Marble mylonites in the Bancroft shear zone, Ontario, Canada: microstructures and deformation mechanisms

Mylonitization of medium-grade marbles in the Bancroft shear zone, Ontario, Canada, is characterized by decreasing grain-size of both calcite and graphite, and a variety of textures. Calcite grain-sizes vary from several millimeters in the protolith, to 50–200 μm in mylonite, to <30 μm in ultramylonite. Corresponding calcite grain shapes are equant in the protolith, elongate in protomylonite (first-developed dimensional preferred orientation), equant in coarse mylonite, elongate in fine mylonite (second-developed dimensional preferred orientation) and generally equant in ultramylonite, which suggests that external energy (applied stress) that tends to elongate grains competed with internal energy sources (e.g. distortional strain) that favor equant shapes. Graphite grain-size changes from several millimeters to centimeters in the protolith to submicroscopic in ultramylonite. In the mylonitic stages, graphite is present as dark bands, while in the ultramylonitic stage it is preserved as a fine coating on calcite grains.Based on textural evidence, twinning (exponential creep; regime I), dynamic recrystallization (power law creep; regime II) and possibly grain boundary sliding superplasticity (regime III) are considered the dominant deformation mechanisms with increasing intensity of mylonitization; their activity is largely controlled by calcite grain-size. Calcite grain-size reduction occurred predominantly by the process of rotation recrystallization during the early stages of mylonitization, as indicated by the occurrence of core and mantle or mortar structures, and by the grain-size of subgrains and recrystallized grains. Grain elongation in S-C structures indicates the activity of migration recrystallization; these structures are not the result of flattening of originally equant grains. Differential stress estimates in coarse mylonites and ultramylonites, based on recrystallized grain-size, are 2–5 and 14–38 MPa, respectively. Initial grain-size reduction of graphite occurred by progressive separation along basal planes, analogous to mica fish formation in quartzo-feldspathic mylonites.Calcite-graphite thermometry on mylonitic and ultramylonitic samples shows that the metamorphic conditions during mylonitization were 475 ± 50°C, which, combined with a differential stress value of 26 MPa, gives a strain rate of 1.2 x 10⁻¹⁰s⁻¹ based on constitutive equations; corresponding displacement rates are <38 mmyr⁻¹.     

Construction of crossed girdles by superposing four subfabrics,each with a single maximum

Commonly, basal glide is the predominant deformation mechanism of quartz in tectonites. Therefore, local deformation is probably mostly progressive simple shear rotating the sheared domains as well as deforming them. If a tectonite body is constrained to be deformed irrotationally and approximately homogeneously throughout, it is necessarily traversed by closely spaced material surfaces that are approximately plane and orthogonal originally, and stay so through time. These surfaces act as internal boundaries and enforce cancellation of the rigid-body rotations of, in the general case, four distinct families of domains, with slip planes and directions mutually mirror-symmetric. The overall symmetry of the fabric is orthorhombic, with the mirror planes coinciding with the principal planes of strain. Certain grains with basal planes in favorable orientation for one of the four ideal simple shears could initiate the deformation, and because of the need for compatibility, entrain neighboring grains into a similar strain, making the surroundings of an initiating grain a shear zone. Compatibility also requires thec-axes of grains in a domain to be rotated progressively toward the direction of maximum shortening. If the original orientation of crystallographic axes was random, domains of one family thus acquire a fabric with a single maximum, and the four resulting fabrics with single maxima combine to form crossed-girdle patterns. Depending on the orientation of the average shear planes and slip directions in the four families, the crossed girdles can be of different types; most fabric types that have been observed in quartz tectonites can be obtained by superposition. Crossed-girdle fabrics with low symmetry result from non-coaxial strain histories.     

Dynamic recrystallization near the brittle-plastic transition in naturally and experimentally deformed quartz aggregates

The electron backscattering diffraction technique (EBSD) was used to analyze bulging recrystallization microstructures from naturally and experimentally deformed quartz aggregates, both of which are characterized by porphyroclasts with finely serrated grain boundaries and grain boundary bulges set in a matrix of very fine recrystallized grains. For the Tonale mylonites we investigated, a temperature range of 300–380 °C, 0.25 GPa confining pressure, a flow stress range of ~ 0.1–0.2 GPa, and a strain rate of ~ 10^− 13 s^− 1 were estimated. Experimental samples of Black Hills quartzite were analyzed, which had been deformed in axial compression at 700 °C, 1.2–1.5 GPa confining pressure, a flow stress of ~ 0.3–0.4 GPa, a strain rate of ~ 10^− 6 s^− 1, and to 44% to 73% axial shortening. Using orientation imaging we investigated the dynamic recrystallization microstructures and discuss which processes may contribute to their development. Our results suggest that several deformation processes are important for the dismantling of the porphyroclasts and the formation of recrystallized grains. Grain boundary bulges are not only formed by local grain boundary migration, but they also display a lattice misorientation indicative of subgrain rotation. Dynamic recrystallization affects especially the rims of host porphyroclasts with a hard orientation, i.e. with an orientation unsuitable for easy basal slip. In addition, Dauphiné twins within porphyroclasts are preferred sites for recrystallization. We interpret large misorientation angles in the experimental samples, which increase with increasing strain, as formed by the activity of fluid-assisted grain boundary sliding.     

Evolution of a calcite marble shear zone complex on Thassos Island, Greece: microstructural and textural fabrics and their kinematic significance

The deformation history of a monophase calcite marble shear zone complex on Thassos Island, Northern Greece, is reconstructed by detailed geometric studies of the textural and microstructural patterns relative to a fixed reference system (shear zone boundary, SZB). Strain localization within the massive marble complex is linked to decreasing P–T conditions during the exhumation process of the metamorphic core complex. Solvus thermometry indicates that temperatures of 300–350°C prevailed during part of the shear zone deformation history. The coarse-grained marble protolith outside the shear zone is characterized by symmetrically oriented twin sets due to early coaxial deformation. A component of heterogeneous non-coaxial deformation is first recorded within the adjacent protomylonite. Enhanced strain weakening by dynamic recrystallization promoted strong localization of plastic deformation in the ultramylonite of the calcite shear zone, where high strain was accommodated by non-coaxial flow. This study demonstrates that both a pure shear and a simple shear strain path can result in similar crystallographic preferred orientations (single c-axis maximum perpendicular to the SZB) by different dominant deformation mechanisms. Separated a-axis pole figures (+a- and −a-axis) show different density distributions with orthorhombic texture symmetry in the protolith marble and monoclinic symmetry in the ultramylonite marble consistently with the observed grain fabric symmetry.     

Comments on the interpretation of deformation textures in rocks

In rocks that undergo ductile deformation, preferred orientation develops as a result of intracrystalline slip and mechanical twinning. The orientation distribution is a consequence of the microscopic mechanisms and of the strain path. It can be used to get some insight into the deformation history; however it is never unique. The interpretation relies largely on polycrystal plasticity theory. The concepts of stress equilibrium and strain compatibility, which are two extreme assumptions made to model deformation, are discussed. New approaches such as the viscoplastic self-consistent theory are a compromise and may be applicable to mineral systems which display a high degree of plastic anisotropy. Important extensions allow for heterogeneous deformation in the polycrystal from grain to grain and even within grains in correspondence with microstructural observations. All these theories defy the popular notion which is becoming entrenched in the geological literature, that the microscopic slip plane normal aligns with the axis of maximum principal compressive stress, and that in simple shear the crystallographic slip plane rotates into the macroscopic shear plane and the slip direction into the macroscopic shear direction, an orientation referred to by geologists as ‘easy glide’. It is emphasized that future work on texture development of rocks should be based on rigorous physics rather than ingenious intuition, in accordance with an old recommendation of Walter Schmidt.     

Simulating coseismic deformation of quartz in the middle crust and fabric evolution during postseismic stress relaxation — An experimental study

Non-steady state deformation and annealing experiments on vein quartz are designed to simulate earthquake-driven episodic deformation in the middle crust. Three types of experiments were carried out using a modified Griggs-type solid medium deformation apparatus. All three start with high stress deformation at a temperature of 400 °C and a constant strain rate of 10^− 4 s^− 1 (type A), some are followed by annealing in the stability field of α-quartz for 14–15 h at zero nominal differential stress and temperatures of 800–1000 °C (type A + B), or by annealing for 15 h at 900 °C and at a residual stress (type A + C).The quartz samples reveal a very high strength > 2 GPa at a few percent of permanent strain. The microstructures after short-term high stress deformation (type A) record localized brittle and plastic deformation. Statisc annealing (type A + B) results in recrystallisation restricted to the highly damaged zones. The new grains aligned in strings and without crystallographic preferred orientation, indicate nucleation and growth. Annealing at non-hydrostatic conditions (type A + C) results in shear zones that also develop from deformation bands or cracks that formed during the preceding high stress deformation. In this case, however, the recrystallised zone is several grain diameters wide, the grains are elongate, and a marked crystallographic preferred orientation indicates flow by dislocation creep with dynamic recrystallisation. Quartz microstructures identical to those produced in type A + B experiments are observed in cores recovered from Long Valley Exploratory Well in the Quaternary Long Valley Caldera, California, with considerable seismic activity.The experiments demonstrate the behaviour of quartz at coseismic loading (type A) and subsequent static annealing (type A + B) or creep at decaying stress (type A + C) in the middle crust. The experimentally produced microfabrics allow to identify similar processes and conditions in exhumed rocks.     

Transport properties of olivine grain boundaries from electrical conductivity experiments

Grain boundary processes contribute significantly to electronic and ionic transports in materials within Earth’s interior. We report a novel experimental study of grain boundary conductivity in highly strained olivine aggregates that demonstrates the importance of misorientation angle between adjacent grains on aggregate transport properties. We performed electrical conductivity measurements of melt-free polycrystalline olivine (Fo₉₀) samples that had been previously deformed at 1200 °C and 0.3 GPa to shear strains up to γ?=?7.3. The electrical conductivity and anisotropy were measured at 2.8 GPa over the temperature range 700–1400 °C. We observed that (1) the electrical conductivity of samples with a small grain size (3–6 µm) and strong crystallographic preferred orientation produced by dynamic recrystallization during large-strain shear deformation is a factor of 10 or more larger than that measured on coarse-grained samples, (2) the sample deformed to the highest strain is the most conductive even though it does not have the smallest grain size, and (3) conductivity is up to a factor of ~?4 larger in the direction of shear than normal to the shear plane. Based on these results combined with electrical conductivity data for coarse-grained, polycrystalline olivine and for single crystals, we propose that the electrical conductivity of our fine-grained samples is dominated by grain boundary paths. In addition, the electrical anisotropy results from preferential alignment of higher-conductivity grain boundaries associated with the development of a strong crystallographic preferred orientation of the grains.     

Fabric development in shear zones: theoretical controls and observed phenomena

It is suggested that the kinematic framework controls the orientation of crystallographic fabrics developed in plastically deformed quartzites. Important directions in this framework are those of the instantaneous stretching axes, and the flow plane and flow direction if these can be uniquely defined. Rotation of the crystal axes takes place at any instant of time dependent on the orientation of the grain relative to the stretching axes. Because of this dependence the skeletal outline^* of a pattern of preferred orientation is sensitive to the closing stages of deformation. Thus fabrics measured in major movement zones cannot be related to early thrust or shear displacements without considering the effects of the geological history subsequent to those events.Nevertheless, asymmetric fabrics in movement zones may allow determination of the shear direction and sense of shear. Asymmetry in the intensity distribution is less susceptible to modification than asymmetry in the fabric skeleton, and may remain as a persistent measure of the sense of shear in mylonites subjected to coaxial deformation after non-coaxial events. However, fabric asymmetry need not always be related to the deformation history, and effects related to the population of initial grain-orientations must be considered, as well as the influence of recrystallization and grain growth.A problem of scale is involved in extrapolating the movement picture inferred from the behaviour of a few hundred crystal grains to larger dimensions. This question is also encountered when trying to specify deformation paths in mesoscopic shear zones. It is difficult to obtain simple shear experimentally because of the role discontinuities play in deformation. In certain cases in natural shear zones the quartz grains may be subjected to a coaxial deformation path while the bulk deformation is progressive simple shear. Caution must therefore be exercised when attempting to use quartz fabrics to infer characteristics of the bulk kinematics or movement picture applicable during deformation.     

The simulation of fabric development during plastic deformation and its application to quartzite: the influence of deformation history

The effect of deformation history on the development of crystallographic preferred orientation in quartzities has been simulated using a computer program based on the Taylor-Bishop-Hill analysis. Model quartzities with different combinations of glide systems have been subjected to various coaxial and non-coaxial deformation histories. It is possible to obtain information from the fabrics that develop during simple histories; for example, the location of the axis of extension is generally associated with a pole free area on a c-axis plot, and progressive axial shortening, plane strain and axial shortening produce characteristic fabrics. In progressive simple shear the fabric skeleton becomes asymmetric relative to the sense of shear and a-axes preferentially align in the flow plane parallel to the flow direction. However, this example illustrates that the fabric orientation and characteristics are controlled by the kinematic framework and bear only an indirect relationship to the finite strain accumulated to that point in the history.The imprint of the closing stages of deformation limits to some degree the use of crystallographic fabrics as a tool for structural geologists, but in favourable circumstances data can be obtained concerning characteristics of the deformation history, on the scale of the hand-specimen, for the last part of this history.     

P-T path development derived from shearband boudin microstructure

This work focuses on the development of a regional P-T-path from the Malpica-Lamego Ductile Shear Zone, NW Portugal, based on the microstructures of shearband boudins evolved during progressive simple shear. The combination of microstructural analysis, fluid inclusion studies, crystallographic preffered orientation and fractal geometry analyses, allows to link several stages in the internal evolution of the boudin to regional P-T conditions. The boudinage process is initiated under differential stress after the original layer achieved sufficient viscosity contrast relative to the surrounding matrix. Two main transformations occur simultaneously: i) change in the external shape with continuous evolution from tabular rigid body to sigmoidal asymmetric morphology (shearband boudin) and ii) localized dynamic recrystallization in the sharp-tips of the structure (acute edge of shearband boudin), and along the boudin's margin and grain boundaries. Smaller recrystallized grains, particularly in the sharp-tip domains, accommodate most of the external strain, and larger relict grains are preserved in the centre. Dynamic recrystallization under constant strain rates and strain partitioning inside the boudins is indicated by fractal geometry based on grain boundary and grain area analysis. Progressive deformation leads to the generation of structural and textural heterogeneous domains inside the boudins, and is recorded by quartz c-axis orientation analysis and fluid inclusion studies. The last deformation episode shows the final formation of the blunt-tip domain and internal secondary shear planes. The regional P-T path begins with the crystallization of andalusite after an internal shearband boudin dilation event and ends with quartz dynamic recrystallization on boudin tips. The main deformation stage (310/315 Ma) led to reactivation of internal secondary shear zones with sillimanite crystallization.     

Atypical textures in quartz veins from the Simplon Fault Zone

Samples of monomineralic quartz veins from the Simplon Fault Zone in southwest Switzerland and north Italy generally have asymmetric, single girdle c-axis patterns similar to textures measured from many other regions. Several samples have characteristically different textures, however, with a strong single c-axis maximum near the intermediate specimen axis Y (the direction within the foliation perpendicular to the lineation X) and a tendency for the other crystal directions to be weakly constrained in their orientation about this dominant c-axis maximum. This results in ‘streaked’ pole figure patterns, with an axis of rotation parallel to the c-axis maximum. These atypical samples also have a distinctive optical microstructure, with advanced recrystallization and grain growth resulting in a strong shape fabric (S_B) oblique to the dominant regional foliation (S_A), whereas typical samples have a strong S_A fabric outlined by very elongate, only partially recrystallized, ribbon grains. The recrystallized grains of the atypical samples are themselves deformed and show strong undulose extinction and a core-mantle recrystallization structure. The streaked texture is likely to be a direct consequence of lattice bending and kinking during heterogeneous slip on the favoured first-order prism (10 0) (a) system, the heterogeneity itself being due to problems in maintaining coherence across grain boundaries when insufficient independent easy-slip systems are available for homogeneous strain by dislocation glide. Such bending would be particularly prevalent in very elongate, thin ribbon grains, resulting in high internal strain energy and promoting recrystallization. Thus both the texture and the microstructure could be significantly modified by later strain increments affecting quartz grains with an already developed, nearly single-crystal texture.     

Experimental shear zones and magnetic fabrics

Magnetic fabric analysis has been used as a non-destructive means of detecting petrofabric development during experimentally produced multi-stage, transpressive deformations in ‘shear zones’. Artificial, magnetic-bearing silicate sands and calcite sands, bonded with Portland cement, were deformed at room temperature and at 100 and 150 MPa confining pressure. The slip-rate for the shear zone walls was 0.73 × 10⁻⁴ mm s⁻¹ and the maximum shear strains were about 0.38, across zones that were initially about 5 mm thick. The magnetic fabric ellipsoid rapidly spins so that the maximum and intermediate susceptibilities tend to become parallel to the shear zone walls throughout the sheared zone. The ellipsoid becomes increasingly oblate with progressive deformation. However, in all cases, the anisotropy is strongly influenced by the pre-deformation magnetic fabric. During deformation the cement gel collapses so that cataclasis of the mineral grains is suppressed. In the quartz-feldspar aggregates the magnetite's alignment is accommodated by particulate flow (intergranular displacements) of the grains. In the calcite aggregates stronger magnetic fabrics develop due to plastic deformation of calcite grains as well as particulate flow. However, the calcite grain fabrics are somewhat linear (L ≥ S) whereas the magnetic fabrics are planar (S >L). The preferred dimensional orientations of magnetite are weak and it is possible that the magnetic fabrics are due to intragranular rearrangements of magnetic domains.The transpressive shear zones are much more efficient than axial-symmetric shortening in the increase of anisotropy of the magnetic fabrics, especially in the case of the calcite aggregates. This suggests that flow laws derived for axial-symmetric shortening experiments may not be appropriate for non-coaxial strain histories such as those of shear zones.     

Strain analysis using quartz deformation bands

Quartz deformation bands are kink bands in quartz crystals. A deformation band develops as a region of localized crystal-plastic deformation with boundaries perpendicular to the slip plane and slip direction, which usually is along an -axis in the basal plane. Under cross-polarized light, the difference in crystallographic orientation between a deformation band and its host is indicated by a difference in extinction positions. The displacement between the c axis in a deformation band and the c axis in the host represents the angular shear of the deformation band in the direction of the c axis in the host grain. Assuming the deformation is homogeneous at the grain scale, the angular shear of the grain (the gauge) is calculated by multiplying the angular shear of the deformation band by the ratio of the sheared part to the whole grain. Using the strain-gauge method for three-dimensional infinitesimal strain analysis, a minimum number of five grains measured on universal stage is needed to solve for the deviatoric strain components of the aggregate if the strain is homogeneous in the aggregate. Data from more than five grains are used to find the best-fit strain components by a least-squares method. The principal strains and their orientations are found from these strain components by calculating the eigenvalues and eigenvectors. A 3-D strain ellipsoid also is obtained from strain ellipses in three perpendicular planes determined from the two-dimensional flat-stage measurements by the Wellman method. Both the strain-gauge method and the Wellman method are tested by using synthetic data sets and applied to a naturally deformed sample. Both methods give similar results; the established Wellman method thus confirms the strain-gauge calculation.     

Quartz microstructures developed during non-steady state plastic flow at rapidly decaying stress and strain rate

Synseismic loading to very high stresses (>0.5 GPa) and subsequent creep during stress relaxation in the uppermost plastosphere at temperatures of ca. 300–350 °C, near the lower tip of an inferred once seismically active crustal scale fault, was proposed based on peculiar microstructures identified in rocks exposed over >100 km² in the Sesia Zone, European Western Alps. Here we discuss the conspicuous and highly heterogeneous microstructural record of quartz in disseminated small-scale shear zones. Sub-basal deformation lamellae and arrays of elongate subgrains on the TEM-scale indicate an early stage of glide-controlled deformation at high stresses. Distributed brittle failure is indicated by healed microcracks. Very fine-grained recrystallised aggregates with a pronounced crystallographic preferred orientation reflect intense plastic flow by dislocation creep. Locally, a fine-grained foam microstructure indicates a final stage of static grain growth at low differential stress. For the previously inferred peak stresses of about 0.5 GPa and given temperatures, initial strain rates on the order of 10⁻¹⁰ s⁻¹ are predicted by available flow laws for dislocation creep of quartz. We emphasise the importance of short-term non-steady state deformation in the uppermost plastosphere underlying seismically active upper crust. The related heterogeneous record of quartz is governed by the local stress history at constant temperature.     

Plastic Deformation and Recrystallization of Garnet: A Mechanism to Facilitate Diffusion Creep

Elongate and deformed garnets from Glenelg, NW Scotland, occurwithin a thin shear zone transecting an eclogite body that hasundergone partial retrogression to amphibolite facies at circa700°C. Optical microscopy, back-scattered electron imaging,electron probe microanalysis and electron back-scatter diffractionreveal garnet sub-structures that are developed as a functionof strain. Subgrains with low-angle misorientation boundariesoccur at low strain and garnet orientations are dispersed, aroundrational crystallographic axes, across these boundaries. Towardshigh-strain areas, boundary misorientations increase and thereis a loss of crystallographic control on misorientations, whichtend towards random. In high-strain areas, a polygonal garnetmicrostructure is developed. The garnet orientations are randomlydispersed around the original single-crystal orientation. Somegarnet grains are elongate and Ca-rich garnet occurs on thefaces of elongate grains oriented normal to the foliation. Commonly,the garnet grains are admixed with matrix minerals, and, wherein contact with other phases, garnet is well faceted. We suggestthat individual garnet porphyroclasts record an evolution fromlow-strain conditions, where dislocation creep and recoveryaccommodated deformation, through increasing strain, where dynamicrecrystallization occurred by subgrain rotation, to higheststrains, where recrystallized grains were able to deform bydiffusion creep assisted grain boundary sliding with associatedrotations. KEY WORDS: diffusion creep; EBSD; garnet; plastic deformation; recrystallization     

The development of slaty cleavage, fleurieu peninsula, south australia

In low grade, biotite-rich metasiltstones and slates from the western side of Fleurieu Peninsula, the slaty cleavage is defined by elongate deformed old biotites and by the coincident elongate dimensions and (001) planes of thin, well aligned new biotites. Histograms of frequency versus (001)-S₁ angle (S₁ defined by aligned thin muscovite used as the reference plane) were determined in thin section for both populations. The old biotites show a symmetrical bimodal distribution of (001) about S₁, with maxima at around 20° either side ofS₁. This distribution, together with the preserved intracrystalline strain, indicates that these old grains deformed largely by slip on (001) with some modification of grain boundaries by diffusive transfer. The new biotite grains are very well aligned (standard deviation 3.8°) and show no sign of mechanical deformation. They have not been mechanically rotated into alignment but must have nucleated and grown in a specific orientation. The proportion of new to old grains increases with metamorphic grade, causing a rapid strengthening of the crystallographic alignment. In slates and phyllites with similar microstructure, the mica fabric determined by X-ray texture goniometry cannot be used as a quantitative measure of the geometry and magnitude of the bulk strain, as the intensity of the crystallographic fabric will be strongly influenced by the proportion of new mica, which is itself greatly affected by the metamorphic grade during slaty cleavage formation.     

Dynamic recrystallization and chemical evolution of clinoamphibole from Senja,Norway

Clinoamphibole from a mylonitic amphibolite exhibits microstructures characteristic of dynamic recrystallization, including porphyroclasts in a finer grained matrix of needle-shaped amphibole. The matrix amphibole defines an LS fabric and porphyroclasts have core and mantle structures with a core containing undulose to patchy extinction and (100) deformation twinning surrounded by a mantle of recrystallized grains. In addition intragranular grains also occur within the cores. TEM analyses of the porphyroclasts reveal that they contain a wide variety of lattice defects including high densities (5 × 10⁸cm^–2) of free dislocations and dislocation arrays, dissociated dislocations, stacking faults, and (100) micro-twins. TEM also shows that matrix grains and intragranular grains have relatively low defect densities, and that the intragranular new grains occur at localities in the porphyroclasts characterized by high densities of dislocations. These observations along with the chemical and orientation relationships between the recrystallized grains and porphyroclasts indicate that the new grains may have formed by heterogeneous nucleation and that further growth probably occurred by both strain assisted and chemically induced grain boundary migration or liquid film migration. This recrystallization event is interpreted to be synkinematic based on the fact that no recrystallization textures are present in the matrix grains and that the matrix grains define an LS fabric. However, the low defect densities in the matrix grains and the lack of intracrystalline strain in other phases indicate that post-kinematic recovery processes were active.     

Experiments on preferred orientation of platy minerals

Polycrystalline aggregates of phlogopite, talc, and brucite have been grown hydrothermally from their constituent oxides at 300–600° C, 3–5 kb, and compressed 10–30% in short-term experiments (typically 30 minutes). Under hydrostatic conditions, approximately random orientation of crystals results. When the specimen is strained at high temperature, either during or after growth of the minerals, a preferred orientation of basal planes normal to the axis of compression results. Since a similar result is obtained by straining at room temperature after growth of the minerals, the mechanism of orientation is probably mainly mechanical rotation after formation. Microscope examination showed that the preferred orientation is most marked in coarser grains of the aggregates. A second kind of foliation is defined in some specimens by closely spaced, narrow domains within which coarse grains are slightly rotated. These domains occur in conjugate sets symetrically oriented at about 45° to the axis of compression. They are interpreted as shear domains and are geometrically similar to incipient strain-slip cleavage in foliated rocks. The experiments may represent likely behavior in geological situations where the temperature or time scale precludes recrystallization during deformation, but they are probably not directly revelant to cases of axial-plane cleavage where reorientation through an influence of stress or strain during recrystallization is believed to have occurred. No unequivocal indication of the latter process was obtained in the experiments.     

Domainal fabrics of hematite in schistose,shear zone-hosted high-grade Fe ores: The product of the interplay between deformation and mineralization

Schistose high-grade hematite orebodies (>64 wt % Fe) in the Iron Quadrangle, Minas Gerais, were formed in shear zones by hydrothermal alteration of the Paleoproterozoic Cauê BIF during the Transamazonian orogenesis. The ore is comprised of platy hematite (specularite) grains that define the foliation and overprint a relict banded martite-hematite fabric resembling, at first sight, a mylonite. The EBSD analyses of a m-scale schistose orebody from the Pau Branco mine show that specularite grew as elongated plates with the (00.1) plane parallel to the foliation. The population of the measured grain aspect ratio (GAR) is homogenous in different scales, and the longest axes of the crystals align with the stretching lineation (L//X) building continuous domains, or anastomose around stretched iron oxide aggregates and rootless fold hinges. The pole figure of the (00.1) plane shows usually a maximum centered on the pole of the foliation Z often elongated on a girdle perpendicular to the lineation L. The {10.4} pole figure has the configuration of a symmetric cleft girdle and the corresponding {11.0} and {10.0} pole figures present well developed girdles parallel to the foliation with an elongated maximum centered on X. Microstructures associated with crystal-plastic behavior and dynamic recrystallization are missing and the fabric of the orebody probably results from precipitation of strain-controlled oriented hematite plates and anisotropic syntaxial growth of favorably oriented grains with the intervention of hydrothermal fluids during Fe enrichment. The shear zone provided pathways for the percolation of mineralizing fluids under temperatures that varied from 140 to 350 °C or higher, under ductile or ductile–brittle conditions. The orthorhombic fabric and CPO (crystallographic preferred orientation) of the ore nevertheless contrast with the asymmetry of simple shear as observed in the torsion experiments by Siemes et al., 2010, Siemes et al., 2011, probably due to volume loss and possibly a flattening component of deformation in the ore zone.