Luminescence dating of loessic sediments from the Loess plateau, China

Loess/palaeosol sequences from the Loess plateau in China were investigated by combined infrared optically stimulated luminescence (IRSL) and thermoluminescence (TL) dating techniques in order to study the luminescence properties of the loessic sediments and to provide a direct chronological link for correlation and position of the last interglacial soil in Central Asia and the Loess plateau in China. Sensitivity changes were found for all samples through artificial bleaching of the samples. The greatest sensitivity changes, of up to 50%, were found for very old loess samples designated to be older than the Matu-yama/Brunhes magnetic boundary and hence older than 788,000±1,800 years. The upper dating limit, as investigated by the very old loess samples, ranges from 250,000 to 300,000 years, if the TL additive dose method is applied. The chronological position of the last interglacial soil S1 at the section near Lanzhou indicates luminescence age estimates ranging from 82,000 to 75,000 years for the marine-isotope stage 5 to 4 transition. However, the loess from below S1 yielded luminescence age estimates between 153,200±14,200 and 110,100±20,100 years for TL and IRSL additive dose methods, respectively. Thus, a direct correlation between the S1 and the first intercalated pedocomplex PC1 in Central Asia is most likely. Received: 31 March 1998 / Accepted: 25 October 1998     

Geochronology of Middle and Upper Pleistocene Loess Sections in Hungary

The application of both thermoluminescence and infrared stimulated luminescence dating to the extensively studied “classical” Hungarian loess/paleosol sequences from Basaharc, Mende, and Paks provides a reliable chronological framework and climatostratigraphic reconstruction for the last interglacial/glacial cycle. Based on this combined luminescence dating study a new chronology is proposed for the “Young Loess” in Hungary. Luminescence dating suggests that the loess below the MF2 horizon formed during the penultimate glaciation. The MF1 horizon probably formed during an interstade within oxygen isotope stage 3. For the youngest loess, overlying MF1, a very high accumulation rate was determined. Large time gaps occur above MF2 and MF1, indicating that most of the record of the last glaciation is missing in the standard sections at Basaharc, Mende, and Paks. Either large discontinuities or a very low accumulation rate occurred in all three type sections during the soil-forming periods. High-resolution studies of climatic proxies using this combined luminescence dating approach provide a reliable chronological framework for loess and loess derivatives of the last glacial cycle in Hungary, although a precise and complete chronostratigraphic reconstruction cannot be achieved from the incomplete records found at these sites.     

末次盛冰期北美风成环境变化及其在全球气候突变事件中的意义

本文用末次冰期北美大冰盖南缘的风尘堆积记录来重建末次盛冰期的亚极地环境变化.磁化率、有机碳含量和潜育化程度的资料表明,末次盛冰期的前期(约21000～15000aB P.)植被覆盖较差,而后期(15000～10000aB.P.)植被覆盖较好,15 000aB.P.环境发生了急剧的变化,磁化率曲线显示了大约1000a的氧化-还原周期.这种大约1000a的环境变化周期很可能由低纬地区的海洋和大气的扰动所驱动,这种扰动的能量通过北美大冰盖及时地传递到北大西洋.     

Chronology of late Pleistocene Pampa loess from the Córdoba area in Argentina

In Argentina, loess/palaeosol sequences were studied from the two sections at Monte Ralo and Corralito, located near to the city of Córdoba in the east of the Pampean ranges. Infrared optically stimulated luminescence (IRSL) and thermoluminescence (TL) dating techniques were applied to set up a more reliable chronological framework for the Upper Pleistocene loess record. IRSL ages increase with depth and are stratigraphically consistent. The oldest loess exposed correlates at least to the penultimate glaciation. The luminescence dating study gives evidence for humid climate conditions with soil formation during the last interglacial period and the middle pleniglacial correlating to Marine Isotope Stage (MIS) 5 and 3, respectively. Three extended periods of soil formation are recorded in the loess/palaeosol sequences at the Corralito section. These buried soils most likely correlate with the last interglacial and early last glacial period. During the Middle Pleniglacial, two palaeosols are intercalated in the loess successions. In the Córdoba area, the periods of increased loess accumulation and deposition of loessic sediments correlate with more arid and glacial periods during the Early Pleniglacial, the Middle Pleniglacial and the Late Glacial. Copyright © 2009 John Wiley & Sons, Ltd.     

渭南黄土剖面十五万年以来的主要地层界线和气候事件──年代学方面的证据

本文在渭南黄土剖面所测得的年龄结果和时间标尺研究的基础上，结合粒度、磁化率等气候曲线的分析，对该剖面十五万年以来一些主要地层界线和气候事件的年龄进行了初步讨论，结果如下：１)Ｓ１／Ｌ２界线位于剖面１１８０ｃｍ处，从时间标尺上可知其年龄为１２８８００ａＢ．ｐ．，同末次间冰期起始的年龄相一致；２)Ｌ１／Ｓ１的地层界线年龄为７４２２０ａＢ．Ｐ．，同ＳＰＥＣＭＡＰ曲线中末次间冰期的结束年龄相吻合；３)渭南剖面所指示的末次盛冰期约在２００００～１８０００ａＢ．Ｐ．之间；４)在２００００～１８０００ａＢ．Ｐ．之间的末次盛冰期，有一段不足１０００ａ的快速堆积期，其堆积速率是中国黄土平均堆积速率的１０倍以上。     

Luminescence chronology of the Upper Pleistocene loess record at Kurtak in M iddle Siberia

The loess/palaeosol sequence of Kurtak, situated at the western bank of the upper Yenisei in Middle Siberia, represents one of the best developed Middle and Upper Pleistocene sediment records in Yenisei Siberia. More than 40 m thick loess and loess-like sediments intercalated by at least four pedocomplexes are exposed at a steep erosional slope at the bank of the Krasnoyarsk Water Reservoir. Infrared optically stimulated luminescence (IRSL) and thermoluminescence (TL) dating techniques have been applied on 38 fine grain samples from the upper 23 m of the profile, representing the penultimate and last interglacial–glacial cycle. The IRSL and TL age estimates are in good agreement with the geological estimates up to the last interglacial soil horizon (oxygen isotope substage (OIS) 5e). The luminescence ages show that the lowermost truncated palaeosol of kastanosjem-type is likely to have formed during the penultimate interglacial upon subaerial deposits. Three weak reddish brown palaeosols intercalated by reworked loess-like sediments correlate with early Upper Pleistocene interstadials (OIS5dion of -a), and a succession of humic horizons alternated by cryoturbation processes (Kurtak pedocomplex) is linked with OIS 3. Thick loess deposits between the pedocomplexes show now significant age increase with depth, indicating high accumulation rates at around 23 ka (OIS 2) and 60 ka (OIS 4).     

Typical Geochemical Elements in Loess Deposit in the Northeastern Tibetan Plateau and Its Paleoclimatic Implication

Widespread and thick loess deposit in the northeastern Tibetan Plateau records paleoclimatic changes over the Quaternary period. In this study, we investigate a loess section located in a high terrace of the Huangshui River in the Xining Basin, and collect samples at 20-cm intervals by digging a well of 16-m depth （including paleosol S1 and SO and several loess interlayers over the last glacial-interglacial cycle and the Holocene）. Concentration of some active elements （Sr and Ca） and inert elements （Rb, Zr, Ti） in these loess samples are measured. The results show that ratios of those elements （oxide）, such as Rb/Sr, Ti/Sr, and Zr/CaO ratios, would indicate sensitively paleoclimatic changes, especially the history of precipitation over the last glacial-interglacial and the Holocene. Moreover, the curves of Rb/Sr, Ti/Sr, and Zr/CaO ratios had almost the same variable trends from the bottom to the top and also closely correlated with values of magnetic susceptibility and the global marine δ^18O record. But compared with the curves of magnetic susceptibility, the changes of ratios of these elements （oxide） are clearer and easy to understand. Therefore, the ratios of these typical chemical elements in the loess deposit may be used as an excellent index to investigate the history of paleoclimate, particularly precipitation changes in the northeastern Tibetan Plateau.     

Advances and Issues in Luminescence Dating of Loess Deposits in Arid Central Asia

High-resolution loess deposits are widely distributed in Arid Central Asia (ACA) and provide important records associated with dust transportation, paleoenvironmental and paleoclimatic evolution. The chronology is the foundation of the research into loess deposits as an environmental archive. In recent decades, the gradually developed optical dating method has been increasingly matured and become an important approach to establishing the loess-paleosol sequences. Here, we summarized and discussed previous work on loess chronology mainly based on optical dating approach in ACA. The following understandings have been listed: ① In comparison with optical dating method, the suitable material for ¹⁴C dating is uncommon in ACA. However, the dating range of luminescence dating is more extensive, and the dating materials are accessible. Thus, the optical dating is widely applicable in the establishment of loess framework in this area. ② Until now, the quartz Single Aliquot Regeneration (SAR) method can be applied to the establishment of loess-paleosol sequence since last glacial period. But several issues remain unaddressed. For example, the Optically Stimulated Luminescence (OSL) signal sensitivity of quartz grains are low in some areas. Furthermore, the results of OSL dating of different grain sizes within a single sample are inconsistent in some areas. The solution of these problems still requires more methodological research. ③ The post-IR IRSL (pIRIR) and multiple elevated temperature stimulation (MET-pIRIR) protoCols of feldspar have basically overcome the anomalous fading issue in the traditional IRSL dating process. In ACA, the framework since MIS 7 can be established with K-feldspar luminescence dating method. Compared with quartz luminescence characteristics, the K-feldspar luminescence signals are more sensitive and exhibit a high saturation level. In specific applications, it is necessary to establish the age frame according to the luminescence sensitivity, the age of samples or other factors.     

Late Quaternary aeolian dust input variability on the Chinese Loess Plateau: inferences from unmixing of loess grain-size records

The grain-size distributions (GSDs) of loess–paleosol sequences may provide valuable information on provenance, transport and paleoclimate variability, and consequently, a wide range of methods to extract genetic information from loess GSDs has been proposed. Here it is shown that a genetically meaningful decomposition of a series of Late Quaternary loess grain-size records extending across the Chinese Loess Plateau can be accomplished with the end-member modelling algorithm (EMMA). The unmixing results in conjunction with loess accumulation rate estimates reveal that two contrasting dust supply patterns were active over the Loess Plateau during the last glacial–interglacial cycle: (i) a background sedimentation pattern that was dominant during interglacial periods, especially over the central and southern parts of the Loess Plateau, is reflected by the constant flux of the fine-grained loess component, (ii) an episodic, highly variable dust input pattern, that was dominant during glacial periods throughout the Loess Plateau and noticeable during interglacial periods mainly over the northern Loess Plateau and almost disappearing over the southern Loess Plateau, is reflected in the admixture of two coarse-grained loess components. A genetic interpretation and the paleoclimatic significance of the mixing model are provided by comparison of the modelled end members with modern dust samples in terms of their GSD and flux rates.     

Dust deposition and climate in the Carpathian Basin over an independently dated last glacial–interglacial cycle

Loess in the Carpathian Basin is some of the thickest and most complete in Europe. Located in the Vojvodina region of the southern Carpathian Basin the Crvenka loess-palaeosol section appears to preserve a detailed climate proxy archive of the last glacial–interglacial cycle. Central to the interpretation of the site is a detailed and independent age model. Here, the results of detailed optically stimulated luminescence (OSL) dating and elevated temperature post-IR infrared stimulated luminescence (post-IR IRSL) dating are presented. Quartz OSL ages appear accurate to about 50–60 ka, where 2D₀ values are reached, while elevated temperature post-IR IRSL yields more accurate ages below this. In line with recent results, the latter signal appears to show negligible fading rates. Two age models are developed that combine (a) OSL and post-IR IRSL ages and (b) OSL ages and ‘expected’ ages from tying unit boundaries to the marine record. If the luminescence model is regarded as accurate, differences between this and the OSL/marine age model raise questions over the accuracy of the latter, as well as the processes controlling the zeroing of luminescence dates. The luminescence based age model is then used to derive the first fully independent reconstruction of climate proxies and accumulation rates from Carpathian loess. Such reconstructions can be used to compare to other independent records without assumptions inherent in correlation-based approaches. The findings demonstrate how variable accumulation rate is at the site, and compared to other independently dated Carpathian loess records. Average values vary north–south but are of similar order throughout the basin. Accumulation rate was highest during the later part of the last glacial, but variation on millennial timescales does not always match shifts in grain-size, suggesting diverse and complex influences. Environmental reconstructions using grain-size and magnetic susceptibility show that no one atmospheric system or air mass can explain the changes in the Carpathian Basin and that millennial-scale variability can only intermittently be tied to North Atlantic Heinrich events. Expanded ice sheets during the peak last glacial, combined with other atmospheric teleconnections, may have served to develop a strong anticyclone in the region. It was likely windier during earlier parts of the last glacial, but Atlantic and Mediterranean moisture was probably less abundant than during more humid interglacials.     

A new OSL chronology for dust accumulation in the last 130,000 yr for the Chinese Loess Plateau

A sensitivity-corrected Multiple Aliquot Regenerative-dose protocol has been developed for fine-grained quartz OSL dating of Chinese loess. Its reliability has been assessed on the basis of the methodology and by dating reference samples of known age close to the transition from the last interglacial paleosol (S₁) to the last glacial loess (L₁), which corresponds to the Marine Oxygen Isotope Stage (MIS) 5/4 transition. On the basis of the fine-grained quartz OSL-age estimates for 33 loess samples from the upper part of the Luochuan profile, a detailed chronostratigraphy of continuous dust accumulation in the past 130 ka has been proposed. Changes in the accumulation rate occurred during the last glacial period (MIS 4 to MIS 2); unexpectedly, high accumulation rates were found in the weakly developed L_1-2(S) paleosol of the last interstadial (MIS 3), rather than in the classic L_1-1 and L_1-3 loess of the cold-dry glacial condition (MIS 2 and 4). The OSL ages show some disagreement with the previous numerical chronology for the loess-paleosol sequence based on correlation of variations in grain size with sedimentation rate; the latter method resulted in an almost constant accumulation rate from 72 to 12 ka.     

天山北麓黄土记录的30万年以来古气候演变

对天山北麓黄土分布特点与形成年代的研究,以及以此为载体应用各代用指标的古气候重建已经取得了不少进展。在前人工作的基础上,选取黄土—古土壤序列分明,底部S3古土壤发育的鹿角湾剖面为主要研究对象,结合天山北麓的其他多个典型黄土剖面,运用色度、粒度、常量地球化学元素含量和环境磁学参数等指标,探讨大约30万年以来的古气候演变。鹿角湾黄土实验结果显示,各古气候代用指标随剖面深度变化与黄土—古土壤更替大概一致,剖面上部（L2及其以上）与下部区别明显。粒度分布揭示黄土物源输入主要受控于两股不同风系,随黄土古土壤的更替两者的主次地位发生变化。环境磁学实验结果显示,剖面下部磁性弱,频率磁化率低,但古土壤层稳定单畴含量较高,反映湿润成壤环境下超顺磁亚铁磁性矿物溶解或转化为弱磁性矿物;剖面上部比剖面下部的磁性要强,磁性矿物粒度更粗;S0为磁性成壤增强模式,与其他黄土古土壤层不同。再结合其他典型剖面的记录,可以推断研究区30万年以来有干旱化的趋势,但S2发育阶段总体上可能比S3发育阶段略为湿润,这一阶段之后气候明显变干,S1发育阶段明显比S2与S3发育阶段干旱,干旱化趋势一直保持至全新世开始之前。     

Mangshan Loess in Central China and the Paleomonsoon Variationssince the Last Interglaciation

The Mangshan Yuan is a loess platform on the southern bank of the Yellow River, which is located in northwestern Zhengzhou of Henan Province, China. The typical Zhaoxiayu section of the Mangshan Yuan preserves stratigraphical loess units above S10 with a total thickness of 172.1 m, which includes 15.7 m of the last interglacial paleosol S1, 77.3 m of the last glacial loess L1 that consist of 41.6 m of the late stade L1LL1, 13.2 m of the interstade L1SS1 and 22.5 m of the early stade L1LL2. Based on the age marking points by correlating magnetic susceptibility of the section with the SPECMAP curve, the timescale of the section was constructed, and the average accumulation rate and the resolution of each loess strata over the S2 were subsequently calculated using the     

Loess sedimentation in Tibet: provenance,processes, and link with Quaternary glaciations

Well-preserved loess deposits are found on the foothills of mountains along the middle reaches of the Yarlung Zangbo River in southern Tibet. Optically stimulated luminescence (OSL) dating is used to determine loess ages by applying the single-aliquot regeneration technique. Geochemical, mineralogical, and granulometric measurements were carried out to allow a comparison between loess from Tibet and the Chinese Loess Plateau. Our results demonstrate that (i) the loess deposits have a basal age of 13–11 ka, suggesting they accumulated after the last deglaciation, (ii) loess in southern Tibet has a “glacial” origin, resulting from eolian sorting of glaciofluvial outwash deposits from braided river channels or alluvial fans by local near-surface winds, and (iii) the present loess in the interior of Tibet has accumulated since the last deglaciation when increased monsoonal circulation provided an increased vegetation cover that was sufficient for trapping eolian silt. The lack of full-glacial loess is either due to minimal vegetation cover or possibly due to the erosion of loess as glaciofluvial outwash during the beginning of each interglacial. Such processes would have been repeated during each glacial–interglacial cycle of the Quaternary.     

A 180 ka record of environmental change at Erdut (Croatia): a new chronology for the loess–palaeosol sequence and its implications for environmental interpretation

While there are numerous thick loess–palaeosol sequences preserved across the Carpathian Basin, well dated sites that provide terrestrial palaeoenvironmental records extending beyond last glacial–interglacial cycle are scarce. Robust chronologies are essential for correlations of loess with other long-term Quaternary records and to further understanding of the palaeoenvironment and climate of this important region beyond the last 125 ka. Here a new geochronology based on 13 post-infrared infrared stimulated luminescence ages focused on the lower part of the loess–palaeosol sequence at Erdut is presented. The results show that the lower part of the Erdut profile spans the penultimate glacial cycle (MIS 7 to MIS 5). The considerable sediments overlaying the investigated part of the profile suggest that this section spans two glacial cycles, rather than the previously suggested one. The most likely source of the discrepancy is the use of uncorrected infrared stimulated luminescence signal, which can cause age underestimation if not accounted for. This study demonstrates the need to revisit sites such as Erdut, re-date them using updated measurement protocols, and update existing palaeoenvironmental interpretations.     

最后两个冰期旋回季风-沙漠系统不稳定性的高分辨率黄土记录

黄土高原西北部黄土沉积的粒度变化同时受控于沙漠进退和冬季风强度波动,因此,此区粒度可视为季风-沙漠系统变迁的替代性指标。本研究以2cm为间隔,对李家塬和新庄源S₂以上部分做了粒度分析。结果表明,倒数第二次冰期中的冰阶时段与末次冰期类似,存在着频繁的千年尺度的气候波动;而末次间冰期这类变化并不明显。     

The Požarevac loess–paleosol sequence: a record of increased aridity in the south-eastern margin of the Carpathian Basin during the last 350 ka

The loess sequence preserved in the Požarevac brickyard in north-eastern Serbia comprises eight loess units separated by seven paleosols. Geochronological investigation using amino acid racemization and luminescence dating support stratigraphic correlations of loess units L3, S2LL1 and L1 at the Požarevac section with loess of glacial cycles E [Marine Isotope Stage (MIS) 10], D (MIS 9–8), C (MIS 7–6) and B (MIS 5–2) across central Europe. Correlation with the marine oxygen-isotope stratigraphy and associated paleoclimatic inferences are further supported by magnetic susceptibility, particle size and carbonate content measured in Požarevac sediments. Malacological investigations at the Požarevac section reveal the continuous presence of the Chondrula tridens and Helicopsis striata faunal assemblages throughout the last 350 ka. The loess malacological fauna, which is characterized by the complete absence of cold-resistant and cold-preferring species, suggests a stable, dry and relatively warm glacial and interglacial climate, compared with other central European loess localities. Together these data suggest that the south-eastern part of the Carpathian (Pannonian, Middle Danube) Basin was a refugium for warm-preferring and xerophilous land-snails during the generally unfavorable glacial climates of the late Middle and Late Pleistocene.     

近13万年来黄土高原干湿气候的时空变迁

第四纪时期，黄土高原粉尘物质的搬运、沉积及其后的成土过程受控于干湿气候的变化。对黄土高原这一特定地区而言，风成沉积序列在地域上的差异主要与东亚地区的季风环流在时间和空间上的变化有关。本文的研究揭示出，近１３万年里，最为显著的成壤期有６期，与这６个成壤期对应的时段也应当是夏季风环流加强、气候温湿的时期；在空间上，全新世适宜期及末次间冰期中与深海氧同位素阶段５ａ，５ｃ，５ｅ对应的时期，夏季风足可以深入到毛乌素沙漠腹地，并具有占优势的环境效应。在阶段３的早、晚期及５ｂ时期夏季风虽然也能深入沙漠－黄土边界带，但其环境效应在黄土高原北部及毛乌素沙漠南缘已不再显著。在阶段２、阶段４及阶段３的中期夏季风已不能深入沙漠－黄土边界带。     

Progress in Danube Loess and Paleoenvironment Study

Danube loess, located at the westernmost part of the widespread Eurasian loess belt, is one of the most well-preserved aeolian dust deposits in Europe with the basal age dating back over 1 Ma. Owing to its unique location and formation processes, Danube loess plays an important role in understanding the linkage of climate changes in different climate regimes over Eurasian continent and paleoclimatic changes in middle-high northern latitudes. Major research advances of the Danube loess, including compositions, provenance, chronology, stratigraphy and paleoenvironment changes were systematically reviewed and the focuses of future research were suggested. To better understand loess provenance, the compositions of sediments in all the potential source areas should be investigated, and methodological study of provenance indicators and application of multi-proxies approaches need to be carried out. Chronologically and stratigraphically, feldspar luminescence dating and tephrochronology methods should be widely used, and the establishment of a uniform stratigraphic framework and correlation scheme should be constrained by precise chronology. In terms of the paleoenvironment, it is necessary to conduct high-resolution multi-proxies reconstruction of paleoenviroment for the entire loess-paleosol sequence, extending from the last interglacial period (130 ka to present) to interval of last 1 Ma. The future progress in Danube loess is crucial to improving the study of continental paleoclimate comparison and paleoclimate dynamics over the Eurasian loess region.     

浑善达克沙地南缘晚更新世黄土-古土壤序列的高分辨率磁性气候记录

浑善达克沙地处于季风边缘区,目前对该区域末次间冰期以来的古气候演化历史及其动力学机制尚不清楚。文章以浑善达克沙地南缘山间低洼地带北沟剖面总厚度4.72 m(未见底)的黄土-古土壤序列为研究对象,开展了光释光测年和精细的岩石磁学、环境磁学、地球化学和漫反射光谱分析。结果表明:1)该剖面记录了末次间冰期以来完整的风成堆积历史,并通过东亚夏季风指标(Rb/Sr及χARM/χ)与深海氧同位素曲线的对比建立了13万年来该黄土-古土壤序列精细的年龄模式;2)在黄土高原上常规的用来指示成壤强度和夏季风强度的磁参数并不完全适用于干旱-半干旱地区(400 mm等降水线附近)的风成黄土,而地球化学指标在指示季风边缘区的地球化学风化过程上表现出一定的合理性,北沟剖面复杂的磁信号可能是对末次冰期季风边缘区显著减弱的夏季风的阈值响应;3)在末次间冰期东亚夏季风可以延伸到内蒙古中东部,北沟剖面记录了浑善达克沙地南缘末次间冰期以来区域古季风的演化历史。