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911.
Improved Platinum-Group Element Extraction by NiS Fire Assay from Chromitite Ore Samples Using a Flux Containing Sodium Metaphosphate 总被引:1,自引:0,他引:1
Many chromite-rich rocks contain relatively high concentrations of the platinum-group elements (PGE). In many cases, the phases carrying PGE occur as either platinum-group minerals (PGM) or as base metal sulfides in solid solution in sulfides. In some cases, such as the UG-2 unit of the Bushveld Complex, the PGM are occluded inside chromite grains. Chromites are notably difficult to dissolve in most fluxes and if the chromite contains some PGM the possibility exists that not all the PGE will be recovered during fusion. In this work, shortcomings in published methods of analysis based on the nickel sulfide fire assay procedure were investigated and a new procedure developed based on the addition of sodium metaphosphate to the fusion mixture. Optimum composition of the fusion mixture was found to be 10 g sodium metaphosphate and 9 g silica to 10 g sample, 15 g sodium carbonate, 30 g lithium tetraborate, 7.5 g nickel and 4.5 g sulfur to achieve complete dissolution of chromite grains. The new flux mixture was evaluated by the analysis of reference material CHR-Pt+ (which is known to contain PGM inside chromite grains) and no undissolved chromite grains were found in the glassy slag. Analysis of the nickel sulfide beads from this fire assay using neutron activation analysis showed similar results for Rh and Ru when compared with published conventional true (or accepted) values, while Au, Ir, Os, Pd and Pt values determined here were 10 to 30% higher than the corresponding published conventional true values. It was concluded that the addition of sodium metaphosphate improved chromite dissolution in the flux and appears to improve PGE recovery. 相似文献
912.
Geostatistical characterization of soil moisture and chloride distribution in deep vadose profiles of the Badain Jaran Desert,Northwestern China 总被引:1,自引:0,他引:1
Feng?PanEmail author Jinzhu?MaEmail author Xangyang?Zhou W.?Mike Edmunds Gohn?B.?Gates 《Environmental Earth Sciences》2013,70(3):977-991
Geostatistical analysis of soil moisture and ion accumulation can provide a deep understanding of aspects of a region’s hydrology such as recharge rates and flow paths. By combining this approach with detrended canonical correspondence analysis, the present study investigated the vertical and spatial variation of soil moisture and chloride (Cl?) in vadose profiles of megadunes near lakes in the southeastern Badain Jaran Desert, northwestern China. Soil moisture varied vertically within the dune profiles following exponential, logarithmic, or log-normal distributions at different sites as a result of regulation by different local controls. The main local controls for Cl? concentration were slope and orientation of the dune. Cl? was not affected by local controls at depths >5 m. Sills of spatial variation in soil moisture and Cl? in the variogram analysis were highly sensitive to local controls in the top 4 m of the profiles, and the values were three times those at depths >4 m. The lag for soil moisture was insensitive to local controls, and was 50–60 m in the top 4 m of the profiles and 20 m in deeper layers, whereas the lag for Cl? was about 20 m at all depths. The results demonstrate that understanding recharge rates using factors such as Cl? accumulation requires a careful survey to ensure that the local controls that regulate these factors are adequately accounted for. 相似文献
913.
In this comment we argue that the premise on which the peat mound model developed by Armstrong (Earth Surface Process and Landforms, 1995, 20 , 473–477) is based, that hydraulic conductivity shows an exponential decline with depth in bog peats, is unsound. Empirical evidence in the literature for such an exponential decline is less sound than Armstrong suggests. In addition, Armstrong's suggestion that the hypothesis of Baird and Gaffney (Earth Surface Processes and Landforms, 1995, 20 , 561–566) supports an exponential decline is shown to be erroneous. 相似文献
914.
This paper records sedimentary data which indicate that at least part of the Wilsons River floodplain, on the margins of the subtropical rainforest known as the 'Big Scrub', has a long and certainly pre-European history of relative treelessness. Despite a general presumption that this lowland subtropical region was completely forested prior to European settlement, recent historical research has indicated that certain areas were naturally open. While the historical information is clear, the data reported here-a fossil pollen record and one radiocarbon date- reinforces that information for one type of locality, providing an initial indication of time depth. 相似文献
915.
Conservative tracers are necessary to obtain groundwater transport velocities at the field scale. Deuterated water is an
effective tracer for this purpose due to its similarity to water, chemical stability, non-reactivity, ease of handling and
sampling, relatively neutral buoyancy, and reasonable price. Reliable detection limits of 0.1 mg deuterium/L may be obtained
in field tests. A field example is presented in which deuterated water, bromide, and pentafluorobenzoic acid are used as groundwater
tracers. Deuterated water appeared to be transported conservatively, producing almost identical breakthrough curves as that
of other soluble tracers.
Electronic Publication 相似文献
916.
Jean-Franois Pastre Agns Gauthier Sbastien Nomade Paul Orth Ana Andrieu Franck Goupille Herv Guillou Stphane Kunesch Stphane Scaillet Paul Randall Renne 《Comptes Rendus Geoscience》2007,339(16):987-997
The Alleret maar (Massif Central, France) provides a long lacustrine sequence (40.6 m) attributed to the early Middle Pleistocene. Sediment, pollen and diatoms analysis of its upper part (AL2 core, 14.6 m) indicates two temperate phases marked by high lake levels, forest development and vegetation expansion. They are separated by a cold period during which lake level drops, coarse sediment input increases and steppic and xerophilous plants develop. Pollen data suggests that this sequence belongs to the upper part of the Cromerian complex. These results are in agreement with the 557 ± 3 ka (±12 ka, including all errors) 40Ar/39Ar age obtained from an interbedded tephra layer emitted by the Mont-Dore/Sancy strato-volcano and establish that this sequence probably covers the MIS 15 substages. 相似文献
917.
918.
An inexpensive Pull-Up Shallow Water Seismometer (PUSS) has been designed and built to conduct long range seismic refraction experiments in the North Sea and the continental shelf around Britain, with the particular goal of studying the crustal and lithospheric structure under the epeirogenic basin of the North Sea. Signals from a gimbal-mounted 3-component geophone and a hydrophone are frequency modulated and mixed with clock and flutter correction signals before being recorded on a standard speed cassette tape recorder, with one hour of recording time. A 100 hour programmable timer allows the interval between the time of reset of the clock and each shot window of optional 5 or 10 min duration, to be preselected. The PUSS is launched and recovered using a pull-up technique originally developed for current meters. The replay system is also described.In May 1976 sea trials of 5 PUSSes were conducted along a 200 km refraction line in the North Sea. The encouraging performance of the equipment resulted in the decision to build a further 10 units and to proceed with a 400 km refraction line planned for the summer of 1977. 相似文献
919.
A minor generalization of the theory of random walk is used as a basis for a model of ocean current flow. The model is then applied in a computer simulation of drifter motion. The results of simulation indicate that the geometry of a coastline can have significant impact on the distribution of drifter landings. 相似文献
920.
Burghard W. Flemming 《Sedimentary Geology》2007,202(3):425-435
To this day, deterministic physical models capable of explaining the evolution of grain-size distributions in the course of transport are still lacking. For this reason, various attributes of particle frequency distributions, in particular curve shapes and textural parameters, have for many decades been investigated for potential information about transport behaviour and size-sorting processes of sediments in numerous environments. Such approaches are essentially conceptual and hence rely heavily on the validity of the assumptions on which they are based. A factor which has to date been largely ignored in this context, is the fact that different methods of grain-size analysis (e. g. sieving, laser absorption and diffraction, settling velocity measurements), when applied to the same sample material, produce variable curve shapes, and hence incongruous textural data. This is illustrated by selected examples showing the differences between sieving and settling results, conversion of settling velocities into equivalent settling diameters (psi-phi-transformations), and the influences of particle shape, particle density, and water temperature. It is demonstrated that particle-size distributions are not only method-dependent but also dependent on the adopted post-processing procedure. As a result, only frequency curves generated by the same method and subsequently processed by identical computational procedures can be meaningfully compared. Furthermore, the computation of textural parameters from bi- or multimodal size distributions produces spurious results which are unrelated to the processes leading to the mixing of different size populations frequently observed in nature. In such cases, only the decomposition of such distributions into individual populations and the spatial comparison of such populations makes any sense. Because a physical explanation for the generation of size distributions is lacking, a particular curve shape of a grain-size population has no meaning on its own. Only a systematic comparison of progressively changing curve shapes (and associated textural parameters) of sediments collected on a closely spaced grid can yield data suitable for sediment trend analysis. 相似文献