Investigation of ion beam techniques for the analysis and exposure of particles encapsulated by silica aerogel: Applicability for Stardust

Abstract— In 2006, the Stardust spacecraft will return to Earth with cometary and perhaps interstellar dust particles embedded in silica aerogel collectors for analysis in terrestrial laboratories. These particles will be the first sample return from a solid planetary body since the Apollo missions. In preparation for the return, analogue particles were implanted into a keystone of silica aerogel that had been extracted from bulk silica aerogel using the optical technique described in Westphal et al. (2004). These particles were subsequently analyzed using analytical techniques associated with the use of a nuclear microprobe. The particles have been analyzed using: a) scanning transmission ion microscopy (STIM) that enables quantitative density imaging; b) proton elastic scattering analysis (PESA) and proton backscattering (PBS) for the detection of light elements including hydrogen; and c) proton‐induced X‐ray emission (PIXE) for elements with Z > 11. These analytical techniques have enabled us to quantify the composition of the encapsulated particles. A significant observation from the study is the variable column density of the silica aerogel. We also observed organic contamination within the silica aerogel. The implanted particles were then subjected to focused ion beam (FIB) milling using a 30 keV gallium ion beam to ablate silica aerogel in site‐specific areas to expose embedded particles. An ion polished flat surface of one of the particles was also prepared using the FIB. Here, we show that ion beam techniques have great potential in assisting with the analysis and exposure of Stardust particles.     

Ocean-floor hydrothermal metamorphism in the Limousin ophiolites (western French Massif Central): evidence of a rare preserved Variscan oceanic marker

The Limousin ophiolite is located at the suture zone between two major thrust sheets in the western French Massif Central. This ophiolitic section comprises mantle‐harzburgite, mantle‐dunite, wehrlites, troctolites and layered gabbros. It has recorded a static metamorphic event transforming the gabbros into undeformed amphibolites and the magmatic ultramafites into serpentinites and/or pargasite‐bearing chloritites. With various thermobarometric methods, it is possible to show that the different varieties of amphibole have registered low‐P (c. 0.2 GPa) conditions with temperature ranging from high‐T, late‐magmatic conditions to greenschist–zeolite metamorphic facies. The abundance of undeformed metamorphic rocks (which is typical of the lower oceanic crust), the occurrence of Ca–Al (–Mg) metasomatism illustrated by the growth of Ca–Al silicates in veins or replacing the primary magmatic minerals, the P–T conditions of the metamorphism and the numerous similarities with oceanic crustal rocks from Ocean Drilling Program and worldwide ophiolites are the main arguments for an ocean‐floor hydrothermal metamorphism in the vicinity of a palaeo‐ridge. Among the West‐European Variscan ophiolites, the Limousin ophiolites constitute an extremely rare occurrence that has not been involved in any HP (subduction‐related) or MP (orogenic) metamorphism as observed in other ophiolite occurrences (i.e. France, Spain and Germany).     

A lower limit to the field strength in magnetic reconnection sites in solar flares inferred from hard X-ray bursts

It is shown how the hard X-ray burst count rate and itse-folding ime can be used to estimate the minimum magnetic fieldB _min required in a flare magnetic reconnection site for the burst to be interpreted in terms of a thick target model. Application of the method to data from the Solar Maximum Mission (HXRBS) indicates absolute minimum fields well in excess of 100 G, and impossibly high values for some reconnection geometries.     

Seasonal variations in prey selection by estuarine black-headed gulls (Larus ridibundus)

The number of black-headed gulls (Larus ridibundus) in the Clyde Estuary is large. In summer the average density has reached 1350 gulls km^?2 and in winter 180 gulls km^?2. This paper compares prey selection and feeding efficiency in gulls during summer and winter on tidal flats, and considers how seasonal differences may be adaptations to cope with seasonal changes in prey availability.Gross and net rates of energy intake were highest in summer because gulls captured more of the polychaete N. diversicolor than the amphipod C. volutator. In winter, gulls selected for C. volutator and therefore an energetically less profitable diet. Throughout the year gulls selected more C. volutator relative to N. diversicolor than expected on energetic grounds and so apparently did not maximize potential net rate of energy intake.Gulls used three techniques to capture prey and made most intensive use of the ‘crouch’ technique. Crouching gulls attained a much higher net rate of energy intake than ‘upright’ or ‘paddling’ gulls.A log-linear model showed that (a) season, water depth and gull density determined feeding technique and (b) feeding technique and season independently determined foraging success and prey selection. Thus gull density and water depth acted on prey selection through imposed variations in feeding technique.Reasons for gulls selecting energetically unprofitable C. volutator and for the use of several distinct feeding techniques are discussed.     

Geothermal palaeogradients and metamorphic zonation from the conodont colour alteration index (CAI)

The conodont colour alteration index (CAI) is potentially valuable in thermal history investigations, but there are problems in its use. An approach is proposed herein to overcome the problem of establishing reliable geothermal palaeogradients in areas with burial metamorphism, based on knowledge of the stratigraphic succession thickness, the boundaries of chronostratigraphic units, and the age and duration of deformation episodes. Although also problematical that a correlation between CAI and Kübler index (KI) values does not exist, there are areas where CAI and KI values are notably consistent for the anchizone boundaries; however, anomalous correlations between CAI and KI values have also been found in some areas. A CAI anchizone (or ancaizone) is defined in order to enable CAI values to be used independently to establish a metamorphic zonation.     

Is dark matter created in the gravitation field of galaxies?

Using the heuristic arguments of quantum physics we describe a new mechanism of the creation of short-living particles from the virtual ones in a stationary gravitation field. The mass of these particles is a function of the intensity of gravitation field. We suppose that the particles created in the gravitation field form a part of the non-baryonic dark matter. Having the intensity of gravitation field in a galaxy we can calculate the density of dark matter created in it by the vacuum quantum fluctuation. We calculate the distribution of this dark matter in a model galaxy and show that its total mass is comparable with the visible mass of the galaxy.     

Solar-planetary cycles in Jupiter's great red spot darkness

The change in the darkness of the Great Red Spot (GRS) of Jupiter (1894–1974) has been analysed with Fourier (FFT), Maximum Entropy and Power spectrum (Blackman-Tukey window) (PSA) methods of spectrum analysis. Significance, non-randomness and stationarity tests assigned high variance to periodicities of 33 ± 4, 13–15, about 11, 9 and 3 yrs. The highest correlation between solar activity and GRS darkness was found for the 14th and 16th solar cycle. The periodicities obtained are interpreted as the combined eftects of solar activity, planetary resonances and internal jovian mechanisms.     

Brief description of bare essentials of surface transfer and results from simulations with the HAPEX-MOBILHY data

The Bare Essentials of Surface Transfer (BEST) land surface scheme is briefly described and the key physical parameterisations discussed. Results are then presented to illustrate how the model performs, with forcing data for HAPEX-MOBILHY, compared to a series of other schemes in the simulation of evaporation and sensible heat. The implications of the models performance, and some indications of the future development of the scheme are provided. The basic version of BEST was found to overestimate evaporation for the HAPEX-MOBILHY data, simulating 816 mm yr⁻¹ compared to a range of 550 to 816 mm yr⁻¹ for all models. A modification to the β parameterisation reduced the evaporation to 759 mm yr⁻¹ which, although an improvement, is still probably too high.