钛(Ⅳ)催化极谱的研究——应用于天然水中痕量钛的测定

(一)仪器 SJP-1A型示波极谱仪(浙江丽水无线电厂),阳极为饱和甘汞电极.毛细管特性:在蒸馏水中m=0.63毫克/秒,t=7.3秒,汞柱高度52厘米.(二)试剂 全部试剂均采用二级试剂,溶液均用重蒸馏水配制.     

Photoinduced toxicity single and binary mixtures of four polycyclic aromatic hydrocarbons to the marine diatom Skeletonema costatum

Diatom Skeletonema costatum Cleve is one of the main predominant phytoplankton species in the Changjiang Estuary in China. In order to provide some basic information for future assessment of the potential risk on phytoplankton communities in this estuary caused by polycyclic aromatic hydrocarbons(PAHs), this alga was selected as a representative to investigate the photoinduced toxicity of PAHs, in single and mixture. Four PAHs including three-ring phenanthrene and anthracene, four-ring fluoranthene and pyrene were tested in the laboratory. The single toxicity of each PAH on this microalga was compared with and without the simulated solar UV radiation. The results showed that this microalga was sensitive to PAH's photoinduced toxicity. Ratios of the 72 h median effect concentration obtained for fluorescent and UV light tests were about 8.4 for phenanthrene, 13.0 for anthracene, 6.5 for fluoranthene, and 5.7 for pyrene, indicating that UV light enhanced the PAH toxicity to this alga significantly. Under the fluorescent radiation (lacking UV), the dose-response curves based on chemical concentrations revealed that the order of toxic strength was fluoranthene greater than pyrene greater than anthracene greater than phenanthrene; while under the UV radiation (476 μW/cm2 for UVA, 6.5 μW/cm2 for UVB) it became fluoranthene approximately equaling anthracene greater than pyrene greater than phenanthrene, indicating that the UV light also changed its relative toxicity to this alga. The photoinduced toxicity of PAHs to the marine diatom S. costatum might be a synergistic effect of photosensitization reactions (e.g., generation of single-state oxygen) and photomodification (photooxidation and/or photolysis).The combined effects of six binary mixtures on the marine diatom S. costatum were investigated using the additive-index method. Four binary-mixtures (phenanthrene plus anthracene; phenanthrene plus pyrene; anthracene plus fluoranthene; anthracene plus pyrene) were found to be synergistic joint action mode, while two binary-mixtures (phenanthrene plus fluoranthene; fluoranthene plus pyrene) displayed antagonist, revealing a complex pattern of possible interactions. The combined action mode of PAHs might be related to various factors such as the mixture compounds, mixture ratios and test conditions, etc.     

罗氏沼虾育苗用水中Mg2+与Ca2+含量及Mg2+/Ca2+对出苗率的影响

１９９１年３－６月和１９９２年３－６月在南汇县东海水产养殖公司对罗氏沼虾育苗用水调配原则与不同基础水的调配方法进行试验研究。结果表明，育苗用水中Ｍｇ＾２＋与Ｃａ＾２＋含量及Ｍｇ＾２＋／Ｃａ＾２＋必须达到一定的范围，这是调配的基本原则。以鱼塘水作基础水时，需添加６种化学药品，其中Ｍｇ＾２＋与Ｃａ＾２＋含量可适范围分别为３００．０－４４０．０ｍｇ／Ｌ与１７０．０－２４４．０ｍｇ／Ｌ，Ｍｇ＾２＋／Ｃａ＾     

The second order spectrum of two-dimensional random waves

Ｔｈｅｓｅｃｏｎｄｏｒｄｅｒｓｐｅｃｔｒｕｍｏｆｔｗｏ－ｄｉｍｅｎｓｉｏｎａｌｒａｎｄｏｍｗａｖｅｓ￥ＤｉｎｇＰｉｎｇｘｉｎｇ；ＳｕｎＦｕａｎｄＹｕＺｈｏｕｗｅｎ（ＲｅｃｅｉｖｅｄＪａｎｕａｒｙ１５，１９９３；ａｃｃｅｐｔｅｄＭａｙ３１，１９９３）Ａ...     

全数字十二相稳压稳流微机控制系统

提出用于十二相可控整流器的８０９８单片机控制系统的电路原理和软件策略。包括自适应控制算法和触发相序计算在内的多种操作全部用软件实现．与通常的方法相比，此系统的成本更低，动态性能和静态性能更好。     

Full-range nonlinear analysis of fatigue behaviors of reinforced concrete structures by finite element method

Ｆｕｌｌ－ｒａｎｇｅｎｏｎｌｉｎｅａｒａｎａｌｙｓｉｓｏｆｆａｔｉｇｕｅｂｅｈａｖｉｏｒｓｏｆｒｅｉｎｆｏｒｃｅｄｃｏｎｃｒｅｔｅｓｔｒｕｃｔｕｒｅｓｂｙｆｉｎｉｔｅｅｌｅｍｅｎｔｍｅｔｈｏｄ￥ＳｏｎｇＹｕｐｕ；ＺｈａｏＳｈｕｎｂｏ；ＷａｎｇＲｕｉｍ...     

海底管道开沟机械的技术经济性能评定与选型

本文在对水下管道开沟机械的需求市场、实际应用和研制开发动向作深入调研的基础上，选择水下管道开沟机械特有的技术先进性、适用性、安全可靠性以及经济性评价指标，构造评价模型，对水下管道施工作业中广为应用的水力冲射开沟机械、海底管道犁、机械开沟机和土壤液化法埋管设备及其机型的技术经济性能作了较为详尽地分析对比及综合评价。在此基础上，笔者提出了水下管道开沟机械的一般选型原则和对我国海底管道开沟机械研究开发工     

海藻糖类的气相色谱分析 Ⅱ.红藻及红藻多糖中D-半乳糖和3, 6-内醚半乳糖的测定

红藻中的糖类主要以多糖形式存在(琼胶、卡拉胶等)，其中主要的单糖组分是D-半乳糖和3, 6-内醚半乳糖，除此之外还含有少晕的木糖、葡萄糖及甘露糖等成分。由于各单糖的相互干扰，难以用比色等着通化学分析方法对每一种单糖准确地定性定量。作者曾研究过褐藻中单糖的气相色谱测定法, 但该法不能测定3, 6-内醚半乳糖，囚为这种内醚糖对酸水解不稳定。据Dutton和Nozawa等人报道, 将多糖经甲醇分解后进行气相色谱分析，结果令人满意。本文用琼胶(Difco bacto-agar)作代表，研究探讨了红藻胶甲醇-HCI分解的条件，确定了红藻胶中D-半乳糖和3, 6-内醚半乳糖的气相色谱分析方法，并将其应用于红藻中D-半乳糖和3, 6-内醚半乳糖的分析。     

鱼类生长激素的体内代谢、分泌调控和作用机制研究的进展

主要对１９８３－１９９６年间关于鱼类生长激素的体内代谢、分泌调控和作用机制的研究进展予以综合评述。通过鱼类划性放射免疫测定法的建立和体风代谢动力学研究，证实，外源生长激素在鱼体内不会产生积累。鱼类生长激素的分泌调控受下丘脑分泌的生长激素释放因子（ＧＨＲＦ）和释放抑制因子（ＳＲＩＦ）的双重；促性腺激素释放激素（ＧｎＲＨ）、雌二醇（Ｅ２）、促甲状腺素释放激素（ＴＲＨ）和神经肽（ＮＹＰ）对鱼类生长激素的     

LZY1—1型光电浊度仪

本文介绍了LZY_(1-1)型光电浊度仪的设计原理,标定方法及使用结果,该仪器用经典法校准后,能快速测量大批量样品的悬浮物含量。