Evidence for the Blake event in volcanic rocks from Lipari (Aeolian Archipelago)

Palaeomagnetic and geochronological measurements have been carried out on the late Pleistocene basaltic–andesitic unit of Monte Chirica–Costa Rasa, on the island of Lipari (Aeolian Archipelago). The lava flow sequence is about 10  m thick and has been sampled in detail. Magnetic properties are rather uniform; Curie temperatures of 540° to 580 °C, and the saturation IRM reached at applied values of 0.1  T point to titanomagnetite as the main magnetization carrier. Thermal and AF demagnetization have shown the presence of secondary magnetization components. These were removed mostly at 450°–500 °C or 20–30  mT, indicating a highly stable ChRM with directions from transitional to reverse. Where a ChRM could not be isolated by application of the demagnetization techniques, the converging remagnetization circles method gave a mean ChRM value fully comparable with that obtained from other methods. ⁴⁰Ar/³⁹Ar determinations were performed on two lava flows, in the lower and upper parts of the sequence. The former shows a transitional ChRM direction and a whole-rock age of 157±12  ka, the latter a reverse direction, a whole-rock age of 143±17  ka and a ground-mass age of 128±23  ka. The radiometric data and the reconstructed stratigraphy, which indicate ages of 150±10  ka and 104±3.5  ka, respectively, for the volcanic units at the bottom and top of the Monte Chirica–Costa Rasa unit, suggest that the reverse directions recorded in Lipari are related to the Blake event.     

The detection of single-domain greigite (Fe3S4) using rotational remanent magnetization (RRM) and the effective gyro field (Bg): mineral magnetic and palaeomagnetic applications

The intensity of rotational remanent magnetization (RRM) acquired by single-domain greigite at a rotation frequency of 5 rps was combined with measurements of anhysteretic remanent magnetization (ARM) to calculate the effective biasing field ( Bg ) that produced the RRM. Samples of single-domain greigite had Bg values between -137 and -84 μT, and a MDF_RRM of c. 80 mT. By contrast, a suite of natural and synthetic ferrimagnetic iron oxide samples, including single-domain magnetite and y Fe₃O₄ tape particles, acquired Bg values between -3 and -14 μT, and MDF_RRM ranged between 43 and 68 mT (when RRM was acquired). Multidomain magnetite did not acquire a RRM. Bg values at 5 rps were calculated from previously published data for magnetite particles of different grain sizes, which revealed a minimum Bg value of -24 μT and a MDF_RRM of 57 mT for the finest fraction (0.2-0.8 μm in diameter). In a geological example, measurements of Bg and MDF_RRM were used to detect the presence of greigite in a 4 m long Late Weichselian sediment core. Variations in inclination, declination and the intensity of the natural remanent magnetization (NRM) correlate with changes in magnetic mineralogy.     

Palaeomagnetism of the Tudor gabbro, Ontario: evidence for divergence between Grenvillia and interior Laurentia

Summary. After thermal and alternating field (AF) cleaning, the characteristic high blocking temperature A component of natural remanent magnetization (NRM) of the Tudor gabbro of southern Ontario has a mean direction D = 326°, I =–46° ( k = 132, α₉₅= 4.8°, N = 8 sites). The corresponding palaeopole, 133°E, 12°N ( dp = 4°, dm = 6°), confirms the palaeopole 137°E, 17°N (α₉₅= 8.4°) reported earlier by Palmer & Carmichael, based on AF cleaning only. The A NRM has unblocking temperatures > 515–525°C which exceed the estimated 500°C peak temperature reached locally during ∼ 1050 Ma Grenvillian regional metamorphism. The A NRM therefore predates metamorphism and is probably a primary thermoremanence (TRM). The age of the Tudor NRM has previously been taken to be about 675 Ma, but recent ⁴⁰Ar/³⁹Ar dating by Baksi has shown that this is the time of post-metamorphic cooling to 200–250°C. Hornblendes record initial cooling of the intrusion to 590±20°C at 1110 Ma and this is the best estimate of the age of the A remanence. Successful Thellier-type palaeointensity determinations on 11 Tudor samples confirm that the A NRM is a TRM and indicate a palaeofield at this time of 18–27 μT, about 50–70 per cent of the present field intensity at 27° magnetic latitude. The anomalous Tudor A palaeopole, which lies well to the west of both 1000–800 Ma Grenvillian palaeopoles and 1100–1050 Ma poles from Interior Laurentia, is interpreted as recording divergence between Grenvillia and Interior Laurentia just before the Grenvillian orogeny, rather than a post-metamorphic extension of the apparent polar wander path as previously assumed.     

Palaeomagnetism of alkaline lava flows from El Salto-Almafuerte, Córdoba Province, Argentina

Summary. Stable components of magnetization have been isolated in 15 lava flows (mean K-Ar age 123 ± 4 Myr) from the alkaline sequence outcropping at El Salto-Almafuerte, Province of Cordoba, Argentina. Magnetic and geologic stratigraphy, as well as K-Ar ages indicate that this sequence was probably extruded in the Lower Cretaceous during the first volcanic cycle of the Sierra de los Cóndores Group (Vulcanitas Cerro Colorado Formation).
The palaeomagnetic pole-position for El Salto-Almafuerte lava flows, computed from the mean of 15 virtual geomagnetic poles and denoted SAK₇, is: 25° E, 72° S ( k = 35, α₉₅= 6.5°); it is fairly close to other Lower Cretaceous palaeomagnetic poles for South America. The elongated distribution of Cretaceous palaeomagnetic poles suggest recurrent drift for South America in early Cretaceous time.
The palaeomagnetic and radiometric data for the igneous rocks from El Salto-Almafuerte support the magnetic reversal time-scale for the early Cretaceous suggested by oceanic magnetic lineations.     

Coercive force of single crystals of magnetite at low temperatures

The temperature dependence of coercive force H _c was studied on well-characterized and stoichiometric millimetre-sized single crystals of magnetite at a series of 16 temperatures from 300 to 10 K using a SQUID magnetometer. H _c decreases gradually with cooling to the isotropic temperature, T _i = 130 K, where the first magnetocrystalline anisotropy constant K ₁ becomes zero. H _c exhibits a sharp increase at the Verwey transition, T _v = 120 K, where the structure changes from cubic to monoclinic. In crossing the Verwey transition, H _c increases by more than two orders of magnitude, from 20 μT to 2.4 mT, and the shape of the hysteresis loops becomes wasp-waisted.
Observed coercivity between 300 K and 170 K varies with temperature as λ _s / M _s , where λ _s is the magnetostriction constant and M _s is the saturation magnetization, indicating that the coercivity in MD magnetite is controlled mainly by internal stress associated with dislocations or other crystal defects. It seems likely that the stable single-domain-like magnetic memory observed in large MD magnetite crystals is due to magnetoelastically pinned domain walls. The discontinuous change in H _c at the Verwey transition is controlled by abrupt changes in magnetocrystalline and magnetostriction constants due to crystal deformation from cubic to monoclinic structure.     

Reappraisal of surface wave magnitudes in the Eastern Mediterranean region and the Middle East

We report on a detailed palaeomagnetic study of the Miocene Farellones volcanic formation in the Chilean Andes near Santiago (two sections, 37 sites, about 400 orientated cores). Petrological observations show evidence of low-grade metamorphism increasing downwards through the volcanic sequence. Optical observations of opaque minerals and magnetic experiments suggest that in many cases maghemitization is associated with hydrothermal alteration. However, thermal demagnetization data indicate that the low-grade metamorphism did not significantly modify the direction of the primary remanent magnetization recorded at the time of emplacement of the volcanic lava flows. Four intervals of polarity with two intermediate palaeodirections were observed in the ~650-m-thick composite section. According to the dispersion of flow average directions, palaeosecular variation was slightly larger than that observed in general during the Upper Cenozoic. The site mean directions obtained in this study differ significantly from the expected Miocene direction. Clockwise rotations of up to 20° of small blocks are probably associated with the deformation of the Andean Cordillera since middle Miocene times. Geomagnetic palaeointensity data were obtained, using the Thellier method, on 24 samples from eight distinct lava flows. The flow mean VDM varies from 1.4 to 4.0 × 10²² A m⁻². Altogether, our data seem to suggest the existence of a relatively low geomagnetic field undergoing large fluctuations. Although a linear relationship was observed between the natural remanent magnetization and the thermal remanent magnetization acquired during the Thellier–Thellier experiments, undetected chemical alteration of the magnetic minerals during hydrothermalism may also explain the unusually low palaeointensity obtained.     

Palaeomagnetic results from the Cretaceous Bagh Group in the Narmada Basin, central India: evidence of pervasive Deccan remagnetization and its implications for Deccan volcanism

A palaeomagnetic study of 115 samples (328 specimens) from 22 sites of the Mid- to Upper Cretaceous Bagh Group underlying the Deccan Traps in the Man valley (22°  20'N, 75°  5'E) of the Narmada Basin is reported. A characteristic magnetization of dominantly reverse polarity has been isolated from the entire rock succession, whose depositional age is constrained within the Cretaceous Normal Superchron. Only a few samples in the uppermost strata have yielded either normal or mixed polarity directions. The overall mean of reverse magnetization is D _m=144°, I _m=47° ( α ₉₅=2.8°, k =152, N =18 sites) with the corresponding S-pole position 28.7°S, 111.2°E ( A ₉₅=3.1°) and a palaeolatitude of 28°S±3°. The characteristic remanence is carried dominantly by magnetite. Similar magnetizations of reverse polarity are also exhibited by Deccan basalt samples and a mafic dyke in the study area. This pole position falls near the Late Cretaceous segment of the Indian APWP and is concordant with poles reported from the Deccan basalt flows and dated DSDP cores (75–65  Ma) of the Indian Ocean. It is therefore concluded that the Bagh Group in the eastern part of the Narmada Basin has been pervasively remagnetized by the igneous activity of Deccan basalt effusion. This overprinted palaeomagnetic signature in the Bagh Group indicates a counter-clockwise rotation by 13°±3° and a latitudinal drift northwards by 3°±3° of the Indian subcontinent during Deccan volcanism.     

Palaeomagnetism of Dhar traps and drift of the subcontinent during the Deccan volcanism

Summary. Palaeomagnetic investigations were carried out on nine lava flows around the Dhar region, which constitute the northern part of the Deccan traps. The stability of remanent magnetism of these specimens was analysed by an alternating magnetic field, thermal demagnetization and memory tests. Six flows exhibited characteristic components of magnetization, with a mean direction of D =143°, I =+46° ( K = 107.1, α₉₅=5.5°). This gives a VGP located at 29° N, 67° W (δ_p=4.5°, δ_m= 7.0°). The lower site with normal magnetization and the upper five sites with reverse magnetization indicate a geomagnetic field reversal during the initial phases of Deccan volcanism in the Early Tertiary period. A rapid northward migration of about 18° in latitude and a simultaneous anticlockwise rotation of 37° is calculated for the subcontinent.     

Thermochronometry and palaeomagnetism of the Archaean Nelshoogte Pluton, South Africa

²⁰⁷Pb/²⁰⁶Pb single-grain zircon, ⁴⁰Ar/³⁹Ar single-grain hornblende and biotite, and ⁴⁰Ar/³⁹Ar bulk-sample muscovite and biotite ages from the Nelshoogte trondhjemite pluton located in eastern Transvaal, South Africa, show that this granitoid had a protracted thermal history spanning 3213±4  Ma to about 3000  Ma. Whole-rock ⁴⁰Ar/³⁹Ar ages from cross-cutting dolerite dykes indicate that these were intruded at about 1900  Ma. There is no evidence of this or other, later events significantly affecting the argon systematics of the minerals from the pluton dated by the ⁴⁰Ar/³⁹Ar method.
  The pluton has a well-defined palaeomagnetic pole which is dated at 3179±18 (2 σ ) Ma by ⁴⁰Ar/³⁹Ar dating of hornblende. This pole (18°N, 310°E, A ₉₅=9°) yields a palaeolatitude of 0°, significantly different from other Archaean poles from the Kaapvaal Craton. The palaeolatitude difference implies that there was significant apparent polar wander during the Archaean. A second, overprinting magnetization seen in the pluton is also seen in the lower-Proterozoic dolerite dykes, and is consistent with other lower-Proterozoic (2150–1950  Ma) poles for southern Africa.     

Permo-Carboniferous (Kiaman) palaeointensity results from the western Bohemian Massif, Germany

Thellier palaeointensity analyses were carried out on samples from three quartz porphyry intrusions located within the western part of the Bohemian Massif close to the German-Czech Republic border. These intrusives have been dated at 280-275 Ma. which places them in the main part of the Permo-Carboniferous (Kiaman) Reversed Superchron (P-CRS). This age is consistent with the mean characteristic remanence direction calculated at D/ I = 204/- 1, giving a VGP at 36N, 341E. Palaeointensity values range from 6.6 μT to 22.1 μT, with a mean value of 12.0 ± 1.3 μT, which has a corresponding VDM value of (3.0 ± 1.2) × 10²² A m². This suggests that the geomagnetic field strength recorded by the quartz porphyries is only 37 per cent of the current value, supporting recent studies that report a field strength of between 25 and 40 per cent of the present-day value during the P-CRS.     

Magnetostratigraphy of Palaeocene basalts from the Vaigat Formation of West Greenland

A palaeomagnetic study comprising the directional results from 289 individual lava flows, sampled along eight sections in the Palaeocene basalts of West Greenland, is reported. The eight individual sections are correlated using lithostratigraphical marker horizons to form a single composite profile. Generally, the lithological correlation is in good agreement with the record of geomagnetic secular variation.
  The total composite palaeomagnetic profile represents a stratigraphic thickness of 1.6  km through the Vaigat Formation, which is the lowermost of the two volcanic formations formed during the main stage of plateau volcanism. Only two polarity zones are found in the composite profile, suggesting a very short duration for the West Greenland main plateau-building volcanism. ⁴⁰Ar/³⁹Ar dates support a high extrusion rate and also indicate that the lower normal polarity zone is Chron C27n and that the upper reverse polarity zone is Chron C26r.
  The C27n–C26r transition is fully recorded along one of the sections (Nuusap Qaqqarsua), with intermediate directions covering a 200  m thick succession of lavas. A combined palaeomagnetic, field and geochemical study along this profile showed good agreement; that is, geochemically and geologically derived single magmatic events show groupings of the palaeomagnetic directions. Supposing a duration for the geomagnetic transition of 5000 years, the eruption frequency during this period was as high as one flow every 80 years.     

Palaeomagnetism of Neogene Ocros dyke swarm, the Peruvian Andes: implication for the Bolivian orocline

Summary. Remanent magnetization directions of 32 dykes and lava flows sampled near Ayacucho, the Peruvian Andes revealed 14.2°± 5.5° counterclockwise rotation after the Neogene intrusion of this dyke swarm. Palaeo-magnetic results of these rocks and other palaeomagnetic evidences from the Central Andean Mesozoic rocks suggest relatively recent occurrence of the Andean oroclinal bending around the axis at the Peru-Chile border.     

Palaeomagnetism of the Lower Cretaceous Sierra De Los Condores Group Cordoba Province Argentina

Measurements are described of the directions of remanent magnetization of 89 samples from nine lava flows and red beds. Stable remanent magnetization was isolated after AC demagnetizing. All the units have normal remanent magnetization, except one lava flow which yields a direction toward the north with positive inclination. From the mean direction of stable remanence, referred to the bedding, of each unit a virtual geomagnetic pole is computed; the mean of eight of these poles is 90·6 °E, 84·2° South, α₉₅= 4·7° and represents the position of the palaeomagnetic pole for the exposures of the Sierra de Los Condores group from El Estrecho-Cerro Libertad. The position of this pole is reasonably close to the positions of the South American Lower Cretaceous palaeomagnetic poles for the Serra Geral and Vulcanitas Cerro Colorado formations and the trachybasaltic dykes from Rio Los Molinos. This supports the interpretations that the South Atlantic Ocean was formed in Lower Cretaceous times and that the Earth's magnetic field was on average similar to that of a geocentric dipole in South America in the Lower Cretaceous, and suggests that there has not been substantial relative movements between Central Argentina and Southern Brazil.     

Palaeointensity results from Ethiopian basalts: implications for the Oligocene geomagnetic field strength

From a large collection of Ethiopian flood basalts (~30  Myr old) sampled for magnetostratigraphy, ⁴⁰Ar/³⁹Ar geochronology and geochemical investigations, 47 samples were selected in order to test their suitability for Thellier palaeointensity experiments. Only 17 samples from eight individual flows yielded reliable palaeointensity estimates, with flow-mean virtual dipole moments ranging from 3.0 to 10.5 × 10²²  A  m² .
  A critical review of the Oligocene palaeointensity data set, including these new Ethiopian data, indicates an Oligocene mean virtual dipole moment of 5.1 ± 2.5 × 10²²  A  m² for the complete data set. After applying mild selection criteria, the reduced data set yields a mean value of only 4.6 ± 1.9 × 10²²  A  m² . This value is significantly lower than the present-day field strength but is higher than the Mesozoic dipole low mean field. This low Oligocene field might be in agreement with the high palaeosecular variation and rather high non-dipole field invoked around 30  Ma. However, the Oligocene data set is largely dependent on the palaeointensity determinations from Armenia, obtained mainly from baked contacts, which show amazingly low dispersion at both flow and between-flow levels. More data are needed to reduce the weight of these determinations on the mean value and avoid a possible bias.     

Palaeomagnetism and K—Ar age of the Upper Ordovician Alcaparrosa Formation, Argentina

Summary. Palaeomagnetic data from 71 hand samples of igneous rocks of Late Ordovician age exposed in western Argentina (31.3°S, 69.4°W, Alcaparrosa Formation) are given. Stable remanent magnetization was isolated in the majority of samples; they yield a palaeomagnetic pole at 56°S 33°E ( N = 8, α₉₅= 16°). Whole rock K-Ar age determinations yield an age of 416 ± 10 Myr for a pillow lava of the Alcaparrosa Formation.
Palaeomagnetic data for South America, Africa, Australia, Antarctica and India suggest that Gondwana was a unit at least as far back as 1000 Myr. The palaeomagnetic data define a rapid polar migration for Gondwana in Ordovician time which is consistent with the widespread occurrences of Late Ordovician glacial deposits across this supercontinent.     

Preliminary palaeomagnetic results of an Archaean dolerite dyke of west Greenland: geomagnetic field intensity at 2.8 Ga

The geomagnetic field intensity during Archaean times is evaluated from a palaeomagnetic and chronological study of a dolerite dyke intruded into the 3000 Ma Nuuk Gneisses at Nuuk (64.2°N, 51.7°W), west Greenland. Plagioclase from the dolerite dyke yields a mean K-Ar age of 2752 Ma. Palaeomagnetic directions after thermal demagnetization of the dyke and the gneiss reveal a positive baked-contact test, indicating that the high-temperature-component magnetization of the dyke is primary. Thellier experiments on 12 dyke specimens yield a palaeointensity value of 13.5±4.4 μT. The virtual dipole moment at ca. 2.8 Ga is 1.9±0.6 × 10²² Am², which is about one-quarter of the present value. The present study and other available data imply that the Earth's magnetic field at 2.7 ∼ 2.8 Ga was characterized by a weak dipole moment and that a fairly strong geomagnetic field similar to the present intensity followed the weak field after ca. 2.6 Ga.     

Continuous GPS measurements across the Western Alps, 1996–1998

Global Positioning System (GPS) data are analysed from three permanent sites, two in the Western Alps (Grasse, France, and Zimmerwald, Switzerland) and the third in the Po Basin (Torino, Italy), for the 2.5-year period from 1 January 1996 to 1 July 1998. An analysis of the stochastic properties of the position time series reveals a significant amount of spatially and temporally correlated noise, which best fits a model combining white noise and flicker noise. The coloured noise is drastically reduced by spatially filtering the time series, suggesting that it is not due to site-specific effects such as monument motion, but rather to noise sources common to the three sites, such as reference frame, satellite orbit or Earth orientation errors. We find velocity uncertainties (95 per cent confidence interval) of 2.7  mm  yr⁻¹ at GRAS, 2.3  mm  yr⁻¹ at ZIMM, and 2.9  mm  yr⁻¹ at TORI. The residual velocity in the Eurasian reference frame is statistically greater than zero at ZIMM only, with 2.4 ± 2.3  mm  yr⁻¹ of motion in a NW direction. These uncertainties place an upper bound on the expected deformation in the Western Alps. Velocities relative to stable Eurasia do not exceed 3  mm  yr⁻¹, corresponding to a maximum strain rate of 0.03  μstrain  yr⁻¹ over the GRAS–TORI–ZIMM triangle.     

A pseudo-Thellier relative palaeointensity record, and rock magnetic and geochemical parameters in relation to climate during the last 276 kyr in the Azores region

In the pseudo-Thellier method for relative palaeointensity determinations (Tauxe et al. 1995) the slope of the NRM intensity left after AF demagnetization versus ARM intensity gained at the same peak field is used as a palaeointensity measure. We tested this method on a marine core from the Azores, spanning the last 276  kyr. We compared the pseudo-Thellier palaeointensity record with the conventional record obtained earlier by Lehman et al . (1996 ), who normalized NRM by SIRM. The two records show similar features: intensity lows with deviating palaeomagnetic directions at 40–45  ka and at 180–190  ka. The first interval is associated with the Laschamps excursion, while the 180–190  ka low represents the Iceland Basin excursion (Channell et al. 1997). The pseudo-Thellier method, in combination with a jackknife resampling scheme, provides error estimates on the palaeointensity.
  Spectral analysis of the rock magnetic parameters and the palaeointensity estimates shows orbitally forced periods, particularly 23  kyr for climatic precession. This suggests that palaeointensity is still slightly contaminated by climate. Fuzzy c -means cluster analysis of rock magnetic and geochemical parameters yields a seven-cluster model of predominantly calcareous clusters and detrital clusters. The clusters show a strong correlation with climate, for example samples from detrital clusters predominantly appear during rapid warming. Although both the pseudo-Thellier palaeointensity m _a and fuzzy clusters show climatic influences, we have not been able to find an unambiguous connection between the clusters and m _a .     

Seismic quiescence before the M 7, 1988, Spitak earthquake, Armenia

A detailed analysis of the 35  yr of seismicity between 1962 and 1997 using a gridding technique shows that the M 7, Spitak earthquake of 1988 December 7 was preceded by a quiescence anomaly that started at approximately 1984±0.5, and lasted about 5±0.5  yr, up to the main shock. This quiescence anomaly had a radius of about 20±3  km, estimated from circular areas with 75 per cent rate decrease, centred at the point of maximum significance of the anomaly. The quiescence was clearly present in the aftershock volume during the 5  yr before the 1988 main shock, but its statistically strongest expression was located 30  km NW of the epicentre. This anomaly fulfills the association rules between precursory quiescence anomalies and main shocks, even for a tight definition, and is therefore proposed as a case of precursory quiescence. The largest value of the standard deviate Z , found by random selection of samples by gridding, was Z =14 for a time window of T _w=3  yr, using a sample size of N =300 events. This makes this anomaly the strongest observed so far, and it is the first documented in an environment of continental collision. There are no false alarms exceeding in significance the precursor. The Armenian earthquake catalogue used for this study had 4600 earthquakes with M ≥ M _min=2.2 in the area bounded by 39.5° to 42°N/42.5° to 47°E. From the point of view of homogeneous reporting this is the best catalogue we have analysed so far. The limits of the data used and the density of the grid are dictated by the data, and have no influence on the results. The choice of free parameters does not influence the results significantly within the following limits: 100≤ N ≤500, 2≤ T _w≤7, 2.2≤ M _min≤2.8.     

Microwave palaeointensity from the R3–N3 geomagnetic field reversal

The microwave palaeointensity technique has been used to determine palaeointensity during the R3–N3 geomagnetic field reversal, using lavas from the Esja region of southwestern Iceland. The resulting intensity determinations have been compared to two previous studies which used the Shaw and Thellier techniques. Both reported low field intensities during the reversal except for four flows that produced high values (20.4–36.8 μT) using the Shaw technique compared to a single maximum intermediate value of 15.9 μT using the Thellier method. In this paper, an average microwave transitional palaeointensity of 6.95 ± 2.07 μT is found for samples used in the Shaw technique study, and of 7.80 ± 1.61 μT for samples used in the Thellier study, demonstrating that there is no evidence for strong fields during this reversal.