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71.
A New Reference Material for Tritium Organic Molecules in Sediment: Results of an International Intercomparison Exercise 下载免费PDF全文
Phillip E. Warwick Ian W. Croudace Richard M. Marsh Nicolas Baglan Sang Bog Kim 《Geostandards and Geoanalytical Research》2018,42(2):253-262
Solid matrix 3H reference materials are challenging to prepare given the volatile nature of 3H and are often unrepresentative of the range of 3H forms that may be encountered during routine analysis. As a result, few 3H reference materials are currently available, undermining verification of analytical techniques for environmental 3H measurement. To address this, an International Working Group on Organically‐Bound Tritium Analysis determined to produce a tritium natural matrix reference material (NMRM). The reference material comprises marine sediment blended with sewage sludge contaminated with 3H‐organic species arising from authorised discharges from a radiopharmaceutical manufacturing site. Previous studies have demonstrated that the 3H species have persisted in the environment over three decades providing valuable supporting data to underpin the characterisation of the NMRM. The preparation and characterisation of the NMRM are described along with the subsequent application of the reference material in an international intercomparison exercise involving nineteen laboratories from nine countries. A reference value of 168 ± 22 Bq kg?1 was derived from the data arising from the proficiency test. 相似文献
72.
Shane?M.?RooyakkersEmail authorView authors OrcID profile Colin?J.?N.?Wilson C.?Ian?Schipper Simon?J.?Barker Aidan?S.?R.?Allan 《Contributions to Mineralogy and Petrology》2018,173(5):35
Quenched juvenile mafic inclusions (enclaves) are an occasional but informative component in the deposits of large felsic eruptions. Typically, the groundmasses of these inclusions rapidly crystallize as the mafic magma is chilled against a more voluminous, cooler felsic host, providing a physical and chemical record of the nature and timing of mafic–felsic interactions. We examine mafic inclusions of two compositional lineages (tholeiitic and calc-alkaline) from deposits of the 25.4 ka Oruanui eruption (Taupo, New Zealand). 2-D quantitative textural data from analysis of back-scattered electron images reveal a marked diversity in the groundmass textures of the inclusions, including median crystal sizes (amphibole: 14–45 µm; plagioclase: 21–75 µm) and aspect ratios (amphibole: 1.7–4.2; plagioclase: 2.1–4.0), area number densities (amphibole: 122–2660 mm?2; plagioclase: 117–2990 mm?2), area fractions (?) of minerals (?plag?=?23–45%, ?amph?=?0–28%, ?cpx?=?0–6%, ?oxides?=?0.6–5.5%), and the relative abundance of plagioclase and amphibole (?plag/?amph?=?1.0–4.6). Textural parameters vary more significantly within, rather than between, the two compositional lineages, and in some cases show marked variations across individual clasts, implying that each inclusion’s cooling history, rather than bulk composition, was the dominant control on textural development. Groundmass mineral compositions are also diverse both within and between inclusions (e.g. plagioclase from An34–92, with typical intra-clast variability of ~?20 mol%), and do not correlate with bulk chemistry. Diverse groundmass textures and mineral and glass chemistries are inferred to reflect complex interplay of a range of factors including the degree and rate of undercooling, bulk composition, water content and, possibly, intensive variables. Our data are inconsistent with breakup of a crystallizing ponded mafic layer at the base of the Oruanui melt-dominant body, instead implying that each inclusion partially crystallized as a discrete body with a unique cooling history. Extensive ingestion of mush-derived macro-crystals suggests that mechanical breakup of mafic feeder dikes occurred within a transition zone between the mush and melt-dominant magma body. In this zone, the mush lacked yield strength, as has been inferred from field studies of narrow (meters to few tens of meters) mush-melt transition zones preserved in composite intrusions. Evidence for plastic deformation of inclusions during eruption and the abundance of fresh residual glass in inclusions from all eruptive phases suggest that the inclusions formed syn-eruptively, and must have been formed recurrently at multiple stages throughout the eruption. 相似文献
73.
Jonathan R. Lee Ian Candy Richard Haslam 《Proceedings of the Geologists' Association. Geologists' Association》2018,129(3):452-481
During the Neogene and Quaternary, tectonic and climatic processes have had a profound impact upon landscape evolution in England and, perhaps as far back as 0.9 Ma, patterns of early human occupation. Until the Late Miocene, large-scale plate tectonic processes were the principal drivers of landscape evolution causing localised basin inversion and widespread exhumation. This drove, in places, the erosion of several kilometres of Mesozoic cover rocks and the development of a regional unconformity across England and the North Sea Basin. By the Pliocene, the relative influence of tectonics on landscape evolution waned as the background tectonic stress regime evolved and climatic influences became more prominent. Global-scale climate-forcing increased step-wise during the Plio-Pleistocene amplifying erosional and depositional processes that operated within the landscape. These processes caused differential unloading (uplift) and loading (subsidence) of the crust (‘denudational isostasy’) in areas undergoing net erosion (upland areas and slopes) and deposition (basins). Denudational isostasy amplified during the Mid-Pleistocene Transition (c.0.9 Ma) as landscapes become progressively synchronised to large-scale 100 ka ‘eccentricity’ climate forcing. Over the past 0.5 Ma, this has led to the establishment of a robust climate record of individual glacial/interglacial cycles enabling comparison to other regional and global records. During the Last Glacial-Interglacial Transition and early Holocene (c.16–7 ka), evidence for more abrupt (millennial/centennial) scale climatic events has been discovered. This indicates that superimposed upon the longer-term pattern of landscape evolution is a more dynamic response of the landscape to local and regional drivers. 相似文献
74.
Jan Zalasiewicz Colin Waters Mark Williams David C. Aldridge Ian P. Wilkinson 《Proceedings of the Geologists' Association. Geologists' Association》2018,129(3):482-491
The Anthropocene deposits of England, here regarded as those formed after ~1950 CE, are now extensive, take various forms, and may be characterized and recognized by a number of stratigraphic signals, such as artificial radionuclides, pesticide residues, microplastics, enhanced fly ash levels, concrete fragments and a novel variety of ‘technofossils’ and neobiotic species. They include the uppermost parts of both ‘natural’ deposits such as the sediment layers formed in lakes and estuaries, and more directly human-made or human-influenced ones such as landfill deposits and the ‘artificial ground’ beneath urban areas and around major constructions. ‘Negative deposits’ include the worked areas of quarries and regions such as the English Fenland, where thick peat deposits have ablated to leave a strongly modified underlying landscape, and extend beneath into the subterranean realm as mine workings, metro systems and boreholes. The production of these is still rapidly increasing and evolving in character, while the early signs of global change, such as warming, sea level rise, and modifications to biotic assemblages, are beginning to further modify the emerging geology of this new phase of Earth history. 相似文献
75.
Bernhard Jenny Daniel M. Stephen Ian Muehlenhaus Brooke E. Marston Ritesh Sharma Eugene Zhang 《制图学和地理信息科学》2018,45(1):62-75
Origin-destination flow maps are often difficult to read due to overlapping flows. Cartographers have developed design principles in manual cartography for origin-destination flow maps to reduce overlaps and increase readability. These design principles are identified and documented using a quantitative content analysis of 97 geographic origin-destination flow maps without branching or merging flows. The effectiveness of selected design principles is verified in a user study with 215 participants. Findings show that (a) curved flows are more effective than straight flows, (b) arrows indicate direction more effectively than tapered line widths, and (c) flows between nodes are more effective than flows between areas. These findings, combined with results from user studies in graph drawing, conclude that effective and efficient origin-destination flow maps should be designed according to the following design principles: overlaps between flows are minimized; symmetric flows are preferred to asymmetric flows; longer flows are curved more than shorter or peripheral flows; acute angles between crossing flows are avoided; sharp bends in flow lines are avoided; flows do not pass under unconnected nodes; flows are radially distributed around nodes; flow direction is indicated with arrowheads; and flow width is scaled with represented quantity. 相似文献
76.
Rhys G. O. Timms Ashley M. Abrook Ian P. Matthews Christopher P. Francis Agnieszka Mroczkowska Ian Candy Stephen J. Brooks Alice M. Milner Adrian P. Palmer 《第四纪科学杂志》2021,36(3):339-359
The influence of the North Atlantic on the margins of Europe means the region is particularly sensitive to changes in the ocean–atmospheric system. During the Last Glacial–Interglacial Transition (16–8 cal ka bp ) this system was repeatedly disrupted, leading to a series of abrupt and short-lived shifts in climate. Despite much research, the number and magnitude of these ‘centennial-scale’ events is not well understood. To address this, we expand upon investigations at Quoyloo Meadow, Orkney, Scotland, one of the best chronologically constrained palaeoclimate records in northern Britain. By coupling stable isotope and chironomid fossil analyses with existing data, this study identifies multiple phases of centennial-scale disturbance at: c. 14.0, 11.1, 10.8, 10.5, 10.45 and 10.3 cal ka bp , with the events at 14.0 and 10.3 exhibiting a particularly pronounced cold-climate signature. During the Holocene, the strongest response to climate forcing was at c. 10.3–10.0 cal ka bp , expressed as a two-stage drop in mean July temperatures, a shift in pollen spectra indicative of ‘less-stable’ climatic regimes, and a depletion in δ18O values. We interpret this as the first reliably dated incidence of the ‘10.3-ka event’ in the British Isles and consider the wider impact of this climatic reversal in other Holocene records. 相似文献
77.
78.
For the first time Arundian and Holkerian faunas have been recognized from the lower part of the Dinantian succession in North Wales. These limestones and sandstones, hitherto regarded as Asbian, have a macrofauna and microfauna confirming their older age, and this discovery' has necessitated a revision of the palaeogeography in the North Wales region. Biostratigraphical correlations have been made with contemporaneous platform successions in the Central, Northern, and Southwest Provinces of Britain. A new genus and species of foraminifer, Groessensella moldensis, is described. 相似文献
79.
Hikari Hasegawa Takashi Mikouchi Akira Yamaguchi Masahiro Yasutake Richard C. Greenwood Ian A. Franchi 《Meteoritics & planetary science》2019,54(4):752-767
Northwest Africa (NWA) 6112, Miller Range (MIL) 090206 (plus its pairs: MIL 090340 and MIL 090405), and Divnoe are olivine‐rich ungrouped achondrites. We investigated and compared their petrography, mineralogy, and olivine fabrics. We additionally measured the oxygen isotopic compositions of NWA 6112. They show similar petrography, mineralogy, and oxygen isotopic compositions and we concluded that these five meteorites are brachinite clan meteorites. We found that NWA 6112 and Divnoe had a c axis concentration pattern of olivine fabrics using electron backscattered diffraction (EBSD). NWA 6112 and Divnoe are suggested to have been exposed to magmatic melt flows during their crystallization on their parent body. On the other hand, the three MIL meteorites have b axis concentration patterns of olivine fabrics. This indicates that the three MIL meteorites may be cumulates where compaction of olivine grains was dominant. Alternatively, they formed as residues and were exposed to olivine compaction. The presence of two different olivine fabric patterns implies that the parent body(s) of brachinite clan meteorites experienced diverse igneous processes. 相似文献
80.
Paula Lindgren Lydia Hallis Fredrik S. Hage Martin R. Lee John Parnell Anders Plan Alistair Doye Ian MacLaren 《Meteoritics & planetary science》2019,54(11):2698-2709
A carbon‐rich melt fragment from the Gardnos impact structure has been studied for a better understanding of the preservation and structural form(s) of carbon that have been processed by impact melting. The carbon was analyzed in situ in its original petrographic context within the melt fragment, using high‐resolution techniques including focused ion beam‐transmission electron microscopy and electron energy loss spectroscopy. Results show that the carbon is largely uniform and has a nanocrystalline grain size. The Gardnos carbon has a graphitic structure but with a large c/a ratio indicating disorder. The disorder could be a result of rapid heating to high temperatures during impact, followed by rapid cooling, with not enough time to crystallize into highly ordered graphite. However, temperature distribution during impact is extremely heterogenous, and the disordered Gardnos carbon could also represent material that avoided extreme temperatures, and thus, it was preserved. Understanding the structure of carbon during terrestrial impacts is important to help determine if the history of carbon within extraterrestrial samples is impact related. Furthermore, the degree of preservation of carbon during impact is key for locating and detecting organic compounds in extraterrestrial samples. This example from Gardnos, together with previous studies, shows that not all carbon is lost to oxidation during impact but that impact melting can encapsulate and preserve carbon where it is available. 相似文献