Quartz and feldspar zoning in the eastern Erzgebirge volcano-plutonic complex (Germany, Czech Republic): evidence of multiple magma mixing

Zoned quartz and feldspar phenocrysts of the Upper Carboniferous eastern Erzgebirge volcano-plutonic complex were studied by cathodoluminescence and minor and trace element profiling. The results verify the suitability of quartz and feldspar phenocrysts as recorders of differentiation trends, magma mixing and recharge events, and suggest that much heterogeneity in plutonic systems may be overlooked on a whole-rock scale. Multiple resorption surfaces and zones, element concentration steps in zoned quartz (Ti) and feldspar phenocrysts (anorthite content, Ba, Sr), and plagioclase-mantled K-feldspars etc. indicate mixing of silicic magma with a more mafic magma for several magmatic phases of the eastern Erzgebirge volcano-plutonic complex. Generally, feldspar appears to be sensitive to the physicochemical changes of the melt, whereas quartz phenocrysts are more stable and can survive a longer period of evolution and final effusion of silicic magmas. The regional distribution of mixing-compatible textures suggests that magma mingling and mixing was a major process in the evolution of these late-Variscan granites and associated volcanic rocks.

Quartz phenocrysts from 14 magmatic phases of the eastern Erzgebirge volcano-plutonic complex provide information on the relative timing of different mixing processes, storage and recharge, allowing a model for the distribution of magma reservoirs in space and time. At least two levels of magma storage are envisioned: deep reservoirs between 24 and 17 km (the crystallisation level of quartz phenocrysts) and subvolcanic reservoirs between 13 and 6 km. Deflation of the shallow reservoirs during the extrusion of the Teplice rhyolites triggered the formation of the Altenberg-Teplice caldera above the eastern Erzgebirge volcano-plutonic complex. The deep magma reservoir of the Teplice rhyolite also has a genetic relationship to the younger mineralised A-type granites, as indicated by quartz phenocryst populations. The pre-caldera biotite granites and the rhyodacitic Schönfeld volcanic rocks represent temporally and spatially separate magma sources. However, the deep magma reservoir of both is assumed to have been at a depth of 24–17 km. The drastic chemical contrast between the pre-caldera Schönfeld (Westfalian B–C) and the syn-caldera Teplice (Westfalian C–D) volcanic rocks is related to the change from late-orogenic geotectonic environment to post-orogenic faulting, and is considered an important chronostratigraphic marker.     

鄂尔多斯盆地东南缘延长组地层热演化史研究： 镜质体反射率和磷灰石裂变径迹证据

对鄂尔多斯盆地东南缘韩城和洛南地区的晚三叠世延长组地层的6件样品进行了煤线和碳质泥岩的镜质组反射率测定,同时测定了同组地层6件砂岩样品的磷灰石裂变径迹.结果表明鄂尔多斯盆地东南缘晚三叠世延长组热演化程度较高,韩城地区R0值在0.65％～0.78％之间.洛南地区由于受秦岭中生代陆内造山作用的影响,三叠系延长组Ro值高达2.67％～3.71％.实际测得的裂变径迹年龄,随深度增加裂变径迹年龄减小,根据裂变径迹年龄及长度恢复出每个样品所经历的热历史.研究结果表明鄂尔多斯盆地东南缘中生代晚期存在一期约100 Ma的重要构造热事件,东南缘韩城地区与洛南地区属于不同的热演化史类型,韩城地区属于埋藏增温型,而洛南地区属于受构造岩浆活动控制类型.这一认识与野外地质证据一致.     

The Constitute of Thick Tight Sandstone Belt and the Main Controlling Factors of Effective Reservoir

<正>1 Introduction The western 3D region of the Sulige gas field is located in the Yi-shan slope north of northern Su47 and south of Su48 medium sand belt of the Ordos Basin,the area of it is about 431 km2.The average thickness of He8 is 69.1m,the thickness of it is 83.9m;The effective sand thickness is14.4 m,the thickness of it is 21.5m.     

Tectonic Units Division of Crystalline Basement in the Tarim Basin, NW China

<正>By the geological investigation for crystalline basement outcrops in Northeast and northwest margins of Tarim Basin,we provide essential constrains interpreting the structure,petrology and age of the pre-Sinian basement.On the basis of interpretation for aeromagnetic anomalies,     

含粗粒金矿样品采集加工与分析研究进展

含粗粒金矿,由于粗粒金的存在使其样品的采集、加工和分析极具挑战性,如何获得具有代表性和均匀性的化学分析样品,并提供准确的分析结果,长期以来一直是该类金矿资源勘查评价急待解决的技术难题。本文对近年来国内外含粗粒金矿样品的采集、加工和分析方法等3方面开展的研究工作及主要成果进行归纳分析,认为:1含粗粒金矿样品的采集是确保样品代表性的首要环节,含粗粒金矿样品分析结果的潜在误差有80%来源于样品采集,因此研究经济、有效的样品采集方法至关重要。2含粗粒金矿样品的加工主要从提高自然金的粉碎度,改进加工流程,选择样品加工设备等方面进行,但查明金的粒度分布及伴生矿物是拟定样品加工流程的关键。3含粗粒金矿样品的分析方法有常规的化学分析方法、批量浸金法和人工重砂加权平均法,相对于复杂的加工流程研究,后者有望成为此类样品经济有效的分析方法。本文指出,含粗粒金矿资源评价质量的误差来源于地质、采样、加工、分析等诸多方面,总体而言应最小化所有阶段误差,应特别重视样品采集方法的研究,确保采集样品的代表性是提高该类金矿资源评价质量的前提。     

Meso‐Cenozoic Tectonothermal History of Permian Strata,Southwestern Weibei Uplift: Insights from Thermochronology and Geothermometry

This study provides an integrated interpretation for the Mesozoic-Cenozoic tectonothermal evolutionary history of the Permian strata in the Qishan area of the southwestern Weibei Uplift, Ordos Basin. Apatite fission-track and apatite/zircon(U-Th)/He thermochronometry, bitumen reflectance, thermal conductivity of rocks, paleotemperature recovery, and basin modeling were used to restore the Meso-Cenozoic tectonothermal history of the Permian Strata. The Triassic AFT data have a pooled age of ～180±7 Ma with one age peak and P(χ2)=86%. The average value of corrected apatite(U-Th)/He age of two Permian sandstones is ～168±4 Ma and a zircon(U-Th)/He age from the Cambrian strata is ～231±14 Ma. Bitumen reflectance and maximum paleotemperature of two Ordovician mudstones are 1.81%, 1.57% and ～210°C, ～196°C respectively. After undergoing a rapid subsidence and increasing temperature in Triassic influenced by intrusive rocks in some areas, the Permian strata experienced four cooling-uplift stages after the time when the maximum paleotemperature reached in late Jurassic:(1) A cooling stage(～163 Ma to ～140 Ma) with temperatures ranging from ～132°C to ～53°C and a cooling rate of ～3°C/Ma, an erosion thickness of ～1900 m and an uplift rate of ～82 m/Ma;(2) A cooling stage(～140 Ma to ～52 Ma) with temperatures ranging from ～53°C to ～47°C and a cooling rate less than ～0.1°C/Ma, an erosion thickness of ～300 m and an uplift rate of ～3 m/Ma;(3)(～52 Ma to ～8 Ma) with ～47°C to ～43°C and ～0.1°C/Ma, an erosion thickness of ～500 m and an uplift rate of ～11 m/Ma;(3)(～8 Ma to present) with ～43°C to ～20°C and ～3°C/Ma, an erosion thickness of ～650 m and an uplift rate of ～81 m/Ma. The tectonothermal evolutionary history of the Qishan area in Triassic was influenced by the interaction of the Qinling Orogeny and the Weibei Uplift, and the south Qishan area had the earliest uplift-cooling time compared to other parts within the Weibei Uplift. The early Eocene at ～52 Ma and the late Miocene at ～8 Ma, as two significant turning points after which both the rate of uplift and the rate of temperature changed rapidly, were two key time for the uplift-cooling history of the Permian strata in the Qishan area of the southwestern Weibei Uplift, Ordos Basin.     

加标回收在水质分析中的应用及回收率计算方法

阐述了水质分析中加标回收分析的方法步骤、条件控制及计算方法。当加标体积影响试样在加标水样中的浓度时,直接使用回收率理论计算公式的计算值,均较其真实的回收率偏低,且其偏低值随加标体积的增加而增大。根据加标回收分析的定义,分别以加标前后被测组分质量浓度(mg/L)的变化或含量(μg)的变化为依据,导出两个计算加标回收率的实用公式。采用该公式,加标体积可以不受严格控制,其计算结果与真实的回收率一致,适用于日常水质分析工作。     

鄂尔多斯盆地延长组长7段凝灰岩锆石U-Pb年龄、Hf同位素组成特征及其地质意义

鄂尔多斯盆地延长组长7优质烃源层中广泛分布了薄层和纹层状凝灰岩,凝灰岩中锆石U-Pb同位素年代学研究表明,长7段凝灰岩结晶年龄为234Ma左右。对比勉略缝合带、南秦岭的花岗岩的年龄,三叠系延长组凝灰岩应该形成于俯冲阶段。锆石的Hf同位素分析表明延长组长7段凝灰岩主要来自地壳岩石部分熔融,并且有一定的地幔物质加入。Hf同位素二阶段模式年龄大部分集中在1.1~1.3Ga,其中以1.2Ga为主峰,表明延长组凝灰岩主要来自元古代增生的地壳物质,在物质组成和时代上可能类似于南秦岭基底中的耀岭河群基性火山岩和郧西群酸性的混合。     

铜镍硫化物铼-锇标准物质定值的溯源性讨论及总不确定度评估

对按国家一级标准物质技术规范研制的铜镍硫化物Re-Os标准物质定值的溯源性及其总不确定度进行讨论与评估。铜镍硫化物标准物质样品采用Carius管溶解,高精度的TRITON同位素质谱仪、MAT-262热电离质谱仪、四极杆等离子体质谱仪、多接收器等离子体质谱仪和高分辨四极杆等离子体质谱仪测量Re、Os含量和Os同位素比值,其中Re-Os含量可以溯源至基准物质,而187Os/188Os同位素比值可以溯源至国际纯粹与应用化学联合会(IUPAC)。在定值数据误差计算时,采用国际通用的ISOPLOT软件利用加权的方法对数据进行处理;在合成总不确定度时,考虑了物质的均匀性和稳定性,同时考虑了稀释剂标定和同位素丰度以及称量误差等影响测定因素的不确定度。标准值的不确定度由三部分组成:第一部分是通过所有参与定值数据,采用ISOPLOT软件,利用加权的方法对数据进行计算处理得到的不确定度;第二部分是物质的均匀性和稳定性的不确定度;第三部分是影响测定其他因素的不确定度。     

南边界强迫的非线性临界层与副高的形成、维持和振荡

用非线性准地转正压涡度方程模式，在南边界取定常强迫波，采用４种方案模拟了非线性临界层及其上激发的Ｋｅｌｖｉｎ猫眼，以确定热带的定常强迫对副高的形成、维持和振荡的影响。结果表明，南边界定常强迫仍在非线性临界层内激发行星尺度的准定常反气旋的Ｋｅｌｖｉｎ猫眼流场，猫眼的移动、强度和形状变化与夏季副高比较相似．而北边界定常强迫所得结果与夏季副高差异较大。因此，南边界所激发的非线性临界层上的Ｋｅｌｖｉｎ猫眼可能是夏季副高形成、维持和振荡的一种更为重要的新物理机制。文中还提出准定常行星波穿越副热带的非线性临界层的物理机制。