Effect of annealing temperature on the reactivity of Lunar fines toward adsorbed water

The ability of adsorbed water to react with feldspar-rich lunar soils, create fine pores, and expand the specific surface area is reduced about five-fold if the fines are heated at 700°C rather than 300°C. The loss of reactivity is attributed to the annealing of radiation damage tracks which reduces their etchability by water. Although the pore volume which can be induced decreases drastically, the distribution of pore sizes is not altered significantly. Most of the induced pores have a width of about 45Åwith a smaller population concentrated at about 120Å. For fines without water treatment, loss of specific surface area by sintering does not occur at temperatures below 700°C.     

Spatial variability of soils developing on basalt flows in the Potrillo volcanic field,southern New Mexico: prelude to a chronosequence study

If the systematic spatial variability of soils in a chronosequence is identified and accounted for, the accuracy of quantitative data derived from soil chronosequence studies will be increased. A sample design using landscape positions with minimal variability could result in more accurate chronofunctions from these studies. Four basalt flows in the Potrillo volcanic field, southern New Mexico, with ages ranging between 20 ka and 260 ka (⁴⁰Ar/³⁹Ar and/or cosmogenic ³He methods) provide a sound basis for a soil chronosequence study. Basalt flow surface relief in the Potrillos reduces with time as depressions fill with basalt rubble and aeolian dust. Soil variability is primarily a function of landscape position with respect to ridges and swales in the original basalt flow topography. Soils developing over original topographic lows (swale soils) form primarily in aeolian dust, have larger amounts of total carbonate and soluble salts, and display greater variability than soils developing over original topographic highs (ridge soils). It is thus concluded that ridge soils, which have minimal variability, should be employed for a soil chronosequence study of basalt surfaces in the Potrillo volcanic field. The spatial variability of swale soils results in part from the significant hydrologic variability of low-lying landscape positions. Depth profiles of chloride concentrations suggest that hydrologic variability systematically correlates with the size and shape of depressions in which soils are forming. The infilling of depressions with aeolian material results in increasingly arid hydrologic conditions both by increasing the volume of aeolian material that is being drained and by reducing the catchment area for runoff into the depression. Depressions fill at different rates, however, depending on their size, shape and catchment area. Small, narrow depressions fill quickly, and their associated soils form under more arid conditions and have stronger development than soils in large depressions. Therefore, a number of geomorphic surfaces of varying age may develop on a single isochronous basalt flow. Each of these surfaces will have unique hydrologic characteristics and consequently different degrees of soil development. The pre-burial high water flux evident in depressions suggests that basalt flows may play an important role in aquifer recharge in this area of New Mexico. Copyright © 1999 John Wiley & Sons, Ltd.     

Magnetic studies at Starunia paleontological and hydrocarbon bearing site (Carpathians,Ukraine)

The Starunia oil-ozokerite deposit occurs in the Boryslav-Pokuttya Unit of the Carpathian Foredeep, which is the main oil- and gas-bearing part of the Ukrainian Carpathians. Starunia is of great interest in studying the relationship between the magnetic properties of rocks, soils and hydrocarbons due to extensive surface microseeps yielding oil and gas, mineral water, and clay pulp containing hydrocarbons. We identified a local negative magnetic anomaly (30–35 nT) with a width of about 700 m within the MAG1 profile. The magnetic high is associated with the area of the largest mud volcanoes in the Starunia structure. Magnetic susceptibility of the soil was measured on a site with three distinct landscape features: a patch of forest with phaeozem and mass-specific susceptibility (χ) of 20–45 × 10^?8 m³/kg for the surface topsoil; an area near the volcano and Nadia-1 well with visible hydrocarbon microseepage at the surface and the topsoil showing no visible evidence of hydrocarbon presence with χ = 20–50 × 10^?8 m³/kg; and a patch of lowland with gleysols and χ = 10–20 × 10^?8 m³/kg. Hydrocarbon-containing clays and soils from the alluvial sediments of the Velyky Lukavets River and bedrock clays near the Nadia-1 well demonstrated high χ values (up to 250–440 × 10^?8 m³/kg).     

Particle dislodgement from a flat sand bed by wind

The rate, with respect to area and time, at which grains are dislodged from a sand bed for given wind conditions is an important factor in determining the grain transport rate and the intensity of grain activity in each of the transport modes. The literature of the subject contains little direct information about particle dislodgement. The paper describes a series of experiments in which dyed sand grains, spread on the surface of quartz dune sand in a wind-tunnel, were photographed at five second intervals while the sand was exposed to wind. The data on rate of loss of coloured grains was used, for two of three chosen size fractions, to deduce the dislodgement rate for each size fraction. The variation of this dislodgement rate with shear velocity is shown graphically for values of u_* between 24 cm s^?1 and 50 cm s^?1. Because of the artificial method of distribution of the coloured sand grains, the results should be applied with caution to natural conditions. The interpretation of the observations of dyed grain loss involved the numerical simulation of the process which comprises removal of coloured grains, slightly offset by replenishment as upwind coloured grains settle briefly in the observed zone. An estimation of grain excursion length has to be incorporated in the simulation. This estimation was made by trial, but general corroboration was found from earlier work. Comparisons are made between dislodgement rates obtained thus and rates estimated by Anderson (1986) and by Jensen and Sorensen (1986). Reasonable agreement with the latter is found in the u_* range 30 cm s^?1.     

Quantifying gravel overlap and dislodgement forces on natural river bars: implications for particle entrainment

Equations for predicting particle entrainment typically assume that clast weight is the only factor resisting motion in the force balance on individual grains. In this work, increases in the force required to dislodge surface particles due to overlapping by surrounding clasts is quantified. Field data were collected at two subaerially‐exposed bars along the Colorado River in central Texas, USA, with median gravel diameters (D₅₀) of 37 and 64 mm. Clast size, shape, weight, the force required for vertical removal, and the fraction of clast area covered by surrounding grains were measured. Small hooks were glued to individual clasts without disrupting their positions and quasi‐static peak forces required to vertically dislodge each clast were measured using a force gauge. Clasts were also colored with dye before being dislodged, and image analysis was used to calculate the fraction of clast surface area covered by surrounding grains. The effect of overlap on the particle force balance is quantified by defining the ‘excess force ratio’ as the dislodgement force divided by the weight of the clast. Excess force ratio varies weakly but systematically with clast size: lifting larger clasts can require forces up to two times the clast's weight, while smaller clasts can require forces up to seven times their weight. The fraction of clast surface area covered by surrounding particles is also weakly correlated with excess force ratio. By assuming that critical shear stresses are proportional to the excess force ratio, the effect that overlap alone may have on particle entrainment is calculated. For a given size class, the most mobile grains should have critical shear stresses controlled only by their weight. However, clast overlap also causes broad distributions of critical stresses for partially‐exposed surface grains. The data quantify the significant fraction of bed area that should be less mobile than grain size alone would predict. Copyright © 2011 John Wiley & Sons, Ltd.     

A preliminary magnetic study of soil samples from west-central Minnesota

Various rock magnetic techniques were applied to characterize magnetically the samples of a soil profile taken from west-central Minnesota. There is a marked change in magnetic properties as a function of depth in the core. X-ray analysis and Curie temperature measurements carried out on the magnetic fractions indicate that magnetite is the dominant iron oxide in both the top soil and the subsoil. The intensity of anhysteretic remanent magnetization (ARM) decreases sharply as the depth increases. In contrast, the stability of ARM was found to be higher for the subsoil. The surface soil sample was capable of acquiring a significant amount of viscous remanent magnetization (VRM). The VRM acquisition coefficient (S_a) of the subsoil (S_{a= 3.18 × 10^?6emu g^?1, 3.18 × 10^?6A m² kg^?1}) was about ten times weaker than that of the top soil sample (S_a = 3.868 × 10^{?7emu g?1, 3.868 × 10?7A m2 kg?1}). The magnetic domain state indicator, the ratio of coercivity of remanence to coercive force, H_cr/H_c, was 1.5 and 3.85 for the top soil and subsoil, respectively. It appears that the observed variations in magnetic properties down the present soil core is due only to a difference in grain size. We conclude that the magnetic grains in surface soil samples were more single-domain (SD) like whereas the magnetite grains in the subsoil samples were more likely in pseudo-single-domain (PSD) or small multidomain (MD) range. The observed lower stability for the surface soil samples is attributed to the presence of superparamagnetic grains whose presence was confirmed by transmission electron micrographs.     

The possible role of magnetic measurements in the discrimination of Sahara/Sahel dust sources

The mineral magnetic properties of deposited dusts collected along a broadly north‐to‐south transect across Niger have been investigated on both a bulk and particle size‐specific basis. Dusts display a general north‐to‐south gradient in fine‐grained ferrimagnetic mineral (magnetite/maghemite) concentrations, with samples south of the Sahara/Sahel transition (south of ~15·5^o N) generally containing greater concentrations than dusts from further north where the climate is much drier. This distinction is seen especially clearly in the clay (< 2 µm) fraction, which harbours the products of weathering and pedogenesis. This gradient in ferrimagnetic mineral concentrations broadly parallels that previously reported for surface soils/sands across a similar latitudinal range. We suggest that the regional distinction in both dust and surface soil/sand magnetic properties can be related to differences in weathering regime between the arid Saharan parts of the transect and the Sahel sites where higher rainfall has permitted stronger weathering and pedogenesis. Given that the weathering‐related magnetic signatures in the clays dominate the magnetic properties of the < 16 µm fractions in these samples, and that this particle size component is most likely to be involved in long‐range transport, magnetic measurements hold out the potential of discriminating Sahara and Sahel dusts deposited in remote areas. Copyright © 2011 John Wiley & Sons, Ltd.     

Plagioclase weathering in the groundwater system of a sandy,silicate aquifer

The weathering rate of plagioclase was estimated in the groundwater system of a sandy, silicate aquifer formed after the Wisconsin Glacial Stage. The study area is an isthmus lying between Crystal and Big Muskellunge Lakes in northern Wisconsin, USA. Plagioclase occupies 3% of the quartz and K‐feldspar dominated sediments. Groundwater in the study area is recharged in part by precipitation through the isthmus soils and in part by seepage from Crystal Lake, which is of low ionic strength and chemically in steady state. Water analysis revealed that the chemistry of groundwater recharged from Crystal Lake is regulated by mineral dissolution reactions. The rate constant for plagioclase was estimated using mass balances for sodium concentrations along a groundwater flowline from Crystal Lake. For this calculation, various kinds of hydrological/mineralogical information were used: groundwater flow path from oxygen isotope analysis, groundwater travel times from flow modelling, mineral composition from microprobe analysis and surface area of minerals from BET (Brunauer–Emmett–Teller) analysis. The overall range of the estimation was less than an order of magnitude (3·5 × 10^?16 to 3·4 × 10^?15 mol/m²/s). The result is up to three orders of magnitude slower than the previous field estimates, which applied geometric methods in measuring mineral surface areas. However, this result is somewhat higher than the estimates reported by other BET area‐based studies, which were undertaken on soil profiles having different hydrological conditions. This rate difference is interpreted as a result of higher mineral reactivity owing to younger sediment age. The rate difference is smaller when this result is compared with the estimates from the soils of similar age, indicating that the differences in hydrological condition are not sufficient to explain the weathering rate discrepancy between the laboratory and field studies, which is up to five orders of magnitude. Copyright © 2002 John Wiley & Sons, Ltd.     

Importance of soil surface characteristics on water erosion in a small grazed Sahelian catchment

This study concerns the problem of water erosion in the Sahel. Surface water and sediment yields (suspended matter and bedload) were monitored for 3 years (1998–2000) at the outlet of a small grazed catchment (1·4 ha) in the northern part of Burkina Faso. The catchment consists of about 64% sandy deposits (DRY soil surface type), which support most of the vegetation, and about 34% of crusted bare soils (ERO soil surface type). The annual solid‐matter export is more than 90% suspended sediment, varying between 4·0 and 8·4 t ha^?1. The bedload represents less than 10% of soil losses. In a single flood event (10 year return period), the sediment yield can reach 4·2 t ha^?1. During the period studied, a small proportion (20 to 32%) of the floods was thus responsible for a large proportion (80%) of the solid transport. Seasonal variation of the suspended‐matter content was also observed: high mean values (9 g l^?1) in June, decreasing in July and stabilizing in August (between 2 and 4 g l^?1). This behaviour may be a consequence of a reorganization of the soil surfaces that have been destroyed by trampling animals during the previous long dry season, vegetation growth (increase in the protecting effect of the herbaceous cover) and, to a lesser extent, particle‐supply limitation (exhaustion of dust deposits during July). The particle‐size distribution in the suspended matter collected at the catchment outlet is 60% made up of clay: fraction ≤2 µ m. The contribution of this clay is maximum when the water rises and its kaolinite/quartz ratio is then close to that of the ERO‐type surfaces. This indicates that these surfaces are the main source of clay within the catchment. Copyright © 2003 John Wiley & Sons, Ltd.     

Defining phases of bedload transport using piecewise regression

Differences in the transport rate and size of bedload exist for varying levels of flow in coarse‐grained channels. For gravel‐bed rivers, at least two phases of bedload transport, with notably differing qualities, have been described in the literature. Phase I consists primarily of sand and small gravel moving at relatively low rates over a stable channel surface. Transport rates during Phase II are considerably greater than Phase I and more coarse grains are moved, including material from both the channel surface and subsurface. Transition from Phase I to Phase II indicates initiation and transport of grains comprising the coarse surface layer common in steep mountain channels. While the existence of different phases of transport is generally acknowledged, the threshold between them is often poorly defined. We present the results of the application of a piecewise regression analysis to data on bedload transport collected at 12 gravel‐bed channels in Colorado and Wyoming, USA. The piecewise regression recognizes the existence of different linear relationships over different ranges of discharge. The inflection, where the fitted functions intersect, is interpreted as the point of transition from Phase I to Phase II transport; this is termed breakpoint. A comparison of grain sizes moved during the two phases shows that coarse gravel is rarely trapped in the samplers during Phase I transport, indicating negligible movement of grains in this size range. Gravel larger than about D₁₆ of the channel surface is more consistently trapped during Phase II transport. The persistence of coarse gravel in bedload samples provides good evidence that conditions suitable for coarse grain transport have been reached, even though the size of the sediment approaches the size limits of the sampler (76 mm in all cases). A relative breakpoint (R_br) was defined by the ratio between the discharge at the breakpoint and the 1·5‐year flow (a surrogate for bankfull discharge) expressed as a percentage. The median value of R_br was about 80 percent, suggesting that Phase II begins at about 80 percent of the bankfull discharge, though the observed values of R_br ranged from about 60 to 100 percent. Variation in this value appears to be independent of drainage area, median grain size, sorting of bed materials, and channel gradient, at least for the range of parameters measured in 12 gravel‐bed channels. Published in 2002 by John Wiley & Sons, Ltd.     

Effects of long soil surface residence times on apparent cosmogenic nuclide denudation rates and burial ages in the Cradle of Humankind,South Africa

In situ cosmogenic nuclides are an important tool for quantifying landscape evolution and dating fossil-bearing deposits in the Cradle of Humankind (CoH), South Africa. This technique mainly employs cosmogenic 10-Beryllium (¹⁰Be) in river sediments to estimate denudation rates and the ratio of 26-Aluminium (²⁶Al) to ¹⁰Be (²⁶Al/¹⁰Be), to constrain ages of sediment burial. Here, we use ¹⁰Be and ²⁶Al concentrations in bedrock and soil above the Rising Star Cave (the discovery site of Homo naledi) to constrain the denudation rate and the exposure history of soil on the surface. Apparent ¹⁰Be-derived denudation rates obtained from pebble- to cobble-sized clasts and coarse-sand in soil (on average 3.59 ± 0.27 m/Ma and 3.05 ± 0.25 m/Ma, respectively) are 2-3 times lower than the bedrock denudation rates (on average 9.46 ± 0.68 m/Ma). In addition, soil samples yield an average ²⁶Al/¹⁰Be ratio (5.12 ± 0.27) that is significantly lower than the surface production ratio of 6.75, which suggests complex exposure histories. These results are consistent with prolonged surface residence of up to 1.5 Ma in vertically mixed soils that are up to 3 m thick. We conclude that the ¹⁰Be concentrations accumulated in soils during the long near-surface residence times can potentially cause underestimation of single-nuclide (¹⁰Be) catchment-wide denudation rates in the CoH. Further, burial ages of cave sediment samples that consist of an amalgamation of sand-size quartz grains could be overestimated if a pre-burial ²⁶Al/¹⁰Be ratio calculated from the surface production is assumed. © 2019 John Wiley & Sons, Ltd.     

Drop size distribution and kinetic energy load of rainfall events in the highlands of the Central Rift Valley,Ethiopia

Abstract

Knowledge of rainfall characteristics is important for estimating soil erosion in arid areas. We determined basic rainfall characteristics (raindrop size distribution, intensity and kinetic energy), evaluated the erosivity of rainfall events, and established a relationship between rainfall intensity I and volume-specific kinetic energy KE_vol for the Central Rift Valley area of the Ethiopian highlands. We collected raindrops on dyed filter paper and calculated KE_vol and erosivity values for each rainfall event. For most rainfall intensities the median volume drop diameter (D₅₀) was higher than expected, or reported in most studies. Rainfall intensity in the region was not high, with 8% of rain events exceeding 30 mm h^-1. We calculated soil erosion from storm energy and maximum 30-min intensity for soils of different erodibility under conditions of fallow (unprotected soil), steep slope (about 9%) and no cover and management practice on the surface, and determined that 3 MJ mm ha^-1 h^-1 is the threshold erosivity, while erosivity of >7 MJ mm ha^-1 h^-1 could cause substantial erosion in all soil types in the area.

Editor Z.W. Kundzewicz; Associate Editor Q. Zhang     

Discriminating residual and colluvial soils using topographic analysis in a small,forested catchment in Japan

Soil moisture plays an important role in hydrology. Understanding factors (such as topography, vegetation, and meteorological conditions) that influence spatio‐temporal variability in soil moisture, and how this influence is manifested, is important for understanding hydrological processes. A number of distributed (quasi‐)physical hydrological models have been developed to investigate this subject. Previous studies have shown that the spatial differences in the distribution of soil types (residual and colluvial soils) dominantly reflect spatio‐temporal fluctuations in soil moisture and runoff. We present a methodology for assessing the spatial distribution of residual and colluvial soils, which differ with respect to their physical characteristics, in a 0·88 km² forested catchment with complex topography and a complex land‐use history. Our method is based on penetration resistance profile data; in this data set, each data point represents soil physical characteristics within an area of about 25 m². If the spatial distribution of soils under similar meteorological, geological, historical land use, and other conditions could be characterized on the basis of similarity in topographic features, then the spatial distribution of soil could be predicted based on relationships between various topographic indices (e.g. topographic index and local slope). We tested whether our model correctly assessed the reference data. The model's results were 90·5% correct for residual soils and 87·3% correct for colluvial soils. Further studies will quantify the relationships between topographic features of land covered by residual and colluvial soils and changes in spatio‐temporal variations in the catchment (e.g. vegetation and land use) as a function of geology or meteorology. Copyright © 2007 John Wiley & Sons, Ltd.     

杭州城区土壤的磁性与磁性矿物学及其环境意义

对杭州城区四个不同功能区块土壤进行了系统的环境磁学测定,结果表明城市土壤的磁化率平均值为128×10^-8m³·kg^-1,频率磁化率平均值3.6%(样品数=182),城市土壤呈现明显的磁性增强. 城市土壤的磁化率与频率磁化率呈极显著指数负相关,表明城市土壤磁性增强明显区别于自然成土过程引起的以超顺磁性(SP)颗粒为主的表土磁性增强机理. 统计分析表明,城市土壤磁化率与软剩磁和饱和等温剩磁(SIRM)呈显著直线正相关,说明亚铁磁性矿物是城市土壤剩余磁性的主要载体. 综合等温剩磁获得曲线、热磁曲线、磁滞回线等岩石磁学测定和SEM/EDX分析,城市土壤的磁性矿物以磁铁矿和赤铁矿为主,磁性矿物以假单畴-多畴（PSD-MD）颗粒存在,粒度明显大于成土过程形成的磁性颗粒,这些磁性颗粒主要来自燃料燃烧、汽车尾气等环境污染物. 因此,城市土壤磁测可作为城市土壤污染监测、污染空间分布和污染物来源判断的新手段.     

Rainfall/runoff processes in a small peri‐urban catchment in the Andes mountains. The Rumihurcu Quebrada,Quito (Ecuador)

Situated at the foot of the Pichincha volcano, the city of Quito is frequently subjected to hydroclimatic hazards. In 1995 an 11·2 km² watershed, located in the vicinity of the city, was equipped with eight rain gauges and two flow gauges to better understand the local rainfall/runoff transformation processes. Rainfall simulation experiments were carried out on more than 40 one‐square‐metre plots to measure infiltration point‐processes. The high density of measurement devices allowed us to identify the origin and nature of the various contributions to runoff for the different physiographic units of the watershed: urban area from an altitude of 2800 to 3200 m; farmland, pasture and forested land, and finally páramo above 3900 m. Runoff occurs mainly in the lower part of the basin and is caused by urbanization; however, the natural soils of this area can also produce Hortonian runoff, which is predominant in a few events. This contribution can be studied through rainfall simulation experiments. In the upper natural zone, the younger and more permeable soils generate less runoff on the slopes. However, almost permanently saturated contributing areas, which are located in the bottom of the quebradas, may generate flood events, the size of which depends on the extent of the area concerned. Variations in the runoff coefficients are related first to the baseflow and second to the amount of rainfall in the previous 24 h. This analysis, which underlines the complexity of a small, peri‐urban, volcanic catchment, is a necessary preliminary to runoff modelling in an area where very few experiments have been carried out on small catchments. Copyright © 2001 John Wiley & Sons, Ltd.     

Effect of Time on Dynamic Shear Modulus of Selected Cohesive Soil of One Section of Express Way No. S2 in Warsaw

Several researches published comprehensive reports on dynamic soil properties of cohesive soils, in which many of them outlined, i.e., key factors affecting the dynamic shear modulus. For cohesive soils, the modulus at small strains (g < 10^t-3 %) is, first of all, a function of void ratio and effective confining stress. For clays, however, secondary time effects and clay mineralogy (fabric and structure) also appear to be important. The influence of confinement of laboratory-prepared as well as naturally deposited clays consists in an increase of shear modulus logarithmically as a function of time. In this paper, the effect of duration of the various confining pressures on dynamic shear modulus (G) of selected cohesive soils from Warsaw area was evaluated. Shear modulus was determined on the basis of resonant column tests, at low and high shearing strain amplitudes. It is shown that the calculated shear modulus is time-dependent; during approximately first 1000 minutes of consolidation, the moduli increased by almost 50%. Moreover, it is characterized by two phases: an initial one results from primary consolidation and a second one, which occurs after the end of primary consolidation, herein about 16-17 hours, and is called “long-term time effect”. This effect was found also for modulus at higher shearing strains (γ > 10³%, e.g., 3 × 10³%, 5 × 10³%, 8 × 10³%, 2 × 10³%).     

Space weathering processes on airless bodies: Fe isotope fractionation in the lunar regolith

Nanophase Fe metal grains (np-Fe°) are a product of space weathering, formed by processes related to meteorite impacts, and solar-wind sputtering on airless planetary bodies, such as the Moon. Iron isotopes of lunar soils are fractionated during these processes, and the np-Fe° in the finest (<10 μm), mature, size fractions of the soil become enriched in heavier isotopes by ∼0.3‰ in ⁵⁶Fe/⁵⁴Fe in comparison to the bulk rocks (0.03±0.05‰), from which the soil was formed. A positive correlation of δ⁵⁶Fe values with the soil maturity index, I_S/FeO, suggests that the high δ⁵⁶Fe values reflect production of nanophase Fe metal that is produced by space weathering that occurs on airless planetary bodies. Furthermore, the enrichment of δ⁵⁶Fe in the smallest size fraction of lunar soils supports a model for creation of np-Fe° through vapor deposition induced by micrometeorites, as well as that by solar-wind sputtering.     

Luminescence dating of quartz from ironstones of the Xingu River,Eastern Amazonia

This study reports on the first investigation into the potential of quartz luminescence dating to establish formation ages of ferruginous duricrust deposits (ironstones) of the Xingu River in Eastern Amazonia, Brazil. The studied ironstones comprise sand and gravel cemented by goethite (FeO(OH)), occurring as sandstones and conglomerates in the riverbed of the Xingu River, a major tributary of the Amazon River. The Xingu ironstones have a cavernous morphology and give origin to particular habitat for benthic biota in an area that hosts the largest rapids in Amazonia. So far, the Xingu ironstones have uncertain formation ages and their sedimentary origin is still poorly understood. In this way, seven samples of ironstones distributed along the lower Xingu River were collected for optically stimulated luminescence (OSL) dating of their detrital quartz sand grains. Additionally, the organic content of some samples was dated by radiocarbon (¹⁴C) for comparison with quartz OSL ages. The luminescence ages of the sand-sized quartz grains extracted from the ironstones were obtained from medium (100–300 grains) and small (10–20 grains) aliquots using the single aliquot regenerative-dose (SAR) protocol. Equivalent doses (D_e) distributions have varied overdispersion (OD) both for medium size aliquots (OD = 19–58 %) and small size aliquots (OD = 29–76 %). No significant trend was observed between D_e and aliquot size. The studied ironstones grow over the riverbed, but stay below or above water throughout the year due to the seasonal water level variation of the Xingu River. However, the effect of water saturation in dose rates is reduced due to relatively low porosity of ironstones. Water saturated dose rates (dry sample dose rates) range from 2.70 ± 0.21 (2.79 ± 0.22) Gy/ka to 12.34 ± 0.97 (13.26 ± 1.12) Gy/ka, which are relatively high when compared to values reported for Brazilian sandy sediments elsewhere (∼1 Gy/ka). Samples with high overdispersion (>40 %) are mainly attributed to mixing of grains trapped in different time periods by goethite cementation. The obtained OSL ages for water saturated (dry) samples range from 3.4 ± 0.3 (3.3 ± 0.4) ka to 59.6 ± 6.0 (58.1 ± 6.4) ka, using D_e determined from medium size aliquots and dose response curves fitted by an exponential plus linear function. Radiocarbon ages of the bulk organic matter extracted from selected ironstone varied from ca. 4 cal ka BP to ca. 23 cal ka BP. Significant differences were observed between OSL and radiocarbon ages, suggesting asynchronous trapping of organic matter and detrital quartz within the ironstone matrix. These late Pleistocene to Holocene ages indicate that ironstones of the Xingu River result from an active surface geochemical system able to precipitate goethite and cement detrital sediments under transport. The obtained ages and differences between OSL and radiocarbon ages point out that the ironstones have multiphase and spatially heterogeneous growth across the Xingu riverbed. Our results also expand the application of luminescence dating to different sedimentary deposits.