS-1 and GSP-1 have been analysed by isotope dilution using thermal ionisation mass spectrometry (ID-TIMS) and by multi-ion counting spark source mass spectrometry (MIC-SSMS). The concentrations of K, Rb, Sr, Ba and the rare earth elements were determined with overall analytical uncertainties of better than 1% (ID-TIMS) and 3% (MIC-SSMS). The analyses of different aliquots and batches of BCR-2, BHVO-2, AGV-2 and GSP-2, respectively, agree within 1%, i.e. approximately the analytical uncertainties of the data. This indicates an homogeneous distribution of the trace elements in these RMs. Differences in element concentrations of up to 17% in different aliquots of the depleted RM DTS-2 are outside the analytical uncertainty of our data. They may be attributed to a slightly heterogeneous distribution of trace elements in this dunite sample. Our trace element data for BCR-2, BHVO-2, AGV-2 and GSP-2 agree within about 3% with preliminary reference values published by the USGS. They also agree within 1-6% with those of the original RMs BCR-1, BHVO-1, AGV-1 and GSP-1. Large compositional differences are found between DTS-2 and DTS-1, where the concentrations of K, Rb, Sr and the light REE differ by factors of 2 to 24. 相似文献
72.
The Preparation and Preliminary Characterisation of Eight Geological MPI-DING Reference Glasses for In-Situ Microanalysis 总被引:13,自引:4,他引:9
Klaus Peter Jochum Donald B. Dingwell Alexander Rocholl Brigitte Stoll Albrecht W. Hofmann S. Becker A. Besmehn D. Bessette H.-J. Dietze P. Dulski J. Erzinger E. Hellebrand P. Hoppe I. Horn K. Janssens G.A. Jenner M. Klein W.F. McDonough M. Maetz K. Mezger C. Müker I.K. Nikogosian C. Pickhardt I. Raczek D. Rhede H.M. Seufert S.G. Simakin A.V. Sobolev B. Spettel S. Straub L. Vincze A. Wallianos G. Weckwerth S. Weyer D. Wolf M. Zimmer 《Geostandards and Geoanalytical Research》2000,24(1):87-133
Eight silicate glasses were prepared by directly fusing and stirring 50-100 g each of basalt, andesite, komatiite, peridotite, rhyolite, and quartz-diorite. These are referred to as MPI-DING glasses and were made for the purpose of providing reference materials for geochemical, in-situ microanalytical work. Results from various analytical techniques indicate that individual glass fragments are well homogenised with respect to major and trace elements at the μm to mm scale. Heterogeneities due to quench crystallisation of olivine have been observed in small and limited areas of the two komatiitic glasses. In order to obtain concentration values for as many elements as possible, the glasses were analysed by a variety of bulk and microanalytical methods in a number of laboratories. The analytical uncertainties of most elements are estimated to be between 1% and 10%. From the analytical data, preliminary reference values for more than sixty elements were calculated. The analytical uncertainties of most elements are estimated to be between 1% and 10%. 相似文献
73.
Jorge?Plá Cid Lauro?Valentim?Stoll?NardiEmail author Pere?Enrique?Gisbert Claude?Merlet Bernard?Boyer 《Contributions to Mineralogy and Petrology》2005,148(6):675-688
Trace and rare earth element contents were determined by SIMS technique in clinopyroxene and mica crystals from minette lamprophyric enclaves in a potassic syenite host. This co-mingled system was crystallized at high pressures, which varied about 3–5 GPa, as indicated by the presence of K-clinopyroxenes and pyrope-rich garnet with measurable amounts of K2O and Na2O, among the near-liquidus phases. Major and trace element composition of these lamprophyric enclaves is quite similar to those observed in silica-rich lamproites, suggesting that similar sources were involved in their origin. In a general view, the concentrations of most trace and rare earth elements in clinopyroxene of the studied enclaves are higher than those referred to by other authors. Clinopyroxene/melt partition coefficient for most trace elements are close to determinations in alkali-basalts and lamproites from Leucite Hills, with considerable differences relative to Gaussberg lamproites. Furthermore, these partition data are completely different from those determined for potassic lavas crystallized under crustal pressures. Spidergrams for clinopyroxenes exhibit negative-Sr anomalies relative to LREE, which have been associated by most authors to crystallization under low-pressures, out of garnet stability field. The presence of pyrope together with K-clinopyroxene excludes such hypotheses for the studied enclaves. Y and HREE are concentrated in clinopyroxene, whilst the other trace elements have Kd<1. LIL elements, except Rb, have incompatible (Kd<1) behavior in phlogopite. The high partition coefficient for Nb (Kd>3) determined in the studied phlogopite is unusual in lamproites, lamprophyres, and basalts, but frequently observed in phlogopite from metasomatic mantle samples, as well as in acid magmas. This partition value may indicate the lack of other mineral phase with high partition for this element during crystallization, and may be enhanced by the liquid composition progressively closer to alkali feldspar, an unsuitable structure for six-coordinated cations. Ce/Yb, Rb/Sr, and Zr/Hf ratios in clinopyroxene and mica suggest that the minettic magma could produce the host Piquiri potassic syenite by fractional crystallization. This hypothesis is not consistent with Ba concentrations in clinopyroxene and mica, which suggest that a Ba-bearing phase (e.g. alkali feldspar) should be among the fractionated phases in order to produce the potassic syenites. 相似文献
74.
Potassic and low- and high-Ti mildly alkaline volcanism in the Neoproterozoic Ramada Plateau, southernmost Brazil 总被引:1,自引:0,他引:1
Carlos Augusto Sommer Evandro Fernandes de Lima Lauro Valentim Stoll Nardi Ana Maria Graciano Figueiredo Ronaldo Pierosan 《Journal of South American Earth Sciences》2005,18(3-4):237-254
Ramada Plateau Neoproterozoic volcanism represents a portion of the shoshonitic and mildly alkaline magmatism related to postcollisional events of the Brasiliano/Pan African cycle of southernmost Brazil. It is constituted by shoshonitic basic-intermediate lavas, followed by a bimodal sequence characterized by pyroclastic deposits, lava flows, and hypabyssal rocks with ages of 549±5 Ma. The shoshonitic magmatism presents greater K2O than Na2O2, K2O/Na2O ratios close to 1, and moderate large ion lithophile and high-field strength element contents. The bimodal basic-acid volcanism presents a transitional chemical affinity with features of sodic, silica-saturated alkaline to continental tholeiitic series. Observed basic and acid rocks with contrasting Ti contents are referred to as high- and low-Ti basalt-rhyolites. Another group of acid rocks with higher Nb, Ta, and Rb values was identified as high-Nb rhyolites. The Ramada Plateau magmatism is comparable to associations related to the final stages of orogenic cycles, in which shoshonitic and high- and low-Ti alkaline magmatism reflects the melting of subduction-modified sources, whereas the high-Nb magmas show less influence of subduction-related metasomatism and are closer to magmas produced from anorogenic sources. A model of magma generation in collisional settings involving slab break-off and asthenospheric upwelling is applied to the evolution of magmatism from subduction-related to anorogenic in the Ramada Plateau. 相似文献
75.
76.
The coccolithophore Emiliania huxleyi was grown in seawater under different Ba concentrations. The relationship of coccolith Ba/Ca ratio and seawater Ba/Ca ratio was found to be linear. The linear regression yields the apparent Ba exchange coefficient of 0.10. Our data support a recently proposed generic model (Langer G., Gussone N., Nehrke G., Riebesell U., Eisenhauer A., Kuhnert H., Rost B., Trimborn S., and Thoms S. (2006) Coccolith strontium to calcium ratios in Emiliania huxleyi: the dependence on seawater strontium and calcium concentrations. Limnol. Oceanogr.51, 310-320.) developed for explaining apparent exchange coefficients of metabolically inert divalent trace metals, such as Sr, in E. huxleyi. This model represents the first approach combining cell physiological processes and data from inorganic precipitation experiments, which quantitatively explains coccolith apparent Sr and Ba exchange coefficients. 相似文献
77.
Reference Values Following ISO Guidelines for Frequently Requested Rock Reference Materials 总被引:2,自引:0,他引:2
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Klaus Peter Jochum Ulrike Weis Beate Schwager Brigitte Stoll Stephen A. Wilson Gerald H. Haug Meinrat O. Andreae Jacinta Enzweiler 《Geostandards and Geoanalytical Research》2016,40(3):333-350
We present new reference values for nineteen USGS, GSJ and GIT‐IWG rock reference materials that belong to the most accessed samples of the GeoReM database. The determination of the reference values and their uncertainties at the 95% confidence level follows as closely as possible ISO guidelines and the Certification Protocol of the International Association of Geoanalysts. We used analytical data obtained by the state‐of‐the‐art techniques published mainly in the last 20 years and available in GeoReM. The data are grouped into four categories of different levels of metrological confidence, starting with isotope dilution mass spectrometry as a primary method. Data quality was checked by careful investigation of analytical procedures and by the application of the Horwitz function. As a result, we assign a new and more reliable set of reference values and respective uncertainties for major, minor and a large group of trace elements of the nineteen investigated rock reference materials. 相似文献
78.
79.
A method for determing the brightness and diameter of galaxies in a large field on Schmidt plates by automatic scanning with a microphotometer is described and applied to the ABELL cluster A 1781. The accuracy of this method is tested. The overall errors (r.m.s.) of brightness and diameter are 0.16 mag and 0″.44. The cluster A 1781 has been prooved to be a very poor cluster of about 10 members up to mB ≈ 19m.5. 相似文献
80.
We present the position and references (if available) of all the galaxies of the Shakhbazian survey being the largest survey of compact galaxy groups. For the estimation of the coordinates the Digitized Sky Survey was used. This paper contains the data of 48 Shakhbazian groups north of δ > + 2deg;30' (Shkh 2, 3, 4, 5, 6, 7, 8, 9, 10, 11, 12, 13, 14, 15, 16, 17, 18, 19, 20, 22, 23, 25, 26, 28, 29, 31, 34, 36, 37, 38, 39, 40, 41, 42, 43, 44, 45, 46, 47, 48, 49, 50, 51, 52, 53, 54, 55, 56). 相似文献