A detailed post‐IR IRSL dating study of the Niuyangzigou loess site in northeastern China

In this study, we report standard quartz SAR OSL and post‐IR infrared (IR) stimulated luminescence (post‐IR IRSL; pIRIR₂₉₀) measurements made on sand‐sized quartz and K‐feldspar extracts from the loess‐palaeosol sequence at Niuyangzigou in northeastern China. The quartz OSL characteristics are satisfactory. Extensive pIRIR_50,290 dose recovery tests were performed by adding doses on top of the natural dose. We found that dose recovery ratios improve significantly when the test dose ranges between ~15 and ~80% of the total dose, and good dose recovery (within ±5% of unity) can be obtained up to ～800 Gy. Otherwise, the dose recovery ratio deviates from unity. The D_e values also depend on the test dose size and so we conclude that the effect of test dose size should be routinely considered in pIRIR dating. First IR stimulation plateau pIRIR₂₉₀ results are compared with multiple elevated temperature ‐pIRIR (MET‐pIRIR) data. It appears that the low temperature MET‐pIRIR data are strongly affected by poor dose recovery, but this is not the case for the pIRIR₂₉₀ results. Natural signal measurements at the highest (first IR) stimulation temperature on a sample expected to be in field saturation suggest that ~10% signal loss occurs in pIRIR signals. Long‐term laboratory bleaching experiments (>80 days) show that a constant (or very difficult to bleach) residual pIRIR₂₉₀ signal is reached after ~300 h, corresponding to a dose of 6.2±0.7 Gy. Quartz OSL and feldspar pIRIR_50,290 ages are in good agreement at least back to c. 70 ka. Beyond this the quartz ages begin to underestimate but the feldspar ages are in agreement with the expected Last Interglacial age palaeosol.     

Timing of fluvial sedimentation in the Upper Rhine Graben since the Middle Pleistocene: constraints from quartz and feldspar luminescence dating

The Heidelberg Basin (HDB) hosts one of the thickest Quaternary sediment successions in central Europe. To establish a reliable Middle and Upper Pleistocene chronology for a recently drilled core from the depocentre of the Heidelberg Basin, we applied multiple luminescence dating approaches, including quartz optically stimulated luminescence (OSL), two feldspar post‐IR IRSL protocols using second IR stimulation temperatures of 225 °C (pIRIR₂₂₅) and 290 °C (pIRIR₂₉₀), and two fading correction models. Relatively high anomalous fading was observed for both the pIRIR₂₂₅ and pIRIR₂₉₀ signals, with mean fading rates of 2.13±0.27 and 2.08±0.49%/decade, respectively. Poor dose recovery behaviour of the pIRIR₂₉₀ signal suggests that the pIRIR₂₉₀ ages are not reliable. The comparison of two fading correction methods for the K‐feldspar ages indicates that the correction method proposed by Kars et al. (2008) Radiation Measurements 43, 786, yields reliable ages, whereas the dose‐rate correction method proposed by Lamothe et al. (2003) Radiation Measurements 37, 493, does not. A chronology for the HDB is established using the quartz ages and reliable fading corrected feldspar pIRIR₂₂₅ ages. Our chronology shows that the sediments in the upper Mannheim Formation were deposited during Marine Isotope Stage (MIS) 4 (c. 70 ka), constrained by two quartz ages in the upper 20 m of the core. Four fading corrected pIRIR₂₂₅ ages of c. 400 ka show that the upper Ludwigshafen Formation was deposited during MIS 12–11, correlated with the Elsterian‐Holsteinian stage. Two ages of 491±76 and 487±79 ka indicate that the Middle and Upper Ludwigshafen Formation were probably deposited during the Cromerian Complex. This luminescence chronology is consistent with palynological results. It also indicates that the IR‐RF ages reported earlier are probably underestimated due to anomalous fading.     

Stability of fine‐grained TT‐OSL and post‐IR IRSL signals from a c. 1 Ma sequence of aeolian and lacustrine deposits from the Nihewan Basin (northern China)

We tested the suitability of the fine‐grained quartz (4–11 μm) Optical Stimulated Luminescence (OSL) and thermally‐transferred OSL (TT‐OSL), and the fine‐grained polymineral (4–11 μm) post‐infrared IRSL (post‐IR IRSL or pIRIR) signals for dating samples from aeolian‐lacustrine deposits from the Xiaochangliang archaeological profile in the Nihewan Basin, China; these deposits include material from the Jaramillo subchron (c. 1.0 Ma). In the upper aeolian section, the OSL and pIRIR₂₉₀ ages are consistent with each other, and show that the upper 8.8 m was deposited between c. 0.3 and c. 140 ka. The luminescence ages indicate a major discontinuity in deposition between the aeolian and the older lacustrine deposits. Below this hiatus at 9.4 m (i.e. in the lacustrine sediments) all three signals are found to be in field saturation (no further systematic increase in burial dose with depth) despite the TT‐OSL signal (apparent mean burial dose ~880 Gy) being well below saturation on the laboratory growth curve. This is in contrast to the pIRIR₂₉₀ signal, which saturates in the field at a level consistent with laboratory saturation. This results in a practical upper limit to the measured burial dose of ~900 Gy (2D₀). Thus for the TT‐OSL and pIRIR₂₉₀ signals, the upper limits for dating lacustrine deposits are <260 ka and c. 240 ka, respectively. These results have major implications for the appropriate future application of these signals. The ages of our lacustrine samples cannot be regarded as necessarily accurate ones; nevertheless, these ages provide the first long series absolute chronology for study of local palaeolithic and geomorphic evolution history aside from the magnetostratigraphical results available before this research.     

洛川黄土细颗粒混合矿物红外释光信号 异常衰减的初步研究*

对洛川末次冰期的黄土细颗粒混合矿物红外释光(IRSL)信号异常衰减行为的初步研究结果表明: 1)预加热只能部分消除异常衰减对等效剂量测定的影响,不能完全消除这种影响,IRSL异常衰减过程也许存在着热效应和非热效应两种组分; 2)对16个已知年龄的马兰黄土(15~70ka)样品细颗粒混合矿物天然IRSL信号的ED值与期望ED值的比较初步显示,马兰黄土细颗粒混合矿物IRSL信号异常衰减不断发生,导致混合矿物IRSL的年龄测定值可能被低估达20 ％ 以上。     

The luminescence dating chronology of a deep core from Bosten Lake (NW China) in arid central Asia reveals lake evolution over the last 220 ka

The lacustrine deposits of lakes in arid central Asia (ACA) potentially record palaeoclimatic changes on orbital and suborbital time scales, but such changes are still poorly understood due to the lack of reliable chronologies. Bosten Lake, the largest freshwater inland lake in China, is located in the southern Tianshan Mountains in central ACA. A 51.6‐m‐deep lacustrine succession was retrieved from the lake and 30 samples from the succession were used for luminescence dating to establish a chronology based on multi‐grain quartz OSL and K‐feldspar post‐IR IRSL (pIRIR₂₉₀) dating. Quartz OSL ages were only used for samples from the upper part of the core. The K‐feldspar luminescence characteristics (dose recovery test, anomalous fading test, first IR stimulation temperature plateau test) are satisfactory and from the relationship amongst the quartz OSL, IR₅₀ and pIRIR₂₉₀ doses we infer that the feldspar signals are likely to be well bleached at deposition. Bacon age‐depth modelling was used to derive a chronology spanning the last c. 220 ka. The chronology, lithology and grain‐size proxy record indicate that Bosten Lake formed at least c. 220 ka ago and that lake levels fluctuated frequently thereafter. A stable deep lake occurred at c. 220, 210–180, c. 165, 70–60, 40–30 and 20–5 ka, while shallow levels occurred at c. 215, 180–165, 100–70, 60–40 and 30–20 ka. Bosten Lake levels decreased by at least ~29 m and possibly the lake even dried up between c. 160 and c. 100 ka. We suggest that the water‐level fluctuations in the lakes of ACA may not respond directly to climatic changes and may be affected by a number of complex factors.     

Hebei loess section in the Anyemaqen Mountains,northeast Tibetan Plateau: a high‐resolution luminescence chronology

The extensive aeolian deposits of the Tibetan Plateau (TP) represent important environmental archives, recording information about the past interplay between the Asian monsoon and Westerlies and the link between dust accumulation and Quaternary glaciations. In the northeast TP, mantles of sandy loess form a distinct belt lying between 3500 and 4500 m a.s.l. on the east‐facing slopes of the Anyemaqen Mountains. However, there is little chronological information about the loess deposits in this region. This study provides a detailed chronology for loess formation in the region using luminescence dating. A total of 29 samples were collected from an 8‐m‐thick homogeneous loess section at Hebei (HB) in order to date sand‐sized (63–90 μm) quartz and K‐feldspar fractions using optically stimulated luminescence (OSL) and infrared stimulated luminescence (IRSL and pIRIR) signals, respectively. The resulting quartz and feldspar ages are in good agreement over the last 40 ka; beyond this (i.e. D_e >120 Gy), the quartz age is underestimated, and the pIRIR₁₇₀ feldspar ages are considered more reliable. The HB loess section records continuous environmental information from c. 50 to c. 30 ka, i.e. throughout Marine Isotope Stage (MIS) 3. Mass accumulation rates (MARs) varied considerably over this period with increased dust accumulation around c. 38 ka and after c. 32 ka; in between, and at the beginning of MIS 3 (50–40 ka), the dust accumulation rate was ~50% lower. Finally, the HB section also records a MIS 2 hiatus of c. 17 ka duration, probably resulting from deflation. This study implies that loess deposition on the TP is predominantly an interglacial/interstadial phenomenon and the TP may be deflating at the same time as the Chinese Loess Plateau is accumulating, at least during MIS 2.     

A chronological and palaeoenvironmental re-evaluation of two loess-palaeosol records in the northern Harz foreland,Germany, based on innovative modelling tools

The continuing development of analytical methods for investigating sedimentary records calls for iterative re-examination of existing data sets obtained on loess-palaeosol sequences (LPS) as archives of palaeoenvironmental change. Here, we re-investigate two LPS (Hecklingen, Zilly) in the northern Harz foreland, Germany, being of interest due to their proximity to the Scandinavian Ice Sheet (SIS) and the position between oceanic climatic influence further west and continental influence towards the east. First, we established new quartz OSL and polymineral IRSL chronologies. Both methods show concordant ages in the upper part of the Hecklingen profile (~20–40 ka), but in the lower part IRSL underestimates OSL ages by up to ~15 ka for the period 40–60 ka. Interpretations hence refer to the OSL data set. Second, we applied Bayesian age-depth modelling to data sets from Hecklingen to resolve inversions in the original ages, also reducing averaged 1σ uncertainty by ~19% (OSL) and ~12% (IRSL). Modelled chronologies point out phases of increased (MIS 2, early MIS 3) and reduced (middle and late MIS 3) sedimentation, but interpretation of numerical rates is problematic because of intense erosion and slope wash particularly during MIS 3. Finally, previously obtained grain-size data were re-investigated by end member modelling analyses. Three fundamental grain-size distributions (loadings) explain the measured data sets and offer information on intensity and – combined with modelled OSL ages – timing of geomorphic processes. We interpret the loadings to represent (i) primary loess accumulation, (ii) postdepositional pedogenesis and/or input of aeolian fine fractions, and (iii) input of coarse aeolian material and/or slope wash. The applied modelling tools facilitate detailed understanding of site-formation through time, allowing us to correlate a strong peak in mean grain size at ~26–24 ka to the maximum extent of the SIS and increased influence of easterly winds.     

Chronology and the upper dating limit for loess samples from Luochuan section in the Chinese Loess Plateau using quartz OSL SAR protocol

Luminescence dating of loess older than 100 ka has long been a challenge. It has been recently reported that, using optically stimulated luminescence (OSL) of fine-grained quartz (4–11 μm) extracted from loess, the range of luminescence dating could be pushed to 0.6 Ma with OSL ages being in agreement with independent ages [Watanuki, T., Murray, A.S., Tsukamoto, S., 2005. Quartz and polymineral luminescence dating of Japanese loess over the last 0.6 Ma: comparison with an independent chronology. Earth and Planetary Science Letters 240, 774–789]. The aim of this study is to provide a luminescence chronology (20 samples) for the standard Luochuan loess section, and to further examine the upper limit of quartz OSL dating for Chinese loess. The growth curve does not saturate at 700 Gy, and should allow reliable equivalent dose (D_e) determination up to at least 400 Gy. However, when compared with independent chronological control, the D_e that could be treated as reliable is less than 230 Gy (corresponding to 70 ka in age for Chinese loess), and the D_e larger than 230 Gy should be underestimated. Ages for samples from the lower part of palaeosol S1 are severely underestimated, with the maximum age of 95 ka for a sample from the bottom of this palaeosol, much younger than the expected age of 128 ka. The maximum D_e obtained for sample L9/M, collected from loess layer L9 which is below the Matuyama–Brunhes (B/M) boundary whose age is 780 ka, is only 403 Gy which corresponds to an age of 107 ka. The cause of underestimation is not yet clear. The previous results by Watunuki et al. (2005) on the extension of OSL dating of loess to 0.6 Ma is not confirmed. When evaluating the validity of OSL ages in S1, another possibility is to question the already established chronological frame for Luochuan section, which is based on the hypothesis of continuous dust deposition. The assumption of an erosion hiatus between L2 and S1 could make the OSL ages look reasonable. However, if this is the case, then it is difficult to explain why the age of sample L9/M is only 107 ka which could be treated as a saturation age, while the OSL can provide a correct age for loess as old as 94.9 ka for sample LC22 collected from the bottom of S1. Much work is required to clarify these confusions.     

OSL dating of a Holocene loess-paleosol sequence in the southern Loess Plateau,China

Optically stimulated luminescence (OSL) dating of polymineral fine-grained loess samples collected from the southern Loess Plateau of China was conducted using the single-aliquot regenerative-dose (SAR) protocol. A ‘Double-SAR’ procedure in which aliquots are subjected to both infrared (IR) and blue stimulations was used, and two sets of equivalent dose (D _e ) determinations were produced. These doses are assumed to be predominantly related to the feldspathic and quartz fine grain populations, respectively. The results revealed that the OSL ages estimated by infrared stimulated luminescence (IRSL) signals and those estimated by [post-IR] stimulated luminescence ([post-IR] OSL) signals disagreed. Specifically, the ages estimated using the IRSL signals were smaller than those estimated using [post-IR] OSL signals. The results of an anomalous fading test of the two types of OSL signals revealed that the [post-IR] OSL signals from the etched sub-sample (by H₂SiF₆ and HF) and the un-etched sub-sample did not fade significantly. However, the IRSL signals from the un-etched sub-sample showed obvious signs of fading. These findings indicate that the lower age estimated by IRSL is due to the anomalous fading of feldspar IR signals in the polymineral fine grains. For samples collected from greater than 100 cm, the estimates of their OSL ages using two types of luminescence signals generally agreed with their pre-estimated ages, especially those of the [post-IR] OSL signals. However, for the three samples that were collected from a depth of less than 100 cm, their OSL ages were remarkably underestimated, possibly due to the enhanced human activity (such as soil cultivation) that has occurred in the region since 3000 a B.P.     

Luminescence dating of lacustrine sediments from Tangra Yumco (southern Tibetan Plateau) using post‐IR IRSL signals from polymineral grains

Radiocarbon dating of bulk organic matter is the most commonly used method for establishing chronologies of lake sediments for palaeoclimate reconstructions on the Tibetan Plateau. However, this method is likely to be problematic because the dated material often suffers from old carbon contamination. Recently, advances in luminescence‐based chronological techniques have provided new options for dating lacustrine sediments. In the current study, we tested for the first time the applicability of a new post‐IR IRSL (pIRIR) measurement protocol for dating fine‐grained polymineral material from a deep‐lake sediment core from the central part of Tangra Yumco, on the southern Tibetan Plateau. Our results show that: (i) radioactive disequilibria in the uranium decay chain were observed in the studied lake sediments, and thus taken into account for dose rate calculation by using a dynamic modelling approach; (ii) the suitability and robustness of the pIRIR protocol measured at 150°C (pIRIR₁₅₀) for our samples are confirmed by a set of luminescence characteristic tests as well as the agreement with an independent age control; (iii) turbidite deposition partly caused an insufficient resetting of luminescence signals and thus apparent overestimation in luminescence dating; (iv) compared with the luminescence‐based age‐depth model, the ¹⁴C ages of bulk organic matter from the studied core generally yielded an age difference of ～2 ka, which is attributed to hardwater reservoir effects in Tangra Yumco. This study highlights the need for multi‐dating approaches of lake sedimentary archives on the Tibetan Plateau.     

Chronologies of sedimentary changes in the south Bohai Sea,China: constraints from luminescence and radiocarbon dating

The alternation of terrestrial and marine deposits is an indicator of past environmental and sea‐level changes. The age of deposition is usually dated by means of radiocarbon. However, radiocarbon dates of molluscan shells from coastal areas may be complicated by various sources of carbon, and problematic for deposits of 40–50 ka or older. Herein, we apply the Optically Stimulated Luminescence (OSL) dating method to date samples from terrestrial and marine/coastal sediments extracted from three cores in the south Bohai Sea, China. Multiple‐ and single‐aliquot regenerative‐dose procedures using OSL signals from fine‐silt (4–11 μm), coarse‐silt (38–63 μm) and fine‐sand (63–90 or 90–125 μm) quartz were employed to determine the equivalent dose (D _e). The results showed that: (i) OSL ages from quartz of different grain sizes and different protocols are consistent with each other; (ii) for Holocene samples, most of the radiocarbon dates agree well with OSL ages; (iii) for pre‐Holocene samples, radiocarbon dates cluster at 40–50 ¹⁴ C ka BP, whereas OSL ages are in stratigraphic order from 11 ka to 176 ka. Because of the self‐consistency of the quartz OSL ages, the stratigraphic agreement in the three cores, and the clustering of the radiocarbon dates, we suggest that the quartz OSL ages are more reliable with respect to dating the samples from the south Bohai Sea. Finally, the four marine strata identified in the south Bohai Sea are likely to have formed during the Holocene, Marine Isotopic Stage (MIS) 3–5, MIS 6 and probably MIS 7, respectively.     

New insights on Illinoian deglaciation from deposits of Glacial Lake Quincy, central Indiana

The deposits of Glacial Lake Quincy overlie a diamicton associated with the classically defined Illinoian limit in central Indiana. This lake covered at least 180 km² with a depth of > 20 m and developed when the Illinoian ice sheet retreated 15 km from the maximum limit, causing lake impoundment against Devore Ridge. Overflow from Glacial Lake Quincy eroded across the ridge forming a number of steeped-walled outlets. A section along Mill Creek exposes a sedimentologic sequence associated with Glacial Lake Quincy from a subglacial diamicton to ice-proximal to ice-distal glacial lacustrine sediments. We report new optical ages by multiple aliquot regenerative dose procedure for the fine-grained rhythmically bedded sediments presumed to represent the lowest energy depositional facies, dominated by suspension settling, which maximized sunlight exposure. In turn, optical ages were determined on the fine-grained (4-11 μm) polymineral and quartz fractions under infrared and blue excitation, which yielded statistically similar ages. Optical ages span from ca. 170 to 108 ka, with the average of 16 optical ages indicating deglaciation at ca. 135 ka, generally coincident with Marine Oxygen Isotope Stage 6-to-5 transition and rise in global sea level.     

Comparison of SAR techniques for luminescence dating of sediments derived from volcanic tuff

In this investigation we evaluate several proposed optically stimulated luminescence single-aliquot regeneration (OSL SAR) procedures to determine which technique has the greatest potential to yield accurate ages for samples collected from tuff-derived alluvial sediments within the narrow, sharply incised canyon systems of the Pajarito Plateau of northern New Mexico. The SAR data collection methods evaluated are: infrared-stimulated luminescence (IRSL), post-IR blue-OSL, IRSL with TL annealing cycles on polymineral fine-grains, and blue-OSL on quartz fine sand. A single-grain laser luminescence (SGLL) procedure for quartz sand is also evaluated. Age estimates obtained from these methods are compared with radiocarbon, soil PDI (profile development index), and IRSL multi-aliquot additive dose (MAAD) age constraints. Our results indicate that the modal D_e of quartz sand SGLL dose distributions yield ages that are consistent with radiocarbon and PDI age constraints for the tuff derived sediments in this investigation and appears to be the most promising method for studies in this area. Additionally, two fine-grained polymineral methods, IRSL SAR and traditional IRSL MAAD, produced ages that were generally in agreement with the SGLL ages and with available ¹⁴C and PDI age constraints. At the present stage of research, we advocate using quartz sand SGLL in conjunction with IRSL SAR or even IRSL MAAD for polymineral fine-grains to provide the most robust and reliable luminescence age data sets for tuff-derived sediments.     

Alternative chronologies for Late Quaternary (Last Interglacial–Holocene) deep sea sediments via optical dating of silt-sized quartz

We summarize the results of a test on the potential of optical dating for the age assessment of Late Quaternary deep-sea sediments. Our approach combines a single aliquot regeneration (SAR) protocol for equivalent dose (D_e) estimation on fine silt-sized quartz with a time-dependent evaluation of supported and unsupported long-lived radioisotopes within the deposited sediment matrix. For this purpose nine samples from two independently dated deep-sea cores from the Indian Ocean were obtained. The SAR analysis resulted in mean D_e estimates with precisions ranging from 0.9% to 3.7%. Combination of these data with measured radioisotope concentrations resulted in stratigraphically sensible ages ranging from ca 7 to 120 ka. These ages exhibit good agreement with existing chronologies for the cores based on radiocarbon age determinations and correlation of key volcanic, palaeoecological and isotopic events. Optical dating may provide an important additional dating method for Late Quaternary deep-sea sediments.     

沙漠边缘厚层黄土上部光释光测年的初步研究*

对处于中国西北黄土高原沙漠边缘曹岘厚层黄土剖面上部进行了光释光年代初步研究。实验结果表明,45~63μm石英颗粒的光释光信号以快组分为主,适合应用单片再生剂量法(SAR)测年。在自然和再生剂量预热温度为260℃持续10秒,检测剂量预热温度为160℃持续0秒的条件下,石英单片再生剂量法获得的光释光年龄随样品深度而增加。但是,剖面底部S₁古土壤和L₂顶部黄土样品的光释光年龄仅为69.1±5.5ka和72.0±4.6ka,表现出30 ％ ~50 ％ 的年龄低估。利用多片再生剂量法(MAR)得到的年龄与SAR方法所得年龄无显著差异,即出现了类似的年龄低估现象。在20.1~18.8ka时段内,该剖面的沉积速率超过500cm/ka。末次冰盛期的寒冷气候,与沙漠的距离以及近邻黄河的地貌特点共同造成了如此高的沉积速率。     

Multiple and single aliquot luminescence dating techniques applied to quartz extracted from Middle and Upper Weichselian loess,Zemechy, Czech Republic

This paper reports the application of optically stimulated luminescence (OSL) dating to relatively coarse grains (100–200 μm) of quartz extracted from loess. Two approaches were tested – a multiple aliquot technique and a new single aliquot approach, which is especially suited to the dating of small quantities of such grains found in some loess. The results are compared with infra‐red stimulated luminescence and thermoluminescence (TL) measurements on the finer‐grained (4–11 μm) polymineral fraction and TL measurements on the relatively coarse grains of quartz. The advantages of the new single aliquot (OSL) approach are described and the iterating, computer‐controlled measurement procedure is given. The automated iterative single aliquot regeneration (AISAR) method corrects for changes in luminescence sensitivity during the measurement sequence by monitoring the response to a test dose. Some initial measurements are presented for the loess section at Zemechy, Czech Republic, and these show that the AISAR method gives more precise results than those using a multiple aliquot method. Copyright © 2000 John Wiley & Sons, Ltd.     

博斯腾湖湖泊沉积物光释光年代测量*

使用光释光年代学的单片再生法测量了博斯腾湖沉积剖面中碳酸盐泥及粉砂质泥底部的浅湖相灰色粉细砂和风成沙的年龄,对剖面上部碳酸盐层中陆生植物残体进行了AMS ¹⁴ C测年。通过不同测片的等效剂量(D_e)值的分布状况评价了样品的晒褪程度,选择不随灵敏度校正后的自然释光信号变化的相对集中的等效剂量(D_e)值计算了样品的埋藏年龄。通过这些年龄结果的对比,发现石英矿物的OSL年龄和AMS ¹⁴ C年龄在地层上是一致的,表明尽管在浅湖相细砂中存在不完全晒褪,但根据相对较小而集中的D_e值计算得到的年龄结果是可靠的。这些年龄结果和地层资料揭示末次冰消期以来至早全新世,博斯腾湖处于无水干盆地向深水湖泊转化的浅水湖泊状态,现代深水博斯腾湖大约形成于距今8ka前后。     

A post-IR IRSL chronology and dust mass accumulation rates of the Nosak loess-palaeosol sequence in northeastern Serbia

In the Middle Danube Basin, Quaternary deposits are widely distributed in the Vojvodina region where they cover about 95% of the area. Major research during the last two decades has been focused on loess deposits in the Vojvodina region. During this period, loess in the Vojvodina region has become one of the most important Pleistocene European continental climatic and environmental records. Here we present the dating results of 15 samples taken from the Nosak loess-palaeosol sequence in northeastern Serbia in order to establish a chronology over the last three glacial–interglacial cycles. We use the pIRIR₂₉₀ signal of the 4–11 μm polymineral grains. The calculated ages are within the error limits partially consistent with the proposed multi-millennial chronostratigraphy for Serbian loess. The average mass accumulation rate for the last three glacial–interglacial cycles is 265 g m⁻² a⁻¹, which is in agreement with the values of most sites in the Carpathian Basin. Our results indicate a highly variable deposition rate of loess, especially during the MIS 3 and MIS 6 stages, which is contrary to most studies conducted in Serbia where linear sedimentation rates were assumed.     

A luminescence‐based chronology for the Harletz loess sequence,Bulgaria

The Harletz loess‐palaeosol sequence is located in northwestern Bulgaria and represents an important link between well‐studied loess sequences in eastern Romania and further sites to the west of the Carpathians (e.g. Serbia and Hungary). The aim of this study was to establish a chronostratigraphy of the deposits, using various methods of luminescence dating, together with basic stratigraphical field observations as well as magnetic properties. Luminescence dating was carried out using the quartz fine grain fraction and a SAR protocol, and the feldspar coarse grain fraction, applying the MET‐pIRIR protocol. Due to underestimation of the quartz fine grain fraction in the lower parts of the sequence, the resulting chronology is mainly based on the feldspar ages, which are derived from the stimulation temperature at 150 °C. A comparison with nearby sequences from Serbia, Hungary and Romania, and interpretations obtained through the stratigraphical and sedimentological signature of the sequence, supports the established chronology. Our data suggest that the prominent palaeosol (soil complex) in the upper quarter of the sequence was formed during MIS 5. It would follow that large parts of the Last Glacial loess overlying this palaeosol were probably eroded, and that the thick loess accumulation underlying this soil complex can be allocated to the penultimate glacial (MIS 6). A prominent MIS 6 tephra, which has been reported from other sequences in the area, is also present at Harletz.     

Sand dunes as a major proximal dust source for late Pleistocene loess in the Negev Desert, Israel

Grain size analyses of three hilltop, primary eolian loess sequences in the Negev desert, southern Israel, show a bimodal grain-size distribution at 50-60 μm and 3-8 μm. Using analyses of mineralogy and OSL ages we demonstrate that the coarse mode is composed mostly of quartz grains and its relative magnitude increases regionally with time, suggesting an enhancement of a time-transgressive proximal dust source compared to a distal, Saharan fine-grain dust. The only proximal dust source for large amount of coarse silt quartz grains is the sands that advanced into Sinai and the Negev concurrently with the loess accretion during the late Pleistocene as a result of the exposure of the Mediterranean shelf. We therefore propose that the coarse silt quartz grains were formed through eolian abrasion within the margins of an advancing sand sea. This relationship between desert sand seas as a source for proximal coarse dust and desert margin loess deposits can be applicable to other worldwide deserts such as Northern Africa, China and Australia.