树脂固定化海洋脂肪酶ADM47601的研究

以海洋脂肪酶ADM47601为研究对象,以树脂为载体,进行了固定化酶的研究。筛选了21种树脂,确定D316型阴离子交换树脂为载体。通过正交试验得到了固定化的最佳条件,每克载体加脂肪酶10 000 U,pH7.5,25℃,150 r/min,固定化时间3 h,固定化酶活力回收率可达65.53%±1.06%。固定化脂肪酶最适作用pH为7.5,在pH6.0~9.0的范围内能够保持85%的活力。最适作用温度40℃,在50℃下贮存1 h后依然保持66%的活力。25℃保存半衰期为55 d,操作8次仍然能维持60%以上的活性,且在多种有机试剂中能够稳定的保持活性。固定化脂肪酶Km和Vmax值分别为4.86×10~(–5) mol/L和1.31×10~(–5) mol/(L·min),对底物亲和性较好。     

中国及其邻区地震深度的特征

系统地研究了中国及其邻区地震深度的一些时空变化特征后发现：５１％的地震发生在０－１９ｋｍ间，１０、１５、２０ｋｍ为几个地震多发层位；大陆地震的深度小于周邻地区地震的深度；大陆西部地震的深度大于东部地震的深度，这与大陆地壳西厚东薄的结果相吻合；中俄朝交界区及日本海、兴都库什－帕米尔、琉球群岛、缅印交界区和台湾地区地震的深度大，这与有关板块间的相互碰撞、挤压或俯冲等运动有关；兴都库什－帕米尔地区的地震     

Durability Characterization of Marls from the Region of Dalmatia,Croatia

Durability is one of the most important engineering properties of weak and clay-bearing rocks. Weathering can induce a rapid change in rock material from initial properties to soil-like properties. The sensitivity of a rock type against weatherability is usually described by a durability parameter, such as the slake durability index. However, marl resistance is not detected satisfactorily by the durability indices by using slake durability test as suggested by ISRM for two wetting–drying cycles. The results of this study are obtained from samples of compact or laminated eocene marls from region of Dalmatia, Croatia. The samples were subjected to 4 cycles of slake durability, point load tests, determination of dry density, determination of carbonate content and absorption of water. The scatter of data suggests that strength probably has no influence on the durability of marls. On the other hand a separate group of marl samples have a second-cycle slake durability index higher than approximately 85%, and the durability of these samples is classified as “medium-high” to “high”, although the visual inspection of samples after testing, suggests that they should have “medium” to “low” durability classification. According to obtained results these samples of marl fulfil the criterions for the durability classification: a carbonate content lower than approximately 65%, a dry density lower than 2.4 Mg/m³, and values of water absorption higher than 5%.     

辽宁本溪早石炭世植物化石

华北与东北南部地区缺失晚奥陶世至中石炭世早期地层(个别地点除外),这一论点长期以来已被中外地质学家所公认。本溪组自1926年创名以来,一直被认为属于中石炭世晚期(莫斯科期)。50年代中期,张文堂提出的论断,因无生物化石佐证,迄今未得到承认。80年代以来,吴秀元、赵修祜和刘发先后指出本溪田师付本溪组下部产纳缨尔期(或中石炭世早期)蜓和腕足类化石。 本文描述了辽宁本溪本溪组下部G层铝土矿顶板黑色页岩中所产植物化石7属12种,认为其时代为早石炭世晚期(维宪期—纳缪尔A期)。     

西北天山莱历斯高尔岩体年代学、地球化学及其成因

西北天山莱历斯高尔岩体主要由花岗闪长斑岩和二长花岗斑岩组成,二者具有相似的地球化学特征,可能为同源岩浆分异演化的产物。锆石SHRIMP U-Pb年龄显示岩体形成于晚泥盆世(374±4 Ma)。莱历斯高尔岩体具有较高的SiO2(67.75% ～74.71%)含量和K2O/Na2O(1.24～2.20)比值,属于高钾钙碱性系列。稀土元素配分曲线为轻稀土富集型(La/Yb)N(5.25～10.57),具有中等—弱的Eu负异常δEu(0.55～0.92)。微量元素特征显示富集大离子亲石元素(LILE),而亏损高场强元素(HFSE),具有较低的Sr(122×10-6～356×10-6)含量、较高的Y(17.19×10-6～21.82×10-6)和Yb(1.78×10-6～2.57×10-6)含量。岩体的Sr-Nd同位素特征为ISr=0.707 867～0.709 654,εNd(t)=-2.79～-1.46。铅同位素特征为206Pb/204 Pb=18.423～19.915,207 Pb/204Pb=15.576～15.685,208 Pb/204Pb=38.344～39.305。元素和同位素地球化学特征表明,莱历斯高尔岩体岩浆源区主要为中元古代下地壳的部分熔融,并有部分地幔物质的加入。岩体形成于晚泥盆世准噶尔洋向伊犁—中天山微板块陡角度俯冲的大陆弧构造环境。     

X射线管辐射谱线分析

经Ni滤波片过滤的CuKa射线，并非为真正的单色X射线，其中含部分白色X射线和非CuKa特征谱线。用石英分析晶体（101）衍射面网将混入CuKa射线中的各种波长的谱线分离开，并测定其波长的范围，确定在CuKa射线中含有铁、镍、钴、铬四种元素的K系列谱线和钨的L系列谱线。发现在X射线粉末图谱中用CuKa（或Kβ）无法解释的弱衍射线却是由铁、镍等元素的特征谱线混入引起的。     

树轮氢氧同位素方法在环境变迁研究中的应用

树轮氢氧同位素方法是过去环境气候变化研究领域内的主要技术手段之一，因其时间分辨率高，反映环境参数多，准确定量的优点，近年日益受到重视。     

高分四号静止轨道卫星高精度在轨几何定标

高分四号是世界上第一颗静止轨道高分辨率光学遥感卫星,高精度的几何定标是确保其成像几何质量的关键。本文分析了静止轨道卫星成像几何误差源及成像区域特点,提出了其严格几何成像模型;并在此基础上提出了静止轨道卫星面阵传感器在轨几何定标模型与定标参数估计方案。本文利用Landsat 8数字正射影像与GDEM2数字高程模型对高分四号卫星进行在轨几何定标,结果表明,通过严格的几何定标,可见光近红外传感器与中红外传感器的内部畸变在沿轨与垂轨方向上均稳定优于1个像素,通过统计分析可知,高分四号静止轨道卫星影像的绝对定位精度会受到成像时间与成像角度的影响而存在显著的波动。     

Effect of fault jogs on frictional behavior: An experimental study

Studying the effect of geometrically irregular bodies on the mechanical behavior of fault activity is of significance in understanding the seismic activity along a fault zone. By using rock mechanics ex- periment with medium-scale samples, we have studied the effect of fault jogs, the most common irregularity along fault zones, on frictional behavior. The research indicates that extensional fault jog can be easily fractured because of its low strength and the fractured jog has no obvious resistance to fault sliding, and the micro-fractures occurring in the jog are indicative of stick-slip along the faults. The fault zone containing extensional jogs is characterized by velocity weakening and can be described by rate and state friction law. Compressional fault jog makes fault sliding more difficult because of its high fracturing strength, but the micro-fractures occurring in the tensile areas around fault ends at higher stress level can provide necessary condition for occurrence of stick-slip along the faults before the jog is fractured and thus act as precursors of fault instability. Compression jog can be taken as a stable indicator of fault segmentation until the jog is completely fractured and two faults are linked.     

鄱阳湖流域干旱气候特征研究

本文利用鄱阳湖流域127个站点1960-2007年逐日降水和温度资料,选用Z指数对鄱阳湖流域的气象干旱进行分析,并将干旱分为偏旱、大旱和特旱三个等级.研究结果表明鄱阳湖流域干旱基本呈现出南少北多、南强北弱的空间分布形式.鄱阳湖流域7-12月发生的干旱以偏旱为主,大旱和特旱主要出现在1-6月.线性趋势变化分析表明,2000年以来干旱范围和干旱强度均呈现出增加的趋势,其中,2003、2004和2007年的干旱较为严重.2003年大部分月份偏旱范围广、强度大,全年大旱和特旱出现的范围均较小,但3-4月和6-7月的大旱和特旱强度较大;2004年大部分月份偏旱范围和强度均相对较小,但在3月和6月出现范围较大且强度较强的大旱和特旱;2007年干旱分布更为极端,仅在7、10和11月出现范围较广或强度较大的偏旱,而在5月集中出现面积超过80%的大旱和特旱.