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β-环糊精包合态三氟氯氰杀虫剂的制备 总被引:3,自引:0,他引:3
为了进一步提高三氟氯氰菊酯农药的防治效果。寻找适宜的农药新剂型,我们用液相法制备了三氟氯氰菊酯-β-环糊精包合物,并以水为基质进行了稳定性观察,同时又以差热分析法和气相色谱法确认了包合物的形成,以旋光度法证明两者间的包合比。结果表明,三氟氯氰菊酯与β-环糊精可形成1:1型包合物,该包合物稳定性高,具有一定的水溶性,而且在水中稳定,所以有望通过环糊 包合作用将三氟氯氰菊酯帛成水剂;当以气相法测试包合态三氟氯氰菊酯含量时,必须将其解络,使之成为游离状态,然后按常规方法进行含量测定。 相似文献
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本文对松辽盆地东南部后五家户气田划分出22种沉积微相,建立7种相层序,分析了扇三角洲及三角洲沉积环境对天然气成藏的控制作用。指出了扇三角洲前缘砂体和三角洲前缘砂体较为发育,沉积物源来自气田东北部和东南部两个方向。后五家户气田多为构造—岩性气藏和岩性气藏。 相似文献
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Introduction The Western Kunlun Mountain Pass M=8.1 earthquake occurred on November 14, 2001 is the other M=8 earthquake occurred 50 years after Dangxiong, Tibet M=8.0 earthquake in Chinese mainland. The earthquake has caused the attention of the seismologists in the following aspects: 1) The fracture length is more than 400 km, which is far away from the estimated length by the statistic empirical function between the magnitude and the fracture length (WANG, et al, 2002); 2) The aftersh… 相似文献
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Short period surface waves, recorded during a seismic refractionsurvey in the Sannio region (Southern Italy), have been modeled to infera shallow velocity model for the area. Based on the decrease of resolutionwith depth, due to the bias on group velocity estimates arising frominterference of the Rayleigh waves with higher modes, we carried out aprocedure of fitting, with synthetic seismograms, of selected filtered traceswith a gaussian filter, having a width at half height equal to 1 Hz and acentral frequency lying in the range [1,4] Hz. We estimated the likelihoodbetween synthetic and observed seismograms by measuring their semblance.In this way we were able to infer a more refined local velocity modelcharacterized by a high Vp and Vs vertical gradient in the sedimentarycover. Two ad hoc resolution studies, based on group velocity andamplitude data respectively, indicate that the local velocity model is a goodvelocity model also for the entire studied area. The increase in the numberof available data when using amplitude information allows us to make amore selective choice in the model parameter space (Vp and Vs of eachlayer) and to solve for the Vp/Vs ratio. The inferred Vp velocity in thehalf-space is equal to 2.8 km/s. This value is in excellent agreement withthat inferred by other authors (3 km/s) by modeling P-wave travel timevs. distance. The best-fit model furnish low Vp/Vs for the sedimentarycover so indicating a high degree of the sediment's compaction in thestudied area. The inferred shallow high-velocity gradient indicates thatthe shallow sedimentary layer in the area could trap and focus the energytraveling into it. 相似文献
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Andesitic pillow lavas containing biogenic, solid bitumen (SB) are a constituent of a Neoproterozoic volcanosedimentary sequence (Teplá-Barrandian unit, Bohemian Massif) in the Mítov area of the Czech Republic. A black shale formation that is crosscut by these andesitic basalts is 565 Ma old. Carbon disulfide extracts of two powdered samples of SB contain 0.2 and 0.3 ppm of C60, respectively, as determined by high-pressure liquid chromatography. The peak assignment based on retention time is fully supported by high-resolution electron ionization mass spectrometry (EI-MS). No C70 was detected, nor was C60 found in two other SB samples from this locality. Other investigated carbonaceous samples from Bohemia (coals and anthracites of Upper Paleozoic age and anthraxolite, graphitoids, and graphite of Upper Proterozoic age) did not contain fullerenes at concentrations above the detection limit of 0.01 ppm. The absence of C60 in these samples was confirmed by EI-MS. The proposed mechanism of fullerene formation involves a primary algal phase, generation of a hydrocarbonaceous mixture in the course of thermal evolution of the sedimentary series, and their high-temperature transformation related to the extrusion of basalt. An important feature for fullerene conservation was the enclosure of fullerenes in SB with a structure similar to glasslike carbon, where the fullerene was protected against oxidation. 相似文献
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