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181.
Roger H. Mitchell Malcolm Alexander Lachlan M. D. Cranswick Ian P. Swainson 《Physics and Chemistry of Minerals》2007,34(10):705-712
The cell dimensions and crystal structures of the fluoroperovskite NaMgF3 (neighborite), synthesized by solid state methods, have been determined by powder neutron diffraction and Rietveld refinement
over the temperature range 300–3.6 K using Pt metal as an internal standard for calibration of the neutron wavelength. These
data show that Pbnm NaMgF3 does not undergo any phase transitions to structures of lower symmetry with decreasing temperature. The cell dimensions and
atomic coordinates together with polyhedron volumes and distortion indices are given for Pbnm NaMgF3 at 25 K intervals from 300 to 3.6 K. Decreases in the a and c cell dimensions reach a saturation point at 50 K, whereas the b dimension becomes saturated at 150 K. The distortion of the structure of Pbnm NaMgF3 from the aristotype cubic
structure is described in terms of the tilting of the MgF6 octahedra according to the tilt scheme a
−
a
−
c
+
. With decreasing temperature the antiphase tilt (a
−) increases from 14.24° to 15.39°, whereas the in-phase tilt (c
+
) remains effectively constant at ∼10.7°. Changes in the tilt angles are insufficient to cause changes in the coordination
sphere of Na that might induce a low temperature phase transition. The structure of Pbnm NaMgF3 is also described in terms of normal mode analysis and displacements of the condensed normal modes are compared with those
of Pbnm KCaF3. 相似文献
182.
The stability of yttrium-acetate (Y-Ac) complexes in aqueous solution was determined potentiometrically at temperatures 25-175 °C (at Ps) and pressures 1-1000 bar (at 25 and 75 °C). Measurements were performed using glass H+-selective electrodes in potentiometric cells with a liquid junction. The species YAc2+ and were found to dominate yttrium aqueous speciation in experimental solutions at 25-100 °C (log [Ac−] < −1.5, pH < 5.2), whereas at 125, 150 and 175 °C introduction of into the Y-Ac speciation model was necessary. The overall stability constants βn were determined for the reaction
183.
Akizumi Ishida Kouki Kitajima Ko Hashizume Michael J. Spicuzza Alexander Zaitsev Daniel J. Schulze John W. Valley 《Geostandards and Geoanalytical Research》2023,47(3):569-578
Simultaneous analysis of carbon and nitrogen isotope ratios by SIMS was applied for the first-time to a natural diamond from the Kelsey Lake kimberlite, State Line Distinct, Colorado (UWD-1). This in situ procedure is faster, reduces sample size for analysis, and measures both isotope ratios from a single ~ 10 μm diameter pit, a critical advantage for zoned diamonds. The carbon isotope ratio (expressed as δ13CVPDB) of the bulk UWD-1 crystal, determined by the conventional combustion method in the present study, is -5.9‰ ± 0.2‰ (VPDB, 2s). Nitrogen mass fraction ([N]) and isotope ratio (expressed as δ15NAir) were determined by stepwise combustion and gas-source mass-spectrometry, resulting in 553 ± 64 μg g-1 and -6.7‰ ± 1.1‰ (Air, 2s), respectively. Secondary ions of 12C2-, 12C13C-, 12C14N-, and 12C15N- were simultaneously measured by SIMS using three Faraday cups and one electron multiplier. The spot-to-spot reproducibility of δ13C and δ15N values for the UWD-1 (178 spots on sixteen chips, 10 μm spots), were 0.3‰ and 1.6‰, respectively (2s). While 12C14N-/12C2- ratios, which are an indicator for [N], varied up to 12% among these sixteen chips, such variation did not correlate with either δ13C or δ15N values. We propose that UWD-1 is a suitable reference sample for microscale in situ analysis of δ13C and δ15N values in diamond samples. 相似文献
184.
Anna ASEEVA Oleg AVCHENKO Alexander KARABTSOV Alexander CHASHCHIN Sergey VYSOTSKIY Victoria YAKOVENKO Natalia ZARUBINA Natalia KHARITONOVA 《《地质学报》英文版》2022,96(1):111-122
Garnet megacryst with a multiphase inclusion from intraplate alkali basalts of the Shavaryn Tsaram(Tariat,Mongolia)was the object of the study.This unusual aggregate consists of porous glass,Ti-rich biotite,orthopyroxene,spinel,clinopyroxene,olivine,and ilmenite.Win TWQ 2.32 thermodynamic simulation of this system revealed a few intervals of equilibrium.Pressure and temperature adjustment reflected in the paragenetic minerals of the melt pocket.The capture of already crystallised garnet megacryst was at P=0.8-1 GPa and T=1120-1160℃.Mineral crystallisation inside the melt pocket,accompanied by external inputs,occurred at P=0.75-0.95 GPa;T=790-1120℃.Symplectite assemblage formed in the garnet megacryst due to decomposition at(P=0.55-0.7 GPa;T=850-930℃).The study of the oxygen isotope content in primary garnet and biotite of the melt pocket showed that the δ18OVSMOW values are the same and correspond to that of typical mantle xenoliths.However,the chemical and microcomponent composition of the melt pocket minerals reveals a material that differs from basalts and peridotites.Thus,it has been revealed that the multiphase inclusion in the garnet megacryst formed not only on account of the garnet’s substance,but also due to the entrapped material of the Earth’s interior. 相似文献
185.
Zhongqiang Liu Farrokh Nadim Alexander Garcia-Aristizabal Arnaud Mignan Kevin Fleming Byron Quan Luna 《Georisk: Assessment and Management of Risk for Engineered Systems and Geohazards》2015,9(2):59-74
The effective management of the risks posed by natural and man-made hazards requires all relevant threats and their interactions to be considered. This paper proposes a three-level framework for multi-risk assessment that accounts for possible hazard and risk interactions. The first level is a flow chart that guides the user in deciding whether a multi-hazard and risk approach is required. The second level is a semi-quantitative approach to explore if a more detailed, quantitative assessment is needed. The third level is a detailed quantitative multi-risk analysis based on Bayesian networks. Examples that demonstrate the application of the method are presented. 相似文献
186.
Accounting for the solar radiation in thermal regime prediction for railway subgrade in cold regions
This paper presents a comparative analysis of simulation processes of seasonal freezing-thawing of railway subgrade and permafrost degradation, with and without accounting for solar radiation. Also, the effect of sun screens to reduce the degradation of subgrade permafrost under different climatic conditions is numerically substantiated. And finally, the temperature criterion of the origination of permafrost is illustrated. 相似文献
187.
Analysis of 3.3 Ga tonalite–trondhjemite–granodiorite (TTG) series granitoids and greenstone belt assemblages from the Bundelkhand craton in central India reveal that it is a typical Archaean craton. At least two greenstone complexes can be recognized in the Bundelkhand craton, namely the (i) Central Bundelkhand (Babina, Mauranipur belts) and (ii) Southern Bundelkhand (Girar, Madaura belts). The Central Bundelkhand greenstone complex contains three tectonostratigraphic assemblages: (1) metamorphosed basic or metabasic, high-Mg rocks; (2) banded iron formations (BIFs); and (3) felsic volcanics. The first two assemblages are regarded as representing an earlier sequence, which is in tectonic contact with the felsic volcanics. However, the contact between the BIFs and mafic volcanics is also evidently tectonic. Metabasic high-Mg rocks are represented by amphibolites and tremolite-actinolite schists in the Babina greenstone belt and are comparable in composition to tholeiitic basalts-basaltic andesites and komatiites. They are very similar to the metabasic high-Mg rocks of the Mauranipur greenstone belt. Felsic volcanics occur as fine-grained schists with phenocrysts of quartz, albite, and microcline. Felsic volcanics are classified as calc-alkaline dacites, less commonly rhyolites. The chondrite-normalized rare earth element distribution pattern is poorly fractionated (LaN/LuN = 11–16) with a small negative Eu anomaly (Eu/Eu* = 0.68–0.85), being characteristic of volcanics formed in a subduction setting. On Rb – Y + Nb, Nb – Y, Rb – Ta + Yb and Ta – Yb discrimination diagrams, the compositions of the volcanics are also consistent with those of felsic rocks formed in subduction settings. SHRIMP-dating of zircon from the felsic volcanics of the Babina belt of the Central Bundelkhand greenstone complex, performed for the first time, has shown that they were erupted in Neoarchaean time (2542 ± 17 Ma). The early sequence of the Babina belt is correlatable with the rocks of the Mauranipur belt, whose age is tentatively estimated as Mesoarchaean. The Central Bundelkhand greenstone complex consists of two (Meso- and Neoarchaean) sequences, which were formed in subduction settings. 相似文献
188.
189.
190.