Exploring IRSL50 fading variability in bedrock feldspars and implications for OSL thermochronometry

Optically Stimulated Luminescence (OSL) is a well-established Quaternary dating method, which has recently been adapted to application in low-temperature thermochronometry. The Infra-Red Stimulated Luminescence (IRSL) of feldspar, which so far is the most promising target signal in thermochronometry, is unfortunately prone to anomalous fading. The fading of feldspar IRSL is at times not only challenging to measure, but also laborious to incorporate within luminescence growth models. Quantification of IRSL fading is therefore a crucial step in OSL thermochronometry, raising questions regarding (i) reproducibility and reliability of laboratory measurements of fading, as well as (ii) the applicability of existing fading models to quantitatively predict the level of IRSL field saturation in nature. Here we investigate the natural luminescence signal and anomalous fading of IRSL measured at 50 °C (IRSL₅₀) in 32 bedrock samples collected from a variety of lithologies and exhumation settings (Alaska and Norway). We report a large span of IRSL₅₀ fading rates between samples (g_2days ranging from ∼0.5 to ∼45%/decade), which further demonstrates (i) a good reproducibility between two common fading measurement protocols, and (ii) the ability of tunnelling models to predict the level of feldspar IRSL₅₀ field saturation in nature. We observe higher IRSL₅₀ fading in feldspar with increasing Ca content, although other factors cannot be dismissed at present. Finally, our dataset confirms that the applicability of feldspar IRSL₅₀ in OSL thermochronometry is limited to rapidly-exhuming settings or warm subsurface environments.     

Small aliquot and single grain IRSL and post-IR IRSL dating of fluvial and alluvial sediments from the Pativilca valley,Peru

Infrared stimulated luminescence (IRSL) and post-IR IRSL are applied to small aliquots and single grains to determine the equivalent dose (D_e) of eleven alluvial and fluvial sediment samples collected in the Pativilca valley, Central Peru at ca. 10°S latitude. Small aliquot D_e distributions are rather symmetric and display over-dispersion values between 15 and 46%. Small aliquot g-values range between 4 and 8% per decade for the IRSL and 1 and 2% per decade for the post-IR IRSL signal. The single grain D_e distributions are highly over-dispersed with some of them skewed to higher doses, implying partial bleaching; this is especially true for the post-IR IRSL. Measurements of a modern analog reveal that residuals due to partial bleaching are present in both the IRSL as well as the post-IR IRSL signal. The g-values of individual grains exhibit a wide range with high individual uncertainties and might contribute significantly to the spread of the single grain D_e values, at least for the IRSL data. Electron Microprobe Analysis performed on single grains reveal that a varying K-content can be excluded as the origin of over-dispersion. Final ages for the different approaches are calculated using the Central Age Model and the Minimum Age Model (MAM). The samples are grouped into well-beached, potentially well-bleached and partially bleached according to the evaluation of the single grain distributions and the agreement of age estimates between methods. The application of the MAM to the single grain data resulted in consistent age estimates for both the fading corrected IRSL and the post-IR IRSL ages, and suggests that both approaches are suitable for dating these samples.     

A test case for anomalous fading correction in IRSL dating

Infrared-stimulated luminescence (IRSL) dating of feldspars has the potential to date deposits beyond the age range of quartz optical (OSL) dating. Successful application of feldspar IRSL dating is, however, often precluded due to anomalous-fading, the tunnelling of electrons from one defect site to another. In this paper we test procedures proposed for anomalous-fading correction by comparing feldspar IRSL and quartz OSL dating results on a suite of samples from continental deposits from the southeastern Netherlands. We find that even after anomalous-fading correction IRSL ages underestimate the burial age of the deposits and argue that this may be a consequence of a dependency of anomalous fading rate on the dose rate and on the absorbed dose.     

A method to evaluate the degree of bleaching of IRSL signals in feldspar: The 3ET method

In addition to dating, IRSL luminescence signals can preserve information about erosional, transport, and depositional histories of a population of grains. Knowledge of the degree of bleaching can be useful in understanding the processes that occurred during previous depositional events, as certain transport conditions result in a well bleached signal, while others result in grains retaining an inherited signal from prior events. This information can be accessed by making single-grain IRSL measurements across successively increasing temperatures, thereby isolating signals from traps of different bleachabilities.A new approach offers a way to evaluate the completeness of bleaching of a grain by testing patterns of equivalent dose (D_E) values measured at three elevated temperatures (3ET), 50, 125, and 225 °C. Consistent D_E estimates across two or more temperatures suggest a single bleaching event of sufficient duration to fully depopulate the traps involved. Incompletely bleached grains with inconsistent D_E values across temperatures will lack a 3ET “plateau.” Modes in the distribution of D_E values for fully bleached grains can suggest depositional ages, subject to assessment of fading. We developed a Python code in a Jupyter Notebook environment for data analysis and visualization to expedite processing the large data sets produced by the 3ET protocol.The 3ET protocol was tested on a radiocarbon dated sequence of playa samples from California, USA and on a set of fluvial terraces in the Marlborough region of New Zealand as part of a larger project to reconstruct regional seismic history. Where standard pIRIR apparent ages can be inconsistent or ambiguous, 3ET age estimates produce generally consistent apparent ages. Modes of 3ET plateaus can be used to infer the most recent and prior events that resulted in a sub-population of grains being fully bleached. These initial results suggest that the 3ET method can be useful to characterize both the age and degree of bleaching of depositional events.     

Comparison of paired quartz OSL and feldspar post-IR IRSL dose distributions in poorly bleached fluvial sediments from South Africa

A comparative study using quartz optically stimulated luminescence (OSL) and feldspar post-infrared infrared stimulated luminescence (post-IR IRSL) was undertaken on Quaternary fluvial sediments from an unnamed tributary of the Moopetsi River in South Africa. The aim is to assess whether the post-IR IRSL signal can be used to date incompletely bleached sediments. Several post-IR IRSL signals using varying stimulation and preheat temperatures were investigated; of these the post-IR IRSL₂₂₅ signal was deemed most appropriate for dating because it bleached most rapidly. The feldspar post-IR IRSL₂₂₅ equivalent dose (D_e) values from this site are consistently larger than those from quartz OSL, probably due to differences in the bleaching characteristics of the two signals. Additionally, the post-IR IRSL₂₂₅ D_e values within a sample showed less variation in precision than the quartz D_e data, possibly due to greater averaging between grains in the feldspar small aliquots. The agreement between ages based on the OSL and post-IR IRSL₂₂₅ signals was better for younger samples (<20 ka) than for older ones (>50 ka); the cause of this variation is unclear.     

The effect of single grain luminescence characteristics on single aliquot equivalent dose estimates

We report an investigation of the effect of different single grain OSL behaviours on multiple-grain (single aliquot) D_e estimates. This was done by creating ‘synthetic aliquots’ in which signals are summed from collections of individual grains. The samples used were taken from aeolian linear dune sediments, from sites located in the Kalahari. We note this is a type of sample for which single multiple-grain aliquots are routinely used for dating. Several grain behavioural types were identified in our samples but the only grain type that systematically affected multiple-grain D_e estimates was the ‘over-saturating’ type (the case where the natural signal (L_n/T_n) is significantly greater than the regenerated L_x/T_x signal at saturation), the presence of which lead to higher estimates of D_e. The magnitude of this effect is controlled by the contribution of ‘over-saturating’ grains to the total light sum of the multiple-grain aliquot and the maximum increase observed in this study was ∼15 Gy. Of the four samples investigated here, inter-aliquot variations in the signal contribution of ‘over-saturating’ grains led to a significant increase in dispersion in just one of the samples. More generally, the presence/absence of these grains is considered to be a likely source of significant ‘intrinsic’ scatter in single aliquot dating and likely to broaden multiple-grain D_e distributions. We suggest all samples are screened for this behaviour before single aliquot dating is attempted.     

Soil and structure damping from single station measurements

In seismology and seismic engineering soils and structures are modeled as oscillators characterized by modal (resonance) frequencies, shapes and damping. In 1973 Cole proposed the RandomDec technique to estimate both the damping and the fundamental mode of structures from the recorded time series at a single point, with no need for spectral analyses. Here we propose a number of modifications to the original RandomDec approach, that we group under the name DECÓ, which allow to determine the damping as a function of the frequency and therefore the damping of all the vibration modes. However, the motion of structures is so amplified at the resonance frequencies that detecting the characteristic parameters by recording ambient vibrations is relatively easy. More interesting is to apply the DECÓ approach to the soil in the attempt to estimate the mode damping from single station measurements. On soils, the resonance frequencies are normally identified as peaks in the horizontal to vertical spectral ratios of microtremors. However, at these frequencies what is observed is a local minimum in the vertical spectral component, sometimes associated to local maxima in the horizontal components, whose visibility depend on the specific amount of SH and Love waves at the site. The determination of soil damping is therefore a much less trivial task on soils than on structures. By using microtremor and earthquake recordings we estimate the soil damping as a function of shear strain and observe that this is one order of magnitude larger than what is measured in the laboratory on small scale samples, at least at low-intermediate strain levels. This has severe consequences on the numerical seismic site response analyses and on soil dynamic modeling.     

Differential weathering of feldspar and pyroxene in an arctic-alpine environment

The relative relief of adjacent plagioclase and pyroxene minerals was accurately measured on a recently-exhumed outcrop of gabbroic rocks in Leirdalen, southern Norway. Above the level of the former soil surface the feldspars protrude above the pyroxenes whereas below that level the pyroxenes are higher. Differential relief declines with increasing depth of burial down to 80 cm. On exposed surfaces the mean loss of pyroxene relative to feldspar is 103 cm³ m^?2 of rock surface. With burial down to 50 cm in an arctic-alpine Brown Soil the mean loss of feldspar relative to pyroxene is 179 cm³ m^?2. These figures represent minimum amounts of weathering over about 9000 years. The results confirm the importance of chemical weathering in arctic-alpine environments and the techniques may provide useful physical measures of degree of weathering for use in rate studies and relative-dating.     

MET-post-IR IRSL luminescence dating of cobbles buried in fluvial terraces in the Northern Chinese Tian Shan

Cobbles can be used as an alternative to the conventionally employed sand-sized mineral luminescence dating. In piedmont environments, cobbles are much more abundant than sand-sized material. The IRSL₅₀ signal has been widely used in previous studies due to its greater sensitivity to exposure events. However, it is well known that the low temperature IRSL signal is more prone to fade than elevated temperature post-IR IRSL signal. In this study, to test the reliability and applicability of cobble sub-surface elevated temperature IRSL luminescence dating, six light-color granite cobbles and two sand-sized samples from silty sand lens were collected from a high terrace of Manas River on the northern piedmont of Chinese Tian Shan. A modified multi-elevated-temperature post-infrared infrared stimulated luminescence (MET-post-IR IRSL) protocol was applied. The age-temperature (A-T) plateau of MET-post-IR IRSL measurement was combined with the conventional age-depth (A-D) plateau in luminescence-depth profile to evaluate the resetting and fading of MET-post-IR IRSL signals. Uncertainties of grain-sizes of K-feldspar within solidified slices were also explored by μ-XRF mapping of potassium content. The A-T plateau was identified between MET-post-IR IRSL₁₇₀ and MET-post-IR IRSL₂₂₅ signals of one cobble, which suggested completeness of bleaching before burial and negligible anomalous fading during burial. This cobble yielded MET-post-IR IRSL₂₂₅ ages of 15.8 ± 2.6 ka and 19.0 ± 3.2 ka for top and bottom side, respectively. These MET-post-IR IRSL₂₂₅ ages were consistent with independent coarse-grained quartz MAM OSL ages (15.7 ± 3.6 ka and 14.8 ± 2.6 ka) of two sand-sized samples. The MET-post-IR IRSL₂₂₅ age of 16.0 ± 1.2 ka for the bottom side of another cobble was also consistent with the independent age, even without the A-T plateau. It was inferred to be caused by anomalous fading of MET-post-IR IRSL signals other than that stimulated at 225 °C by refering to the A-D plateau observed. Our results show that MET-post-IR IRSL measurement can be employed to determine the burial ages of cobbles. The A-T plateau, complemented with the A-D plateau, could be used to assess the reliability of burial ages of cobble luminescence dating from the view of bleaching and fading.     

Testing the accuracy of OSL and pIR IRSL dating of young geoarchaeological sediments in coastal Peru

Luminescence dating of late Quaternary sediments in Peru is challenging, especially on the Peruvian coast. Earlier studies have shown that quartz grains often exhibit a thermally unstable, medium signal that caused the underestimation of Optically Stimulated Luminescence (OSL) ages. InfraRed Stimulated Luminescence (IRSL) dating has shown to produce more reliable ages, depending, amongst other factors, on the age model (Central or Minimum Age Model), and the IRSL signal. IRSL dating of geoarchaeological sediments has, however, hardly been carried out, let along validated, against an independent age dataset. This dating approach is, nonetheless, the only promising way to date the geological substrate in which many of Peru's archaeological sites are buried. Peru contains some of the oldest and most important archaeological heritage sites, yet not much is known of the environmental context in which many of its early civilizations prospered. A better understanding of which luminescence method works best could therefore help in a better understanding of the geological-stratigraphical context of many of Peru's sites.To investigate this matter more fully, we compared the luminescence dating results of seven sediment samples from the top layer of the Lima alluvial fan and from geoarchaeological layers of the Maranga Complex (San Miguel, Lima), with an independent dataset of sixteen ¹⁴C ages. Our results showed that the quartz OSL ages always underestimated the expected ages due to a signal dominated by medium and slow components, and that the post-IR IRSL₂₂₅ (pIR IRSL₂₂₅) and IRSL₅₀ ages of K-feldspars, on basis of the Central Age Model (CAM), always overestimated the expected ages. The Minimum Age Model (MAM) on the other hand, correctly predicted the expected ages for the early Holocene, Lima alluvial fan sediments using the pIR IRSL₂₂₅ signal of K-feldspars, and the late Holocene, geoarchaeological ages using the IRSL₅₀ signal.     

An advanced signal processing technique for deriving grain size information of bedload transport from impact plate vibration measurements

A reliable characterization of bedload transport is required to gauge the engineering and theoretical issues related to the dynamics of sediments transport in rivers. However, while significant advances have been made in the development of monitoring techniques, robust quantitative predictive relationships have proven difficult to derive. In this article, we develop a dedicated signal processing technique aimed at improving the usage of impact plate measurements for material transport characterization. Our set‐up consists of a piezoelectric hydrophone mounted on the bottom side of a stainless steel plate, thus acting as a ‘sediment vibration sensor’. While the classical analysis with such systems is usually limited to rather simple procedures, such as impact counting, a large amount of useful information is contained in the actual waveform of the impact signal, which conveys the force and the contact time that the bedload imposes on the plate. An advanced signal processing technique called ‘first arrival atomic decomposition’ is used to improve the characterization of bedload transport by analysing the amplitude and frequency attributes of each single impact. This new processing approach proves to be well suited for bedload transport monitoring using plate systems and allows us to establish a relationship between the median grain size (D₅₀) and the impact signal properties. This link is first observed and validated with controlled flume experiments and then applied to continuous impact records in a small gravel‐bed river during a flood event. The estimated D₅₀ offers a novel possibility to observe the time‐varying grain size distribution of bedload transport. Copyright © 2014 John Wiley & Sons, Ltd.     

Luminescence properties of single grain quartz to determine the history of a sample from the Sahara Desert

In this work we present luminescence analyses of material taken from a Neolithic hearth in the Sahara Desert in Egypt. The sample was taken from a beach sand layer which contained traces of charcoal. The sample was dated using quartz luminescence, and its luminescence properties were investigated to find whether it had been heated by fire. In doing so we established a procedure to distinguish heated and unheated quartz at single grain level.The OSL age estimate of the sample is 10.6 ± 0.4 ka. Luminescence properties were measured using about 40,000 individual grains. Using an approach similar to that used to measure thermal activation characteristics (TAC), we compared the distribution of OSL sensitivity of single grains following different thermal treatments. It was found that higher temperatures and longer treatment times change the sensitivity distributions systematically from that observed using the natural sample. We conclude that the grains examined in our dating study were not heated by fire prior to burial, and that the hearth is not older than the OSL age.     

Modelling dose rate to single grains of quartz in well-sorted sand samples: The dispersion arising from the presence of potassium feldspars and implications for single grain OSL dating

Single grain OSL has become a widely used approach in Quaternary geochronology. However, the origins of D_e distributions and the sources of variation in individual dose estimates are still poorly understood. The amount of scatter in these distributions on top of the known uncertainties in measurement and analysis is defined by overdispersion and this quantity is generally used for weighting individual D_e values to calculate a central equivalent dose. In this study, we address the nature and amount of different sources of dispersion in quartz single grain D_e estimates, by (i) using appropriate statistical tools to characterize D_e populations and (ii) modelling, with a specifically designed Geant4 code, dose rate distributions arising from the presence of potassium feldspar grains in well-sorted sands. The model uses Monte Carlo simulations of beta emissions and interactions in a random close packing of quartz and feldspar spheres representing a sand sample. Based on the simulation results, we explain the discrepancy between intrinsic and natural overdispersion values in a well-bleached sample, thus validating the model. The three parameters having the most influence on dispersion in dose rate distributions, and modelled in this study, appear to be grain size, potassium content and total dose rate.Finally an analysis of measurement uncertainties and other sources of variations in equivalent dose estimates lead us to conclude that all age models (both logged and unlogged) which include an overdispersion value to weight individual D_e values rely mainly on unknown parameters; this ignorance may lead to an inadvertent bias in D_e estimates. Assuming counting statistics make a small contribution to dispersion (as is often the case), we suggest that in some cases it is most appropriate to use unweighted averages of equivalent doses when dividing by commonly measured average dose rates.     

Detailed measurements of thickness and grain size of a widespread onshore tsunami deposit in Phang‐nga Province,southwestern Thailand

Measurements of thickness and grain size along flow‐parallel transects across onshore deposits of the 2004 Indian Ocean tsunami revealed macroscopic horizontal variations and provided new insights into tsunami sedimentation. The tsunami caused severe erosion of beaches, river mouths, and the shallow seafloor along the coast of southwestern Thailand and supplied sufficient sediment to deposit a kilometer‐wide blanket of sand on the land surface. The tsunami deposits generally fine landward with some fluctuations caused by local entrainment and settlement of sediments. Sediments of medium and fine sand are restricted to a few hundreds of meters inland from their source, whereas finer grained sediments were suspended longer and deposited 1 km or more inland. Although the thickness of the tsunami deposits is strongly influenced by local topography, they generally thin landward. In areas of low‐relief topography, the rate of landward thinning is exponential and reflects the dominance of sediment supply to nearshore areas over that to areas farther inland.     

Variations in luminescence properties of quartz and feldspar from modern fluvial sediments in three rivers

Studies of modern sediments, their sedimentology and depositional processes are important for understanding the behaviour of the luminescence characteristics of quartz and feldspar in fluvial settings. Previous studies have shown large variations in OSL characteristics of quartz from different fluvial systems, while the IRSL and pIRIR signals from K-feldspar have been understudied. We test the effects of fluvial setting on luminescence characteristics by collecting modern (<1 year old) bedload sediments down the courses of three river systems with very different hydrological characteristics, geologic contexts, and catchment lithologies. The single grain (SG) and multi-grain aliquot (MGA) OSL (quartz) and IRSL and pIRIR (K-feldspar) properties of samples were measured and compared to better understand intra- and inter-fluvial system patterns in sensitivity, bleaching, and equivalent dose (D_e) distribution skewness and kurtosis. The quartz OSL and K-feldspar IRSL and pIRIR signal sensitivities increase with downstream transport distance of sediments, confirming previous studies (quartz) and showing that IRSL signals from K-feldspar also increase in response to reworking cycles. Increasing transport distance also results in better bleaching of the OSL signal from quartz samples (MGA and SG) due to more grains being exposed to sunlight. By contrast, the IRSL and pIRIR signals retain significant residuals in all samples, though 5–15% of grains yield zero-dose D_e values and age modelling of SG data yields accurate burial dose estimates. Additionally, the skewness and kurtosis of SG OSL D_e datasets from one river increase with transport distance, with the best bleached samples exhibiting the highest skewness, thereby questioning the applicability of the skewness-value of a D_e dataset as an accurate indicator for partial-bleaching. Our data shows marked variability between (i) different river systems and (ii) the measured minerals, however consistent use of statistical models allows accurate D_e estimation in all contexts. Age modelling of SG data from K-feldspar, thus, provides a valuable tool for future fluvial research in regions where poor OSL characteristics prevent the use of quartz as a dosimeter.     

Testing the potential of using coarse-grain feldspars for post-IR IRSL dating of calcium sulphate-wedge growth in the Atacama Desert

The growth of vertically laminated calcium-sulphate wedges in the Atacama Desert is assumed to be driven by the interaction of moisture supply and salt dynamics in the subsurface. Geochronological data of these wedge laminations is yet sparse but indispensable to resolve wedge-growth phases and episodes of moisture supply and to use these deposits as a palaeoclimate archive in the hyperarid environment. Our pilot study presents a first approach of dating a calcium-sulphate wedge from the Atacama Desert using coarse-grain feldspar luminescence dating. Our results show a widespread and clustered equivalent-dose distribution of two wedge samples from ∼20 Gy up to saturation. Optically stimulated luminescence (OSL) of quartz revealed unsuitable properties for dating wedge deposits. Consequently, we applied post-infrared infrared stimulated luminescence (post-IR IRSL) to coarse-grained feldspars. Since feldspar single-grain measurements yielded a low number of luminescent grains, we used 1 mm aliquots as reliable single-grain proxies for genuine single-grain measurements. Data from energy-dispersive x-ray spectroscopy (EDX) showed that the feldspar single grains have large differences in their internal K content, resulting in an averaged internal K content of 3.9 ± 1.0 % for all luminescent grains. This result was subsequently used for dose rate and age calculations. Our results of equivalent-dose distributions and palaeodoses derived from the minimum age model reveal most recent wedge-growth activities at 10.6 ± 2.2 ka and 7.9 ± 1.8 ka for the two wedge samples.     

Hydrothermal alteration of plagioclase and growth of secondary feldspar in the Hengill Volcanic Centre, SW Iceland

Dissolution of igneous feldspar and the formation and occurrence of secondary feldspar in tholeiitic basalts from the Hengill volcanic centre, in SW Iceland was studied by microprobe analysis of cuttings from two ca. 2000 m deep geothermal wells. Well NG-7 in Nesjavellir represents a geothermal system in a rift zone where the intensity of young, insignificantly altered intrusions increases with depth. Well KhG-1 in Kolviðarhóll represents the margin of a rift zone where the intensity of intrusives is lower and the intensity of alteration higher. This marginal well represents altered basaltic crust in an early retrograde state. The secondary plagioclase in both wells is mainly oligoclase, occurring in association with K-feldspar and chlorite±actinolite. The texture of this assemblage depends on the lithology and intensity of alteration. In Nesjavellir (NG-7) the composition of secondary albite-oligoclase is correlated with the host-rock composition. This connection is not apparent in more intensely altered samples from Kolviðarhóll (KhG-1). The influence of temperature on composition of secondary Na-feldspar is unclear in both wells although Ca is expected to increase with temperature. Any temperature dependence may be suppressed by the influence of rock composition in Nesjavellir and by retrograde conditions at Kolviðarhóll. The absence of clear compositional gradients between igneous plagioclase and secondary feldspar and between Na-feldspar and K-feldspar suggests that secondary feldspars formed by dissolution precipitation reactions.     

Magnetotelluric measurements in Antarctica

During austral summer 1984–1985 magnetotelluric measurements were carried out in North Victoria Land, Antarctica. The magnetic field was measured by a three-component fluxgate magnetometer. Copper screens (50 cm × 50 cm) were used as electrodes for recording the electric field, connected to a two channel electrograph with an input impedance of 10¹² ω. Analogue data are digitized with 12 bit resolution by a data acquisition system. 1 Mb of solid state CMOS-RAM memory was used to store the data in the field until it could be played back onto 3.5 inch floppy discs during station control. All equipment is designed for low power consumption. In the field it is supplied by a battery, which is charged by solar panels. Time series of measured data are presented. The influence of the polar electrojet (PEJ) on the source fields is clearly seen by comparing 24-h time series with the position of the auroral oval at different times of the day. Despite the clear effect of the PEJ in the data, the calculated apparent resistivity and phase curves seem to be rather uninfluenced. Initial interpretations have led to a typical continental resistivity distribution, showing decreasing resistivity with increasing depth.     

Optical dating of Holocene lake sediments: Elimination of the feldspar component in fine silt quartz samples

Optically stimulated luminescence of fine silt quartz was investigated to establish chronologies for lake sediments from the British Isles. Feldspar contamination and its potential effects on equivalent dose (D_e) determination were examined. A new feldspar contamination test based on the thermal quenching of quartz OSL and thermal assistance of feldspar OSL identified feldspar contamination in samples being treated for 20 min in 20% hydrofluoric acid. Feldspar component monitoring based on the post-IR OSL/OSL ratio was not sufficiently sensitive to monitor a feldspar component, but is a good indicator whether a standard SAR procedure can be applied successfully, despite the presence of feldspar. Based on these results we used a modified SAR protocol including a 100 s IRSL stimulation at 50 °C before OSL readout. This protocol could overcome any malign effects of feldspar even for a feldspar bearing polymineral sub-sample.