GDX-502树脂富集高效液相色谱法测定地表水中酚类化合物

采用自制GDX-502固相萃取小柱萃取水中苯酚、对硝基酚、间甲酚、2，4-二氯酚、2，4，6-三氯酚、五氯酚等6种酚类化合物，以乙腈作为洗脱剂，选择280nm和290nm双波长紫外高效液相色谱进行检测。结果表明，方法检出限为0．01-0．05mg／L，IL水的平均加标回收率为82．5％-95．0％，精密度（RSD，n=7）为3．6％-9．2％。方法用于实际地表水中痕量酚类化合物的检测，操作简单，有机溶剂用量少，分析效率高；萃取小柱可多次重复使用，分析成本低。     

青藏高原北部新生代湖相碳酸盐岩碳氧同位素特征及古环境意义

对青藏高原北部地区新生代陆相地层中湖相碳酸盐岩进行了系统采样分析，以碳氧同位素作为古环境和古气候变化的替代指标,试图从古湖泊演化的角度，阐明高原新生代早期环境演变历史和过程。研究结果表明，该区所有分析样品中生物碎屑灰岩类样品的δ¹⁸O和δ¹³C显示最低值，反映它们沉积在一个水体滞留时间短的开放性淡水湖泊系统中。泥晶灰岩类样品的δ¹⁸O和δ¹³C之间具有正相关关系，表明它们发育在蒸发作用明显的封闭性咸水湖泊体系中，而叠层石灰岩类明显富集13C可能与微生物活动有关。从始新世到渐新世至中新世，湖相碳酸盐岩δ¹⁸O值具有逐渐增大的趋势，δ¹³C则由古近纪的负值变为新近纪的正值，反映该区古湖泊系统经历了一个由开放到封闭的过程，预示古近纪到新近纪之交高原古气候格局发生了重大变革。     

滇东伊迪卡拉（震旦）系顶部旧城段多样宏体化石群的发现?

中国云南东部晋宁、江川地区的伊迪卡拉（震旦）系顶部灯影组旧城段新发现了多样的宏体化石群，除了丰富的Vendotaenia与Tyrasotaenia类化石以外，以形体较大的Tawuia类和Longfengshaniaceae科等具固着构造的底栖多细胞藻类化石占据优势，另有一些形态奇特、亲缘关系不明的宏体化石，该组合与华南陡山沱组和灯影组石板滩段的宏体化石组合相比存在着明显的差别。依据形态特征，本文概述了部分产自江川旧城段的具有不同类型固着构造的底栖藻类和归属不明的宏体化石特征。华南滇东地区旧城段形态多样的宏体藻类化石的发现，进一步表明伊迪卡拉纪末期存在后生植物的多样化发展。这一时期浮游微生物和后生植物的共同繁盛可能为早寒武世“澄江生物群”的爆发奠定了生态基础。     

中国优质环保型炼焦煤的评价及资源量等级

我国炼焦煤资源丰富，但优质炼焦煤一直处于短缺局面。根据全国已有煤质数据分析，从优质（主要考虑挥发分指标）、环保（主要考虑硫分和灰分指标）两个方面结合有害微量元素含量，将炼焦煤划分为四种类型，确定了优质环保型炼焦煤资源的评价步骤，对全国五个赋煤区优质环保型炼焦煤的资源量等级进行了统计分析。     

南海夏季风爆发早晚对广西气候的影响

应用广西1960年以来地面88个观测站日平均气温、降水量、相对温度、均风速、总云量等气象资料,以及1970-2001年ECMW F再分析资料850hPa比湿和垂直速度资料,分析南海夏季风异常早晚的广西气象要素特征。结果表明：南海夏季风偏早,广西地面气温偏低,季风爆发当候广西气候特征往多雨方向发生变化,而爆发之后气候趋于较正常状态;南海夏季风偏晚年,爆发前6候,地面气温高,在季风爆发后5候内降水量较多;南海夏季风偏早、偏晚与广西多数固定月、季时间尺度的气温、降水量的关系无明显增加线性相关。     

气象固定资产管理存在问题的探讨

通过对气象固定资产管理中存在的问题及成因分析,提出加强气象固定资产管理的一些建议。     

局域网共享虚拟传真机的实现

介绍了一种利用电话线和Modem配合传真软件建立局域网内共享的“虚拟传真机”的方法。     

中国城市固体废弃物甲烷排放研究

The greenhouse effect of methane (CH4) is only inferior to that of carbon dioxide (CO2). As an important anthropogenic emission source, the calculation of the emission amount of CH4 from waste treatment in landfills plays an important role in compiling greenhouse gases inventory and in estimating the climate change effects caused by increasing of greenhouse gases. Based on the previous work, and according to the sampling and analysis on municipal solid waste (MSW) in typical cities, the degradable organic carbon (DOC) percentile was identified in typical cities in recent years. According to the IPCC greenhouse gases inventory guideline and default method of CH4 emission from MSW landfills, and in light of MSW managing situation in different regions, the amount of CH4 emission was calculated. The results show that the amount of CH4 emission decreases geographically from east to west and it increases temporally from 1994 to 2004 in China.     

Comparison of Two Fading Filters anc Adaptively Robust Filter

Two kinds of fading filters and their principles are introduced. An adaptive robust filter is given with corresponding principle. The basic abilities of the fading filters and adaptively robust filter in controlling the influences of the kinematic model errors are analyzed. A practical example is given. The results of the fading filter and adaptively robust filter are compared and analyzed.     

A method to improve the alignment performance for GPS-IMU System

Zero velocity and zero east component of rotation rate relative to local geographic frame have been traditionally applied as measurements for fine alignment of a GPS-IMU system. The performance of the fine alignment, however, will be affected by several types of inertial sensor errors, which could cause part of the Kalman filter states to be unobservable. To overcome this problem, a new method that utilizes the total outputs of the gyro triad and the accelerometer triad as part of the measurements has been proposed by the authors. The initial results have confirmed the effectiveness of the method. In this paper, the observability for both traditional and new alignment methods will be first reviewed. The results from computer simulations will then be presented to compare the traditional and the new alignment methods for the purpose of evaluating the performance of the proposed new method. Data acquired from real inertial sensors will also be applied to assess the traditional and new alignment methods by analyzing their innovation sequences from the Klaman filter. Based on a paper presented at the 18th International Technical Meeting of the Satellite Division of the Institute of Navigation, Long Beach, California, September 2005.