Palaeosecular variation in Central Mexico over the last 30 000 years: the record from lavas

13 lava flows of known age (ages from ¹⁴C dating), which have been erupted in the last 30 000 years, have been studied to determine the palaeosecular variation of the geomagnetic field in Central Mexico. Samples were taken from two different monogenetic volcanic fields: the Michoacan-Guanajuato volcanic field (six sites) and the Chichinautzin Formation (seven sites), both part of the Transmexican Volcanic Belt. The lavas were studied in detail using rock magnetic methods (magnetic susceptibility at room temperature, low-temperature susceptibility behaviour, hysteresis loops, Curie temperatures), combined with reflected light microscopy, in order to deduce their magnetic mineralogy and the domain states of the magnetic minerals. The magnetic carriers are titanomagnetites, which show differing degrees of high-temperature deuteric oxidation, and seem to be predominantly pseudo-single domain (PSD), though in many cases are probably a mixture of domain states. Mean palaeomagnetic directions and palaeointensity values using Shaw and Thellier techniques were obtained using several specimens from each flow. Our data seem to indicate a sharp easterly swing in declination about 5000 years ago, which is also observed in lake sediments from Central Mexico. The calculated values of the virtual dipole moment (VDM) range from 3.1 to 14.9 × 10²² A m². Our data indicate that the virtual dipole moment seems to have increased gradually in magnitude over the last 30 kyr, with a peak at about 9000 years BP. These are features that have been observed in other parts of the globe and are probably caused by variations in the dipole part of the geomagnetic field.     

Palaeomagnetism of the Lower Cretaceous Sierra De Los Condores Group Cordoba Province Argentina

Measurements are described of the directions of remanent magnetization of 89 samples from nine lava flows and red beds. Stable remanent magnetization was isolated after AC demagnetizing. All the units have normal remanent magnetization, except one lava flow which yields a direction toward the north with positive inclination. From the mean direction of stable remanence, referred to the bedding, of each unit a virtual geomagnetic pole is computed; the mean of eight of these poles is 90·6 °E, 84·2° South, α₉₅= 4·7° and represents the position of the palaeomagnetic pole for the exposures of the Sierra de Los Condores group from El Estrecho-Cerro Libertad. The position of this pole is reasonably close to the positions of the South American Lower Cretaceous palaeomagnetic poles for the Serra Geral and Vulcanitas Cerro Colorado formations and the trachybasaltic dykes from Rio Los Molinos. This supports the interpretations that the South Atlantic Ocean was formed in Lower Cretaceous times and that the Earth's magnetic field was on average similar to that of a geocentric dipole in South America in the Lower Cretaceous, and suggests that there has not been substantial relative movements between Central Argentina and Southern Brazil.     

Palaeomagnetism of Dhar traps and drift of the subcontinent during the Deccan volcanism

Summary. Palaeomagnetic investigations were carried out on nine lava flows around the Dhar region, which constitute the northern part of the Deccan traps. The stability of remanent magnetism of these specimens was analysed by an alternating magnetic field, thermal demagnetization and memory tests. Six flows exhibited characteristic components of magnetization, with a mean direction of D =143°, I =+46° ( K = 107.1, α₉₅=5.5°). This gives a VGP located at 29° N, 67° W (δ_p=4.5°, δ_m= 7.0°). The lower site with normal magnetization and the upper five sites with reverse magnetization indicate a geomagnetic field reversal during the initial phases of Deccan volcanism in the Early Tertiary period. A rapid northward migration of about 18° in latitude and a simultaneous anticlockwise rotation of 37° is calculated for the subcontinent.     

Further reliability tests for determination of palaeointensities of the Earth's magnetic field

Summary. In palaeomagnetic studies of volcanic rocks it is often considered that, if the direction of NRM does not change much and the intensity de-creases gradually and smoothly during ac cleaning, then the remanent magnetization is stable and chiefly composed of TRM. This argument is extended as a consistency check to detect unwanted effects during laboratory heating. A simple procedure which employs orientated samples and a short heating (15 min) for TRM acquisition in the laboratory has been used for determining the ancient geomagnetic field intensity using seven volcanic rocks of Late Cenozoic age from central Mexico. The main reliability tests are based on the stability of direction, the close correspondence of the entire coercitivity spectra of both NRM and TRM to ac demagnetization, the low scatter of TRM directions, close correspondence of the TRM directions and the direction of the laboratory magnetic field, proportionality of TRM intensities to applied field, susceptibility comparison before and after heating, and the within-unit consistency of palaeointensity determinations.     

Magnetic field intensity study of the 1960 Kilauea lava flow, Hawaii, using the microwave palaeointensity technique

It is extremely valuable to study historic lava flows where the geomagnetic field at their time of extrusion is well known. In this study, two vertical sections, 16 m apart, have been sampled from the approximately 1 m thick 1960 Kilauea lava flow, Hawaii. Variations are seen in the rock-magnetic and palaeomagnetic properties between and within the two sections, indicating that there are small-scale lateral and vertical variations in the lava flow. The two sections showed different responses to microwave palaeointensity analysis. Section H6001 generally gave ideal linear behaviour on plots of natural remanent magnetization (NRM) lost against microwave-induced thermoremanent magnetization (T_M RM) gained, whilst the majority of samples from H6002 showed anomalous two-slope behaviour. When all plots were interpreted by taking the best-fitting line through all points, the flow mean intensity for H6001 was 31.6 ± 3.6 μT and that for H6002 was 37.1 ± 6.4 μT, compared with the expected intensity of 36 μT. Additional historic flows need to be studied in order to ascertain whether this behaviour is typical of all lava, and whether it is best to always interpret NRM lost/T_M RM gained plots by taking the line of best fit regardless of shape.     

A paleomagnetic study of the Mull lava succession

Summary. A paleomagnetic study has been made of a succession of 139 non-overlapping basaltic lavas, representing 91 per cent of the longest remaining succession of flows associated with the Paleogene Mull volcano. All the lavas have experienced considerable hydrothermal alteration, probably at up to several million years after initial magnetization and frequently with alteration to the opaque minerals and the production of new potentially magnetic phases. The question of whether directional remagnetization has taken place while preserving within-unit directional consistency and discreteness of unit mean direction is discussed. Extensive directional remagnetization is excluded as an explanation for the data. If stable directions obtained by alternating field remanence cleaning coincide with original TRM directions then a mean pole position for all temporally independent lava directions from the British Tertiary igneous province is at 71.9° N, 167.2° E, with k:22 and α₉₅:3.0°. This pole is significantly different from the geographic pole. If the difference in palaeomagnetic and geographic poles is interpreted in terms of absolute plate motion, then 2010 km of northwards motion of the western part of the Eurasian Plate, at 3.7 cm/yr, has taken place over the last 55 Myr. This motion has implications for the geological history of the Arctic and for the complexity of mantle motions.     

Preliminary palaeomagnetic results of an Archaean dolerite dyke of west Greenland: geomagnetic field intensity at 2.8 Ga

The geomagnetic field intensity during Archaean times is evaluated from a palaeomagnetic and chronological study of a dolerite dyke intruded into the 3000 Ma Nuuk Gneisses at Nuuk (64.2°N, 51.7°W), west Greenland. Plagioclase from the dolerite dyke yields a mean K-Ar age of 2752 Ma. Palaeomagnetic directions after thermal demagnetization of the dyke and the gneiss reveal a positive baked-contact test, indicating that the high-temperature-component magnetization of the dyke is primary. Thellier experiments on 12 dyke specimens yield a palaeointensity value of 13.5±4.4 μT. The virtual dipole moment at ca. 2.8 Ga is 1.9±0.6 × 10²² Am², which is about one-quarter of the present value. The present study and other available data imply that the Earth's magnetic field at 2.7 ∼ 2.8 Ga was characterized by a weak dipole moment and that a fairly strong geomagnetic field similar to the present intensity followed the weak field after ca. 2.6 Ga.     

Palaeomagnetism of the Tudor gabbro, Ontario: evidence for divergence between Grenvillia and interior Laurentia

Summary. After thermal and alternating field (AF) cleaning, the characteristic high blocking temperature A component of natural remanent magnetization (NRM) of the Tudor gabbro of southern Ontario has a mean direction D = 326°, I =–46° ( k = 132, α₉₅= 4.8°, N = 8 sites). The corresponding palaeopole, 133°E, 12°N ( dp = 4°, dm = 6°), confirms the palaeopole 137°E, 17°N (α₉₅= 8.4°) reported earlier by Palmer & Carmichael, based on AF cleaning only. The A NRM has unblocking temperatures > 515–525°C which exceed the estimated 500°C peak temperature reached locally during ∼ 1050 Ma Grenvillian regional metamorphism. The A NRM therefore predates metamorphism and is probably a primary thermoremanence (TRM). The age of the Tudor NRM has previously been taken to be about 675 Ma, but recent ⁴⁰Ar/³⁹Ar dating by Baksi has shown that this is the time of post-metamorphic cooling to 200–250°C. Hornblendes record initial cooling of the intrusion to 590±20°C at 1110 Ma and this is the best estimate of the age of the A remanence. Successful Thellier-type palaeointensity determinations on 11 Tudor samples confirm that the A NRM is a TRM and indicate a palaeofield at this time of 18–27 μT, about 50–70 per cent of the present field intensity at 27° magnetic latitude. The anomalous Tudor A palaeopole, which lies well to the west of both 1000–800 Ma Grenvillian palaeopoles and 1100–1050 Ma poles from Interior Laurentia, is interpreted as recording divergence between Grenvillia and Interior Laurentia just before the Grenvillian orogeny, rather than a post-metamorphic extension of the apparent polar wander path as previously assumed.     

Palaeomagnetism of alkaline lava flows from El Salto-Almafuerte, Córdoba Province, Argentina

Summary. Stable components of magnetization have been isolated in 15 lava flows (mean K-Ar age 123 ± 4 Myr) from the alkaline sequence outcropping at El Salto-Almafuerte, Province of Cordoba, Argentina. Magnetic and geologic stratigraphy, as well as K-Ar ages indicate that this sequence was probably extruded in the Lower Cretaceous during the first volcanic cycle of the Sierra de los Cóndores Group (Vulcanitas Cerro Colorado Formation).
The palaeomagnetic pole-position for El Salto-Almafuerte lava flows, computed from the mean of 15 virtual geomagnetic poles and denoted SAK₇, is: 25° E, 72° S ( k = 35, α₉₅= 6.5°); it is fairly close to other Lower Cretaceous palaeomagnetic poles for South America. The elongated distribution of Cretaceous palaeomagnetic poles suggest recurrent drift for South America in early Cretaceous time.
The palaeomagnetic and radiometric data for the igneous rocks from El Salto-Almafuerte support the magnetic reversal time-scale for the early Cretaceous suggested by oceanic magnetic lineations.     

Microwave palaeointensity from the R3–N3 geomagnetic field reversal

The microwave palaeointensity technique has been used to determine palaeointensity during the R3–N3 geomagnetic field reversal, using lavas from the Esja region of southwestern Iceland. The resulting intensity determinations have been compared to two previous studies which used the Shaw and Thellier techniques. Both reported low field intensities during the reversal except for four flows that produced high values (20.4–36.8 μT) using the Shaw technique compared to a single maximum intermediate value of 15.9 μT using the Thellier method. In this paper, an average microwave transitional palaeointensity of 6.95 ± 2.07 μT is found for samples used in the Shaw technique study, and of 7.80 ± 1.61 μT for samples used in the Thellier study, demonstrating that there is no evidence for strong fields during this reversal.     

Evidence for the Blake event in volcanic rocks from Lipari (Aeolian Archipelago)

Palaeomagnetic and geochronological measurements have been carried out on the late Pleistocene basaltic–andesitic unit of Monte Chirica–Costa Rasa, on the island of Lipari (Aeolian Archipelago). The lava flow sequence is about 10  m thick and has been sampled in detail. Magnetic properties are rather uniform; Curie temperatures of 540° to 580 °C, and the saturation IRM reached at applied values of 0.1  T point to titanomagnetite as the main magnetization carrier. Thermal and AF demagnetization have shown the presence of secondary magnetization components. These were removed mostly at 450°–500 °C or 20–30  mT, indicating a highly stable ChRM with directions from transitional to reverse. Where a ChRM could not be isolated by application of the demagnetization techniques, the converging remagnetization circles method gave a mean ChRM value fully comparable with that obtained from other methods. ⁴⁰Ar/³⁹Ar determinations were performed on two lava flows, in the lower and upper parts of the sequence. The former shows a transitional ChRM direction and a whole-rock age of 157±12  ka, the latter a reverse direction, a whole-rock age of 143±17  ka and a ground-mass age of 128±23  ka. The radiometric data and the reconstructed stratigraphy, which indicate ages of 150±10  ka and 104±3.5  ka, respectively, for the volcanic units at the bottom and top of the Monte Chirica–Costa Rasa unit, suggest that the reverse directions recorded in Lipari are related to the Blake event.     

Effects of weathering on single-domain magnetite in Early Pliocene marine marls

Rock magnetic parameters are often used to recognize variations in the original magnetic mineralogy and for normalizing purposes in palaeointensity studies. Incipient weathering, however, is shown to have a profound but partly reversible influence on the rock magnetic properties of the marls of the Early Pliocene Trubi formation in southern Sicily (Italy). The remanence in the marls resides in single-domain (SD) magnetite grains, but the remanent coercive force (H_cr) shows a strong variation and most values observed are anomalously high ( H_cr) range 36–188 mT).
The enhanced coercivities are attributed to stress in the magnetite grains induced by surface oxidation at low temperature. Upon heating to 150 °C a reduction of coercivities occurs that can be explained by a stress reduction as a result of a reduction of Fe^2- gradient due to a higher diffusion rate at elevated temperature. After heating to 150 °C, coercivities are quite uniform throughout the outcrop and the values are characteristic of SD magnetite (H_cr range 30–38 mT). The bulk susceptibility increases by 4–24 per cent, and the isothermal remanent magnetization (IRM) decreases by 5–11 per cent. The increase in anhysteretic remanent magnetization (ARM) is large: 20–242 per cent. The magnitude of the changes is related to the degree of weathering.
Another effect of heating the marl samples to 150 °C is a substantial reduction of the coercivities of the secondary overprint in the natural remanent magnetization. After heating. separation of the secondary and primary components by alternating-field demagnetization is more efficient. The usual difficulties of thermal demagnetization above 300 °C may thus be avoided by a combination of moderate heating to 150 °C and subsequent alternating-field demagnetization.     

Palaeointensity results from Ethiopian basalts: implications for the Oligocene geomagnetic field strength

From a large collection of Ethiopian flood basalts (~30  Myr old) sampled for magnetostratigraphy, ⁴⁰Ar/³⁹Ar geochronology and geochemical investigations, 47 samples were selected in order to test their suitability for Thellier palaeointensity experiments. Only 17 samples from eight individual flows yielded reliable palaeointensity estimates, with flow-mean virtual dipole moments ranging from 3.0 to 10.5 × 10²²  A  m² .
  A critical review of the Oligocene palaeointensity data set, including these new Ethiopian data, indicates an Oligocene mean virtual dipole moment of 5.1 ± 2.5 × 10²²  A  m² for the complete data set. After applying mild selection criteria, the reduced data set yields a mean value of only 4.6 ± 1.9 × 10²²  A  m² . This value is significantly lower than the present-day field strength but is higher than the Mesozoic dipole low mean field. This low Oligocene field might be in agreement with the high palaeosecular variation and rather high non-dipole field invoked around 30  Ma. However, the Oligocene data set is largely dependent on the palaeointensity determinations from Armenia, obtained mainly from baked contacts, which show amazingly low dispersion at both flow and between-flow levels. More data are needed to reduce the weight of these determinations on the mean value and avoid a possible bias.     

Palaeointensity studies of a late Permian lava succession from Guizhou Province, South China: implications for post-Kiaman dipole field behaviour

Palaeomagnetic results are presented from a volcanic sequence in Zhijin County, Guizhou Province, Southern China. The lavas and associated volcanic breccias comprising the sequence represent a southern extension of the Emeishan volcanic province. Biostratigraphic dating of interbedded limestone units and stratigraphic constraints indicate that the section formed during the late Permian (∼263–255  Ma), and is thus somewhat older than the Emei stratotype section in Sichuan Province, and close in age to reported estimates of the termination of the Permo-Carboniferous (Kiaman) reverse superchron. Rock magnetic analyses and reflected light microscopy indicate that the magnetic mineralogy of the lava units is dominated by fresh, primary magnetites containing a significant fraction of single-domain grains. Thermal demagnetization behaviour of the breccia units is poor, but most lava samples have one or two components of remanence above 250 °C. The normal polarity characteristic remanence held by the lavas implies a post-Kiaman age for this succession and suggests that the termination of the Kiaman occurred prior to 263  Ma, supporting recently published estimates. According to standard criteria, Thellier palaeointensity results from the lavas are of good quality and reveal that the dipole field strength was comparatively low shortly after the termination of the superchron. 80 per cent of samples record relative VDM values in the range 42–52 per cent of the present-day value, supporting recent studies of mid-Kiaman field intensity. This suggests that a low-energy dipole existed at least between 300 and 255  Ma and does not appear to have been confined to the stable reverse polarity interval.     

A pseudo-Thellier relative palaeointensity record, and rock magnetic and geochemical parameters in relation to climate during the last 276 kyr in the Azores region

In the pseudo-Thellier method for relative palaeointensity determinations (Tauxe et al. 1995) the slope of the NRM intensity left after AF demagnetization versus ARM intensity gained at the same peak field is used as a palaeointensity measure. We tested this method on a marine core from the Azores, spanning the last 276  kyr. We compared the pseudo-Thellier palaeointensity record with the conventional record obtained earlier by Lehman et al . (1996 ), who normalized NRM by SIRM. The two records show similar features: intensity lows with deviating palaeomagnetic directions at 40–45  ka and at 180–190  ka. The first interval is associated with the Laschamps excursion, while the 180–190  ka low represents the Iceland Basin excursion (Channell et al. 1997). The pseudo-Thellier method, in combination with a jackknife resampling scheme, provides error estimates on the palaeointensity.
  Spectral analysis of the rock magnetic parameters and the palaeointensity estimates shows orbitally forced periods, particularly 23  kyr for climatic precession. This suggests that palaeointensity is still slightly contaminated by climate. Fuzzy c -means cluster analysis of rock magnetic and geochemical parameters yields a seven-cluster model of predominantly calcareous clusters and detrital clusters. The clusters show a strong correlation with climate, for example samples from detrital clusters predominantly appear during rapid warming. Although both the pseudo-Thellier palaeointensity m _a and fuzzy clusters show climatic influences, we have not been able to find an unambiguous connection between the clusters and m _a .     

Dating of thaw depths in permafrost terrain by the palaeomagnetic method: experimental acquisition of a freezing remanent magnetization

The acquisition of a freezing remanent magnetization (FRM) has been studied in controlled magnetic and thermal environments by successive freezing and thawing (−18 to +20°C) of samples of natural sediments from a frost polygon near Ny Ålesund, Spitsbergen. Successive freeze-thaw cycles cause a significant decrease in the intensity of the initially induced shock remanent magnetization (SRM), associated with directional trends towards the ambient magnetic field direction during the freezing phase. A slow increase in intensity commences after seven to 10 freeze-thaw cycles. The acquisition of a FRM in samples carrying an isothermal remanent magnetization shows a significantly smaller reduction in intensity and only minor directional variations. This result indicates that only a fraction of the magnetic grains in a natural sediment contributes to the natural remanent magnetization. Insignificant changes in lengths and directions of the principal susceptibility ellipsoid axes also indicate that magnetic fabric and remanent magnetization are carried by partly different populations of magnetic grains.
The acquisition of a FRM in nature has yet to be explored. If such a process is confirmed, however, it has the potential for obtaining age estimates of ancient thaw depths and for providing insights into material transport processes in frost polygons.     

11 million years of Oligocene geomagnetic field behaviour

An 11 million year long record of the Oligocene geomagnetic field has been obtained from pelagic sediments of DSDP Hole 522 An average sample spacing of 4 cm yielded approximately one specimen per 4 to 8 kyr. The rock magnetics are remarkabh consistent across the entire interval. Previous work demonstrated a magnetic mineralogy dominated by magnetically stable magnetite. The natural remanent magnetism (NRM) carries an Oligocene polarity timescale that is in excellent agreement with the Oligocene reversal record as determined from marine magnetic anomalies (MMAs), including many of the so-called 'crypto-chrons'. Normalized NRM intensities from the undisturbed portions of the record yield a time series of variations with features consistent with a number of other palaeointensity time series derived from both sedimentary and lava sequences. These features include consistent, major decreases in palaeointensity (DIPs) at reversal boundaries, and occasional DIPs between reversal boundaries that could correspond to lineated 'tiny wiggles' in the MMA records. The data set suggests that the overall field strength was 40 per cent higher in the first half of the Oligocene when the average reversal frequency was 1.6 Myr^-1 than in the second half when the reversal frequency was 4 Myr^-1. There is also a weak dependence of average field strength on length of polarity interval. Finally, in the three cores suited to spectral analysis (of coherent polarity and relative intensity independent of lithological contamination), there is a persistent ca. 30–50ka periodicity in the variations of the relative intensity, suggesting that the geomagnetic field 'pulses' at about this frequency, not only during the Brunhes (as demonstrated by Tauxe & Shackleton 1994), but in the Oligocene as well.     

Magnetostratigraphy of Palaeocene basalts from the Vaigat Formation of West Greenland

A palaeomagnetic study comprising the directional results from 289 individual lava flows, sampled along eight sections in the Palaeocene basalts of West Greenland, is reported. The eight individual sections are correlated using lithostratigraphical marker horizons to form a single composite profile. Generally, the lithological correlation is in good agreement with the record of geomagnetic secular variation.
  The total composite palaeomagnetic profile represents a stratigraphic thickness of 1.6  km through the Vaigat Formation, which is the lowermost of the two volcanic formations formed during the main stage of plateau volcanism. Only two polarity zones are found in the composite profile, suggesting a very short duration for the West Greenland main plateau-building volcanism. ⁴⁰Ar/³⁹Ar dates support a high extrusion rate and also indicate that the lower normal polarity zone is Chron C27n and that the upper reverse polarity zone is Chron C26r.
  The C27n–C26r transition is fully recorded along one of the sections (Nuusap Qaqqarsua), with intermediate directions covering a 200  m thick succession of lavas. A combined palaeomagnetic, field and geochemical study along this profile showed good agreement; that is, geochemically and geologically derived single magmatic events show groupings of the palaeomagnetic directions. Supposing a duration for the geomagnetic transition of 5000 years, the eruption frequency during this period was as high as one flow every 80 years.     

Palaeointensity determination and K—Ar dating of the Tertiary north-east Jalisco volcanics (Mexico)

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Sixteen samples representing eight Tertiary volcanic units from north-east Jalisco, Mexico were studied in an attempt to estimate the palaeointensity of the Earth's magnetic field. The experimental technique used was similar to that proposed by Shaw (1974) and an attempt was made to incorporate further criteria using the directional behaviour of the NRM, TRM and two ARMs during the af treatment and measuring the rate of ARM acquisition before and after heating. The directional information was used for checking the stability of all remanent magnetizations involved and for correcting the ARM test values. In addition the TRM directional behaviour could be a valuable yet simple test to detect the problem of insufficient heating. The use of the ARM acquisition test in the palaeointensity determination permits the full investigation of the coercive force spectrum and could lead to a more reliable palaeointensity method. This combined ARM method was applied to one sample. Further work is needed to understand the NRM—ARM1 and TRM—ARM2 relationships if the ARM tests are to be used for correcting TRM alteration effects. Whole rock K—Ar age determinations were carried out on samples from four selected units. Ten samples, representing six of the units, are considered to yield reliable palaeointensity values. Mean values were computed for each unit and reduced to the palaeoequator. The mean palaeoequatorial values and K—Ar ages determined are: I (13 |Mp 2 Myr), 0.504 Oe; II, 0.453 Oe; III, 0.439 Oe; VI (52 |Mp 10 Myr), 0.074 Oe; VII (14 |Mp 2 Myr), 0.187 Oe and VIII (12 |Mp 2 Myr), 0.251 Oe. These results agree reasonably well with those from previous studies. A large number of palaeointensity estimations, many more than currently available, are required to obtain an average estimate of the behaviour of the Earth's magnetic field during the Tertiary.