用裂变径迹法研究断层活动年龄的初步探讨

裂变径迹年代测定是研究断层活动年龄的新方法,它基于磷灰石中裂变径迹的退火效应。本文报导了取自郯庐断裂带等地区12个磷灰石和一个榍石的裂变径迹年龄,结果表明,在断裂带中磷灰石裂变径迹的退火效应非常明显,效应随离断层带的距离增加而减弱。结合断层带的活动特点和原岩的年龄,对断层带中磷灰石裂变径迹年龄的解释及今后的研究方向作了探讨     

Laser-ablation ICP-MS zircon U-Pb ages for key Pliocene-Pleistocene tephra beds in unglaciated Yukon and Alaska

Tephrochronology is one of the most effective ways to correlate and date Quaternary deposits across large distances. However, it can be challenging to obtain direct ages on tephra beds when they are beyond the limit of radiocarbon dating, do not contain mineral phases suitable for ⁴⁰K-⁴⁰Ar (or ⁴⁰Ar/³⁹Ar) dating, or suitable glass shards for fission-track dating are not available. Zircon U-Pb dating by laser ablation-inductively coupled plasma-mass spectrometry (LA-ICP-MS) is an emerging technique for dating young (<1 Ma) tephra. Here, we demonstrate that LA-ICP-MS zircon U-Pb dating can produce reliable ages for key tephra beds found in Yukon and Alaska. We assessed five different techniques for calculating tephra maximum depositional ages from zircon U-Pb ages for eight tephra beds. Our preferred zircon U-Pb ages (reported with 2σ uncertainties), based on a Bayesian model for calculating maximum depositional ages, are broadly consistent with previously established chronology constructed from stratigraphy, paleomagnetism, and/or glass fission track and ⁴⁰Ar/³⁹Ar ages: Biederman tephra (178 ± 17 ka), HP tephra (680 ± 47 ka), Gold Run tephra (688 ± 44 ka), Flat Creek tephra (708 ± 43 ka), PA tephra (1.92 ± 0.06 Ma), Quartz Creek tephra (2.62 ± 0.08 Ma), Lost Chicken tephra (3.14 ± 0.07 Ma), and GI tephra (542 ± 64 ka). We also present newly revised glass fission-track and ⁴⁰Ar/³⁹Ar ages recalculated from previous determinations using updated ages for the Moldavite tektite and Fish Canyon Tuff standards, and updated K decay constants. For Pleistocene age zircon crystals, corrections for ²³⁰Th disequilibrium and common-Pb are significant and must be treated with caution. Similarly, apparent tephra ages are sensitive to the choice of method used to calculate a maximum depositional age from the assemblage of individual crystallization ages. This study demonstrates that LA-ICP-MS zircon U-Pb dating can be successfully applied to numerous Pliocene-Pleistocene Alaskan-Yukon tephra, providing confidence in applying this method to other stratigraphically important tephra in the region.     

Multi-method radiometric dating of volcano-sedimentary layers from northern Italy: Age and duration of the Priabonian stage

A comparison between conventional KAr (biotite) ages and fission track (zircon and apatite) and UPb (zircon) ages obtained from stratigraphically well-constrained Priabonian (Late Eocene) volcano-sedimentary deposits of northern Italy is presented. Two sections at Priabona (one level) and Possagno (two levels) were dated. The application of fission track dating appears fruitful for obtaining reasonably precise (±4 to 5% 2σ errors) ages useful for time-scale calibration. The concordancy of apatite and zircon fission track ages, and the reproducibility of results provide the time of volcanic eruption and deposition. The UPb analysis of the zircons has not been unsuccessful, but discordancy does not permit accurate dating. Significant dates obtained from Possagno are: KAr method, 35.0 ± 0.5 Ma (duplicate analysis on K-rich biotite from the same level); fission track dating method, 35.8 ± 1.4 Ma (weighted mean age on 2 apatite and 3 zircon separates from the same level); UPb method, 36.7 ± 1.0 Ma (maximum age of discordant zircons from the same level). The comparison between the present results and recent multi-method and multi-laboratory results obtained from time equivalent Priabonian (Late Eocene) biotite-rich layers from the Apennines shows perfect agreement and supports the location of a Priabonian stage between about 37.5 Ma and about 33.7 (±0.5) Ma; the alternative ages preferred by the Decade of North American Geology convention should be abandoned and a large portion of this scale revised accordingly.     

Fission track ages on apatite of Bergell rocks from Central Alps and Bergell boulders in Oligocene sediments

Previous radiometric dating studies indicated that the Bergell region, in contrast to other regions of the Central Alps, experienced an early, rapid uplift, but with decreasing rate. Furthermore, there is also a geological record of the early uplift history of the Bergell granite by the existence of boulders which were derived from this granite and which occur in the Late Oligocene sediments of the Po plain.In this work the uplift history of the Bergell is studied in more detail by fission track dating of additional apatites from the Bergell region. Secondly, by determining apatite fission track ages the granitic boulders of the Po plain can be re-assigned to their original vertical position within the Bergell intrusive before erosion removed them in Late Oligocene time. A rather conservative estimate replaces them 6 km above the present morphology of the Bergell massif. Thus, the thickness of the Bergell granite must have been at least 8 km.Generally, fission track studies on boulders may become an important tool to study the vertical extent of mountain chains during the geological past.     

Fission track dating of kimberlitic zircons

The only reliable method for dating kimberlites at present is the lengthy and specialized hydrothermal procedure that extracts²⁰⁶Pb and²³⁸U from low-uranium zircons. This paper describes a second successful method by fission track dating of large single-crystal zircons, 1.0–1.5 cm in dimension. The use of large crystals overcomes the limitations imposed in conventional fission track analysis which utilizes crushed fragments. Low track densities, optical track dispersion, and the random orientation of polished surfaces in the etch and irradiation cycle are effectively overcome.Fission track ages of zircons from five African kimberlites are reported, from the Kimberley Pool (90.3 ± 6.5 m.y.), Orapa (87.4 ± 5.7 and 92.4 ± 6.1 m.y.), Nzega (51.1 ± 3.8 m.y.), Koffiefontein (90.0 ± 8.2 m.y.), and Val do Queve (133.4 ± 11.5 m.y.). In addition we report the first radiometric ages (707.9 ± 59.6 and 705.5 ± 61.0 m.y.) of crustal zircons from kimberlites in northwest Liberia. The fission track ages agree well with earlier age estimates. Most of the zircons examined in this study are zoned with respect to uranium but linear correlations are established (by regression analysis) between zones of variable uranium content, and within zones of constant uranium content (by analysis of variance). Concordance between the fission track method and the U/Pb technique is established and we concluded that track fading from thermal annealing has not taken place. Kimberlitic zircons dated in this study, therefore, record the time of eruption.     

Zircon fission‐track and U–Pb double dating using femtosecond laser ablation–inductively coupled plasma–mass spectrometry: A technical note

We present a new LA–ICP–MS system for zircon fission‐track (FT) and U–Pb double dating, whereby a femtosecond laser combined with galvanometric optics simultaneously ablates multiple spots to measure average surface U contents. The U contents of zircon measured by LA–ICP–MS and standardized with the NIST SRM610 glass are comparable to those measured by the induced FT method, and have smaller analytical errors. LA–ICP–MS FT dating of seven zircon samples including three IUGS age standards is as accurate as the external detector method, but can give a higher‐precision age depending on the counting statistics of the U content measurement. Double dating of the IUGS age standards gives FT and U–Pb ages that are in agreement. A chip of the Nancy 91500 zircon has a homogeneous U content of 84 ppm, suggesting the possibility of using this zircon as a matrix‐matched U‐standard for FT dating. When using the Nancy 91500 zircon as a U‐standard, a zeta calibration value of 42–43 year cm² for LA–ICP–MS FT dating is obtained. While this value is strictly valid only for the particular session, it can serve as a reference for other studies.     

Dating faults by fission track dating of epidotes — an attempt

An attempt was made to determine the absolute age of faulting by measuring fission track ages of epidotes from mineralization veins along fault and joint planes. The method was applied to epidotes from along faults and fissures in the Sinai Peninsula, which cut Precambrian rocks. Most samples yield Tertiary ages (32-11 m.y.) An Early Cretaceous event is also recorded (120-103 m.y.). Samples from country rocks (igneous and metamorphic) give ages older than 325 m.y. The results are compatible with previous geological information, and suggest that the method can be potentially useful for dating faults.     

The first tephra evidence for a Late Glacial explosive volcanic eruption in the Arxan-Chaihe volcanic field (ACVF), northeast China

A 5 mm thick tephra layer has been identified in the lacustrine sediments of Moon Lake in the Arxan-Chaihe volcanic field (ACVF) in Greater Khingan Mountains (NE China). The visible tephra layer is clearly revealed as a distinct peak in magnetic susceptibility measurements. The tephra layer consists mainly of brown vesicular glass shards and minor amounts of plagioclase, olivine and clinopyroxene. Major and minor element analysis has been carried out on the glass shards and plagioclase minerals. Glass shards show low concentrations of K₂O, similar to the eruptive products derived from post-Miocene volcanoes of the ACVF. The plagioclase phenocrysts in both lava and tephra from ACVF, and in the tephra recorded in Moon Lake are labradorites. During the Late Pleistocene to Holocene, there were also extensive explosive eruptions in the nearby Nuominhe volcanic field (NVF). Volcanic rocks from the ACVF are easily distinguished from those derived from the NVF, having distinctly different K₂O concentrations. This compositional variation is likely the result of different magmatic processes operating in the ACVF and NVF. Radiocarbon dating on organic materials from the lacustrine sediments dates the tephra layer to ca. 14,200 cal yrs BP, which implies that it was generated by a previously unknown Late Pleistocene explosive eruption in the ACVF. These results, for the first time, give a direct tephra record in this area, and suggest that identification of further tephra and/or cryptotephra in local sedimentary basins such as crater lakes of scoria cones and maars will be significant for dating the Late Pleistocene to Holocene volcanic eruptions and will help to establish a detailed record of the volcanic activity in the ACVF. The newly discovered tephra layer also provides a dated tephrochronological marker layer, which will in future studies provide a means to synchronise local sedimentary records of the climatically variable Late Glacial.     

Dating of altered mafic intrusions by applying a zircon fission track thermochronometer to baked country rock,and implications for the timing of volcanic activity during the opening of the Japan Sea

Once a mafic intrusive rock has become altered, it is generally difficult to obtain a reliable intrusion age using conventional isotopic dating methods. To overcome this problem, this study used zircon fission track (ZFT) thermochronometry to determine the timing of crystallization of altered mafic intrusions. ZFT dating was carried out on samples of baked granite country rock adjacent to dolerite dikes (5–10 m thick) in the Takato area of central Japan. Three granite samples collected within 8 mm of a dike contact yielded consistent ZFT ages of 17–16 Ma, with confined track lengths indicative of the complete annealing of pre‐existing tracks by reheating due to dike intrusion. An older ZFT age was obtained for one granite sample collected within 20 mm of the contact, but confined track length measurements indicate that this is an incompletely reset age that lies between the ZFT age of the unbaked granitic country rocks (ca. 55 Ma) and the emplacement age of the dike. Petrographic examinations suggest that post‐intrusion hydrothermal activity did not influence the ZFT ages. We conclude that the 17–16 Ma ZFT age represents the emplacement age of the dikes. Our results show that ZFT dating of baked country rock is an effective tool for dating altered mafic intrusions, for which other dating techniques are not applicable. In the eastern part of Southwest Japan, dispersed volcanic activity occurred in the late Early to early Middle Miocene (18–15 Ma), and the volcanic belt extended into the forearc. This pulse of activity was possibly related to the injection of asthenospheric material into the trench‐side mantle wedge beneath the Japan arc. We also present young apatite fission track ages (ca. 4 Ma) that may reflect a Middle Miocene or later thermal event associated with local magmatic activity near the Takato area.     

Fission track ages of North American tektites

Fission track ages of North American tektites from Texas, Georgia and Martha's vineyard range widely between 0.8 my and 34.2 my with the tektites from Georgia giving the lowest ages. Size studies of the fission track etch pits reveal the thermal history of each individual tektite resulting in the partial loss of tracks. Therefore, the measured fission track ages can be understood as thermally lowered.

Based on annealing experiments, correction factors for the thermally lowered fission track ages are found. The weighted mean of the corrected fission track ages is 34.9 my for the bediasites and the Martha's Vineyard tektite. On the other hand, the corrected fission track ages of the Georgia tektites are much lower resulting from a more complex thermal history.

It may now be stated that North American tektites and Libyan Desert glasses cannot have had a simultaneous origin.     

Quartz and polymineral luminescence dating of Japanese loess over the last 0.6 Ma: Comparison with an independent chronology

There are only a few luminescence dating studies of loess sediments in Japan, but interleaved with these deposits are many well-described tephras of known age based on ¹⁴C and fission track analysis; these independent age controls provide an opportunity to test the reliability of loess luminescence ages. This study provides such a comparison at two sites in central Honshu, the largest island in the Japanese archipelago. Samples were collected from sequences of interleaved volcanic tephra and loess deposited on a Middle Pleistocene river terrace in the Niigata Prefecture and on an Early to Middle Pleistocene dissected fluvial surface at in the Tochigi Prefecture, Honshu. Equivalent doses (D_e) were estimated from fine grains (4–11 μm) using both polymineral IR-OSL and (post-IR) blue-OSL, and quartz blue-OSL. The blue-stimulated luminescence signals could be represented by up to three exponentially decaying components; only the most light sensitive of these components was used in the final D_e estimation. Almost all the estimates of D_e from polymineral IR-OSL are smaller than those from polymineral (post-IR) blue-OSL and quartz blue-OSL, whereas the latter two are in good agreement. The blue-light stimulated luminescence ages using the most light sensitive component are shown to be in good agreement with the independent control, up to 500 ka. Although the IR-OSL signals underestimate the known age, a simple laboratory fading test is found empirically to correct for this underestimation. We conclude that the most rapidly blue-stimulated luminescence signals from quartz extracted from our loess samples give reliable ages, and that future loess dating studies should concentrate on these signals.     

Characteristics of fission tracks in zircon: Applications to Geochronology and Cosmology

We describe a simple method for nearly isotropic revelation of fission tracks in zircon. The etchant is an equivolume mixture of 48% HF and 98% H₂SO₄; etching is carried out under pressure at 150° – 180°C. For fossil track densities above ～ 5 × 10⁶, the etching time is strongly anticorrelated with track density. The total etchable fission fragment track length (2 fragments) is 11 ± 0.5 μm. The length distribution is sharply peaked; the standard deviation in different samples is ± (0.7 – 0.8) μm. Thermal annealing studies indicate a lower activation energy for track fading than was previously repoted using a phosphoric acid etchant. A practical chemical dissolution method is described for quantitatively recovering zircon crystals from rock samples; this method should find application in fission track dating of even zircon poor rocks.     

Metamorphic and cooling history of the Shimanto accretionary complex,Kyushu, Southwest Japan: Implications for the timing of out‐of‐sequence thrusting

Illite crystallinity, K–Ar dating of illite, and fission‐track dating of zircon are analyzed in the hanging wall (Sampodake unit) and footwall (Mikado unit) of a seismogenic out‐of‐sequence thrust (Nobeoka thrust) within the Shimanto accretionary complex of central Kyushu, southwest Japan. The obtained metamorphic temperatures, and timing of metamorphism and cooling, reveal the tectono‐metamorphic evolution of the complex, and related development of the Nobeoka thrust. Illite crystallinity data indicate that the Late Cretaceous Sampodake unit was metamorphosed at temperatures of around 300 to 310°C, while the Middle Eocene Mikado unit was metamorphosed at 260 to 300°C. Illite K–Ar ages and zircon fission‐track ages constrain the timing of metamorphism of the Sampodake unit to the early Middle Eocene (46 to 50 Ma, mean = 48 Ma). Metamorphism of the Mikado unit occurred no earlier than 40 Ma, which is the youngest depositional age of the unit. The Nobeoka thrust is inferred to have been active during about 40 to 48 Ma, as the Sampodake unit started its post metamorphic cooling after 48 Ma and was thrust over the Mikado unit at about 40 Ma along the Nobeoka thrust. These results indicate that the Nobeoka thrust was active for more than 10 million years.     

Validating post IR-IRSL dating on K-feldspars through comparison with quartz OSL ages

Recent developments have opened up the possibilities of using potassium feldspar for dating Pleistocene sediments; a stable (less-fading) part of the infrared stimulated luminescence (IRSL) signal can be selected by largely depleting the unstable part of the IR signal, using a combination of thermal and IR stimulation: post IR-IRSL dating (pIR-IRSL).This study aims to test the validity of pIR-IRSL dating on feldspars. We obtained pIR-IRSL ages on a large suite of samples from several locations in the Netherlands area, covering a wide range of depositional environments and ages. Age control was provided by quartz optically stimulated luminescence (OSL) ages on the same samples; these ages were shown to accord with geological age constraints. Comparison with IRSL ages enabled us to evaluate the improvement that pIR-IRSL dating provides over conventional IRSL methods.The majority of feldspar ages obtained with pIR-IRSL showed good agreement with both the quartz OSL ages and the geological age constraints. Our study demonstrates that pIR-IRSL dating is more robust than conventional IRSL and should be the method of choice in feldspar luminescence dating of Pleistocene sediments.     

柴达木盆地现今大地热流与晚古生代以来构造-热演化

依据钻孔系统稳态测温、静井温度资料与实测热导率数据分析了柴达木盆地地温场分布特征,建立了柴达木盆地热导率柱,新增了17个大地热流数据.柴达木盆地现今地温梯度介于17.1~38.6℃·km-1,平均为28.6±4.6℃·km-1,大地热流介于32.9~70.4mW·m-2,平均55.1±7.9mW·m-2.盆地不同构造单元地温场存在差异,昆北逆冲带、一里坪坳陷属于"高温区",祁南逆冲带属于"中温区",三湖坳陷、德令哈坳陷及欧龙布鲁克隆起属于"低温区",盆地现今地温场分布特征受控于地壳深部结构、盆地构造等因素.以现今地温场为基础,采用磷灰石、锆石裂变径迹年龄分布特征定性分析与径迹长度分布数据定量模拟相结合,研究了柴达木盆地晚古生代以来的沉积埋藏、抬升剥蚀和热演化史,并结合区域构造背景,对柴达木盆地构造演化过程进行了探讨,研究表明柴达木盆地晚古生代以来经历了六期(254.0—199 Ma,177—148.6 Ma,87—62 Ma,41.1—33.6 Ma,9.6—7.1 Ma,2.9—1.8 Ma)构造运动,六期构造事件与研究区构造演化的动力学背景相吻合.其中白垩纪末期(87—62 Ma)的构造事件导致了柴达木盆地东部隆升并遭受剥蚀,欧龙布鲁克隆起形成雏形,柴达木盆地北缘在弱挤压环境下形成坳陷盆地;中新世末的两期构造事件(9.6—7.1 Ma和2.9—1.8 Ma)使柴达木盆地遭受强烈挤压,盆地快速隆升,构造变形强烈,基本形成现今的构造面貌.     

裂变径迹年龄在断裂构造形迹中的应用

本文通过对苏州金山浜花岗岩岩体中北北东向断裂带取样,选矿及对其重矿物——磷灰石分别进行化学蚀刻和热中子辐射,采用白云母外探测器法分别进行自发裂变径迹与诱发裂变径迹的观察、统计及裂变径迹年龄的计算。认为该岩体形成年代是侏罗-白垩纪,而断层破裂形迹的地质事件是晚第三纪中新世。说明运用裂变径迹的方法来研究活断层的测年工作是可取的     

祁连盆地第三纪沉积物磁性地层和岩石磁组构初步研究

祁连山山间盆地内的新生代沉积物是研究新生代以来祁连山构造演化的重要材料.本文以位于祁连山中部祁连盆地内的新生代沉积物为研究对象,利用磁性地层学方法结合碎屑颗粒裂变径迹定年方法获取其沉积时代框架,在此基础上,结合岩性变化与沉积环境变迁分析祁连山构造演化历史.野外实测剖面显示该盆地内的第三系可划分为下部砾岩组和上部砂岩组两大岩性单元.古地磁结果显示砾岩组的沉积时代约为10—14.3Ma.砾岩组沉积大约在14.3 Ma开始形成,指示祁连山14.3 Ma以来构造活动变强烈.磁组构结果显示砾石组顶部沉积形成时的受力方向与现今祁连盆地周缘断层分布所指示的应力方向一致,表明这些断层大约在10 Ma附近开始活动.我们的结果揭示祁连山中部山脉14.3 Ma以来尤其在10 Ma附近构造活动较强烈.这与过去低温热年代学所获得的祁连山山体的快速冷却年龄及祁连山两端大型盆地内的第三系所记录的构造事件发生的时间基本吻合.而砂岩组的古地磁结果并未通过褶皱检验,其古地磁记录发生了后期重磁化,无法获得地层的准确沉积年龄.     

北京千家店地区侏罗系后城组磷灰石裂变径迹分析及其地质意义

运用裂变径迹分析方法, 探讨分析了千家店地区侏罗系后城组地层的构造热演化特征. 千家店地区后城组上段三个磷灰石样品,AFT年龄集中在85.7～76.0 Ma,小于其相应的地层年龄;平均封闭径迹长度为9.4～10.8 μm,小于初始径迹长度(16.3±0.9 μm),呈非对称的单峰态分布,标准偏差为2.1～2.5. 后城组下段的三个AFT样品,AFT年龄集中在82.6～62.4 Ma,小于其相应的地层年龄,也小于上段层位的AFT年龄;平均封闭径迹长度仅为7.2～7.7 μm,远小于初始径迹长度(16.3±0.9 μm),其中YQ-07样品的封闭径迹长度呈似双峰态分布,标准偏差达到3.1;显然,侏罗系样品经历了明显的中度退火行为,最大温度可能接近于90℃. AFT年龄和封闭径迹长度的规律性变化主要是由于埋深不同引起的温度差异造成的. 裂变径迹热历史模拟结果表明,沉积物自进入盆地充填埋藏一直到115 Ma左右,盆地沉积物达到最大埋深3000多米,盆地温度达到最大值90℃多,这一过程沉积速率达到66.7 m/Ma. 115 Ma之后盆地处于相对稳定期,没有明显的温度波动,直到6 Ma左右温度以11.7 ℃/Ma的速度突然下降,表明侏罗系地层遭受剥蚀,迅速上升、快速冷却直至地表,剥露速率超过了500 m/Ma.     

Northward cooling of the Kuncha nappe and downward heating of the Lesser Himalayan autochthon distributed to the south of Mt. Annapurna,western central Nepal

We investigated the tectonothermal history of the Lesser Himalayan sediments (LHS), which are tectonically overlain by the Higher Himalayan Crystalline. Fission‐track dating and the track length measurement of detrital zircons obtained from the Kuncha nappe and the Lesser Himalayan autochthonous sediments in western central Nepal revealed northward cooling of the nappe and possible downward heating of the autochthon by the overlying hot nappe. Nine zircon fission‐track (ZFT) ages of the nappe showed northward‐younging linear distribution from 11.6 Ma in the front at Tamghas, 6 Ma in the central at Naudanda, and 1.6 Ma in the northernmost point at Tatopani. Thermochronological invert calculation of the ZFT length elucidated that the Kuncha nappe gradually cooled down (30 °C/Myr) at the front and rapidly cooled down (120 °C/Myr) at the root zone. In contrast, the ZFT age of the Chappani Formation, located just beneath the Kuncha nappe in the central part, demonstrated a totally reset age of 6.8 Ma, whereas the Virkot Formation, structurally far from the nappe, yielded a partially reset age of 457.3 Ma. This suggests that the LHS underwent downward heating, resulting in a thermal print on the upper part of the LHS; however, the thermal effect was not sufficient to anneal ZFT totally in the deeper part. Presently, the nappe cover is eroded and denuded from this area. Detrital zircons from the Chappani Formation in Tansen area to the south of the Bari Gad Fault did not show any evidence of annealing, suggesting that nappe never covered the LHS distributed to the south of the fault.