Characterisation of brown coal humic acids and modified humic acids using pyrolysis gcms and other techniques

It has been proposed that Victorian brown coal can be considered as a two-component structure — a lignocellulosic “host”, containing various amounts of weakly bound or entrapped “guest” material together with very small amounts of inorganic and/or mineral matter. The latter predominantly consists of wax esters and/or terpenoid material. In this paper we describe attempts to gain structural information regarding the more complex, “host” component of the coal. Our initial model compound has been humic acid that can be readily obtained from the coal by alkaline extraction. It has been found that “pure” humic acid, free from material associated with the “guest” components of the coal, can be obtained by a highly selective, low-yielding alkaline extraction. This humic acid has been studied by nmr spectroscopy and pyrolysis gas chromatography-mass spectroscopy (py-gc/ms). The products arising from py-gc/ms have been compared with those obtained from similar pyrolysis of whole coals. Alkylation of humic acids using alkyl halides in the presence of base has been successfully carried out and reactivity of the resulting materials compared with those of the parent coal and humic acid.     

MD－50型钻机液压系统的设计

介绍了ＭＤ－５０型钻机液压系统的设计原理和主要液压元件的选择依据，并通过对设计和实践的总结，谈了作者在全液压钻机液压系统设计中的一些体会。     

三种锰硅酸盐矿物的鉴别及其研究意义

蜡硅锰矿，粒硅锰矿，鉴别，研究意义     

泡沫泥浆钻进工艺及护壁堵漏机理研究

介绍了所研制的ＤＦ－１型泡沫剂组分及性能；对泡沫泥浆钻进的配方进行了研究，得出的最优配方应用于现场，取得了较好的效果，并对泡沫泥浆的护壁机理进行了研究。     

桩长及水泥掺入量对柔性桩承载力等的影响

采用弹性无限半空间体内的Mindlin应力解和分层总和法，计算分析了柔性桩的荷载传递规律，较详细地讨论了桩长、固化剂（水泥）掺入量对柔性桩复合地基承载力、变形的影响。计算值与实测值比较吻合。     

水库诱发地震的地震动特征

利用新丰江、美国奥洛维尔和蒙蒂赛洛水库地震极近场地面运动资料，研究了水库诱发地震的地震动峰值加速度衰减。结果表明，水库地震的峰值加速度高，衰减快。利用国内水库地震资料研究了水库地震烈度。水库地震烈度与同级天然地震烈度相比，一般是烈度高，衰减慢。水库地震的地震动反应谱频率高，地震动持续时间短     

中强震与江苏新沂地震台地电阻率异常的关系研究

运用速率法、滑动富氏法对江苏省新沂地震台1990年至1999年地电阻率观测资料进行了分析，研究了电阻率异常与江苏省及其邻近地区的中强震的关系。结果表明．从1994年到1997年之间发生的中强震，新沂地震台地电阻率3个测向有不同程度的异常与之对应。研究结果表明．资料异常呈现出的各向异性和其对应性与地球自转加速年份、孕震期的应力状态、震区构造、介质结栖有关。     

VICARIOUS RADIOMETRIC CALIBRATION OF SATELLITE FY-ID SENSORS AT VISIBLE AND NEAR INFRARED CHANNELS

For the problem of in-flight test site radiometric calibration for the FY-1D Meteorological Satellite onboard sensor's visible and near infrared channels,this paper described the calibration method,satellite-ground synchronous observation data acquired at China Dunhuang Calibration Test Site,parameter derivation and radiative transfer computation during the calibration,and the calibration result analysis.At FY-1D seven channels (with central wavelength at Channels 1:630 nm,2:865 nm;6:1610 nm;7:455 nm,8:505 nm;9:555 nm;10:932 nm),calibration coefficients obtained during the ground site calibration were compared with that respectively of prelaunch calibration.It is demonstrated that results of FY-1D onboard two sensors' (A and B) at channels 1,2,6 and 10 were close to pre-calibration,and the absolute difference of Gobi desert reflectance computed using test site and pre-launch calibration coefficients was no more than 2%. At other channels,large pre-launch calibration errors resulted in a poor consistency between the test site and pre-launch calibration.The errors can be corrected by the test site calibration results. Based on a rough estimation,the overall error of the calibration was about 6%. The paper also presented the in-flight vicarious calibration at the visible and near infrared channels of FY-1C sensor A which was launched in 1999 and has been put into operational mode since 2002.The results exhibit that FY-1C sensor's response has 23% attenuation at Channels 7 and 8,while only minor degradation at the other channels was found. During the mission,calibrations were also conducted at NOAA-17's Channels 1 and 2 (1:430-830 nm,2:500-1072 nm).A very good consistency has been achieved between the test site and pre-launched calibration results.     

多尺度分解在地震信号处理中的应用

利用小波分析中的多尺度分解及信号消噪技术，对记录不清、信噪比小、震相无法辨认的地震信号进行处理。结果表明：多尺度分解在弱震信号提取和弱震相的识别等方面有很好的效果。