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1.
Optically stimulated luminescence (OSL) dating methods have been widely applied in Quaternary glaciology. However, glacigenic deposits are considered in general as problematic for OSL dating, mainly because they are transported shorter distances prior to burial and are usually partially bleached. Thus, most researchers choose glaciofluvial and glaciolacustrine sediments (with relatively longer transportation times) for OSL dating when constraining the age of glaciation. In this study, four samples were collected from a lateral moraine series at Zhuqing Village, northern margin of Queer Shan Mountain, eastern Tibetan Plateau, in order to investigate the applicability of OSL dating for morainic deposits. Quartz grains (38–63 μm) were extracted and measured using single aliquot regenerative-dose (SAR) protocol. Internal checks and dose recovery test show that the SAR protocol is appropriate for equivalent dose (De) determination. The effect of thermal transfer is small for all samples and the recycling ratio for each individual sample is close to unity. The symmetry in the De distributions indicates that quartz grains were well-bleached prior to burial. OSL ages show good agreement with geomorphological and field investigations, and are also concordant with an independent ESR age. It is concluded that: (a) the morainic deposits in Zhuqing were well-bleached and suitable for OSL dating; (b) SAR protocol can be applied to morainic deposits for samples under study.  相似文献   

2.
The applicability of the post-IR IRSL single-aliquot regenerative-dose protocol (termed pIRIR protocol) has been tested on K-rich feldspar from recent coastal sediment samples (<500 a) from the southern North Sea coast and southern Baltic Sea coast. The most suitable post-IR IRSL (pIRIR) stimulation temperature is found to be 150 °C by using a preheat temperature of 180 °C. For this pIRIR stimulation temperature, a detectable pIRIR signal is obtained and the residual dose is minimized. Furthermore, anomalous fading is found to be negligible in the pIRIR150 signal for our young samples whereas the fading rates for the conventional IRSL signal measured at 50 °C (IRSL50) is between 5 and 7%/decade. However, the pIRIR150 signal bleaches significantly slower compared to the IRSL50, according to bleaching experiments using daylight, solar simulator and IR diodes, although the residual doses of both signals are similar. The laboratory residual doses in perfectly bleached aliquots are variable from sample to sample and vary between 300 ± 170 and 800 ± 460 mGy for the pIRIR150. The precision of the residual dose determination is generally poor and causes large uncertainties on the residual subtracted ages. The laboratory residual doses alone cannot account for the observed overestimation in our two youngest samples (<70 a), indicating that the feldspar signals in these samples were presumably not fully bleached prior to aeolian or beach deposition. However, even if the age uncertainties are large we obtained pIRIR150 ages in agreement with independent age estimates for the two older samples, which are 70 and 390 years old.  相似文献   

3.
The Yellow River is characterized by its tremendous sediment load. In this study we investigated the residual OSL signals in modern fluvial sand and suspended-sediment samples from the middle reach of the river. The residual equivalent dose (De) is found to vary with grain size, mineralogy and the techniques used for the De determination. The results indicate that the OSL signals in some grains from these samples were not completely bleached prior to burial, the maximum individual De value obtained is up to 56 Gy. The results also show that coarse grains are generally better bleached at deposition than fine grains; the fine-grained quartz from suspended sediments are better bleached than the fine-grained quartz from the fluvial sand deposits. The Des obtained using quartz TT-OSL signals are up to ~380 Gy for these modern samples.  相似文献   

4.
We present quartz single-grain dose distributions for four well-bleached and unmixed sediment samples with independent age control (22–48 ka), from the archaeologically important Bordes-Fitte rockshelter at Roches d'Abilly, France. This site has previously been dated using 14C AMS dating and standard multi-grain OSL dating using both quartz and feldspar. The effect of rejection criteria usually employed in single-grain dating on dose and over-dispersion is tested using both laboratory irradiated samples and natural samples. It is shown that had these samples been analysed in the absence of other age control, standard modelling decisions based on the shape of single-grain dose distributions would have led to significant misinterpretation of results and a corresponding >40% underestimation in age. If we instead ignore this standard decision process and apply weighted average and mixing models then the most likely results deviate from the expected ages by >10%. Finally, we show that by careful consideration of the luminescence characteristics of individual grains, we are able to obtain good agreement with the independent age control by applying alternative rejection criteria but this is at the cost of reducing the accepted grain population by more than an order of magnitude, with the corresponding inevitable decrease in precision.  相似文献   

5.
Luminescence dating has long been used for chronological constraints on marine sediments due to the ubiquitous dating materials (quartz and feldspar grains) and its applicability over a relatively long time range. However, one of the main difficulties in luminescence dating on marine sediments is partial bleaching, which causes age overestimations. Especially, partial bleaching is typically difficult to be detected in the fine grain fraction (FG) of marine sediments. The recently developed feldspar post-IR IRSL (pIRIR) protocol can detect non-fading signals and thus avoid feldspar signal instability. In the current study, fine grains were extracted from a gravity core in the northern Sea of Japan, and the aim is to test the feasibility of using different luminescence signals with various bleaching rates to explore the bleaching conditions of fine grain fraction in marine sediments. The results suggest that the quartz OSL signal and polymineral pIRIR signals at stimulation temperatures of 150 °C and 225 °C (pIRIR150 and pIRIR225) of FG were well bleached prior to deposition. The OSL ages were used to establish a chronology for this sedimentary core and the resulting age-depth relationship is self-consistent and comparable with radiocarbon dates. We conclude that different luminescence signals with various bleaching rates can be used to test the bleaching conditions of fine grain fraction in marine sediments; and the luminescence dating can be applied to marine sediments with great potential.  相似文献   

6.
The high-temperature (e.g., >200 °C) post-infrared infrared (pIRIR) stimulated luminescence of feldspar has been widely used for dating, because it usually suffers negligibly from anomalous fading. However, compared to the quartz optically stimulated luminescence (OSL) or low-temperature (e.g., 50 °C) IR stimulated luminescence (IRSL) from feldspars, the high-temperature pIRIR signals have been shown to bleach more slowly and usually have high residual does of a few Gys or more, which limits its application to date relatively young samples and may cause problems for correcting residual dose/signal. In this study, we investigated the bleachability of K-feldspar pIRIR signals for individual grains. A significant variation in the bleachability of the pIRIR signal was observed among different K-feldspar grains from the same sample. Experiments show that such a variability may result in different residual doses for different grains and, consequently, additional scatter in De values. We present a method for quickly testing the bleachability of individual grains. Our result suggests that selecting the easy-to-bleach grains for De determination provides an efficient way to date young samples using high-temperature pIRIR signals, which avoids the compromise of using low-temperature pIRIR signals that may suffer from anomalous fading.  相似文献   

7.
The prehistoric site of Ifri n'Ammar is situated in northeastern Morocco, in the northern prolongation of the Middle Atlas Mountains. It is a key location in unravelling the history of anatomically modern humans (AMH) in northern Africa as it reveals Middle and Late Palaeolithic occupation phases since ∼170 ka. Whilst the archaeological sequence within the rock shelter has been well studied, the timing of landscape dynamics around Ifri n'Ammar is still poorly understood. This study therefore aims to establish a detailed chronology of the Wadi Selloum profile at the apron of the shelter, based on optically stimulated luminescence (OSL) dating of ephemeral stream deposits. Coarse-grain quartz was used for single-grain and multiple-grain dating procedures to investigate the luminescence properties of these deposits and to get more accurate age information concerning the phases of human occupation. Continuous wave OSL (CW-OSL) revealed a dominant fast component for all quartz samples. The dose distribution of the uppermost samples showed overdispersion values >25% and significant positive skewness. We identified partial bleaching as the main source of scatter in the equivalent dose (De) distribution. The lowermost sample appeared to be close to signal saturation. The shapes of the dose response curve varied widely between aliquots and coarse quartz grains exhibited therefore very different dose saturation behaviours among aliquots. With fully saturated dose response curves (DRCs), meaningful D0 values were assumed for De estimation.The eight OSL samples yielded stratigraphically consistent ages ranging from 1.3 ± 0.2 ka to 76 ± 5 ka, thus reaching the Middle Palaeolithic period. Moreover, a pottery shard dated to 7.4 ± 0.6 ka (Early Neolithic period) by thermoluminescence (TL), perfectly matched the Holocene OSL samples extracted at the same depth of the profile. In summary, our results point to fluvial aggradation during OIS 5.1, the late glacial period, and the Holocene.  相似文献   

8.
In order to test the accuracy of quartz optically stimulated luminescence (OSL) dating for young dune sediments (<100 a), a series of aerial images of a migrating sand dune is used to cross validate OSL ages. The investigated dune is situated on the northern part of the island of Sylt (southern North Sea). Based on aerial images and a map from 1925 to 2009 and the internal architecture of the dune obtained by ground-penetrating radar (GPR), an independent age model has been developed to attribute sedimentary-architectural elements of the dune to time. The annual rate of dune migration is calculated to be around 4.1 m/a. Along a 245 m transect oriented parallel to the direction of dune movement, 13 samples for OSL dating were collected at equidistant locations. Sand-sized quartz (150–250 μm) was used for determining the equivalent dose (De) applying a single-aliquot regenerative-dose (SAR) protocol. Results show that the oldest OSL age from the investigated recent dune appeared to be 110 ± 10 a, whereas the modern analogue was dated to 34 ± 3 a. In comparison with the aerial images, the OSL ages show a systematic overestimation of 10–40 a for six out of seven younger samples, which are expected to be younger than ∼60 a. This offset is negligible for older samples, but a substantial error in these younger ages. The overestimation is originated from a combination of small thermal transfer of 4–12 mGy during preheat and incomplete bleaching in medium OSL component causing a residual dose of about 15 mGy. The contribution of the incompletely bleached medium component cannot be removed totally by an early background subtraction approach. Despite the observed offset for youngest samples, this study corroborates the suitability of the OSL technique to date young dune sediments (<100 a).  相似文献   

9.
Daihai Lake is one of the largest lakes in the mid-latitude of northern China. Previous environmental change investigations using the sediments from the lake have been mainly focused on the last 13 ka. In 2006, we drilled an 80-m borehole on the southwest coast of the lake. Here we report the results of initial optical dating of the upper 22-m sediments from the core. Most of the samples allow separation of the 4–11 μm fine-grained and 45–63 μm medium-grained quartz, both of which were used for equivalent dose (De) determination. Dose recovery test experiments with the single-aliquot regeneration-dose (SAR) protocol indicate that a preheat at 240 °C for 10 s combined with a cut-heat of 240 °C is suitable for these samples. The De values show marked discrepancy between the two grain size fractions with the fine-grained quartz yielding up to over 50% higher De values than the medium ones for some samples. We consider the OSL ages for the samples from upper ~10 m to be overestimated. The main cause of the overestimation is attributed to the incomplete bleaching of the sediment grains at deposition. The OSL ages for the lower part of the sequence are considered to be reasonable age estimates which provide useful temporal constrains on the deposition of the sediments for the period of 20–40 ka.  相似文献   

10.
Two modern coastal sands are studied through single-grain optical dating techniques. The first sample is estimated to be less than 10 y old by means of independent age control and is known to be well-bleached on the basis of preliminary single-aliquot studies. The second sample is less than 1 y old, but an age of 73±24 years had been determined through single-aliquot analysis. For both samples we compare equivalent doses obtained from single-grain analysis to those obtained by means of similar single-aliquot methods. We found that results are comparable although equivalent doses determined through single-aliquot methods are more precise. The reason for this may be ascribed to the limited number of grains on which single-grain measurements were carried out. The presence of poorly bleached grains within a sample could be identified by dose distribution analysis of individual grains.  相似文献   

11.
《Quaternary Geochronology》2008,3(1-2):114-136
We present chronological constraints on a suite of permanently frozen fluvial deposits which contain ancient DNA (aDNA) from the Taimyr Peninsula of north-central Siberia. The luminescence phenomenology of these samples is first discussed, focusing on the optically stimulated luminescence (OSL) decay curve characteristics, thermoluminescence (TL) properties, and signal compositions of quartz from these previously unstudied deposits. Secondly, we assess the suitability of these samples for OSL dating and present the OSL chronologies obtained using both single-grain and multi-grain equivalent dose (De) measurements. The results of our analyses reveal a large amount of inter-aliquot variability in OSL decay curve shape that is directly related to differences in the size of the 280 °C TL peak and the associated slowly bleached ‘S2’ OSL component. Longer OSL stimulation durations are adopted in the De measurement procedure to prevent the progressive build-up of slowly bleached signal components throughout successive single-aliquot regenerative-dose (SAR) measurement cycles. The use of low preheat temperatures in the SAR procedure also reduces the deleterious effects of these slowly bleached signal components. The resultant single-grain and multi-grain OSL chronologies obtained using this approach are stratigraphically consistent and are in close agreement with independently established 14C ages at our sites. The findings of this research reveal the potential of OSL dating as a means of providing a reliable chronometric framework for sedimentary aDNA records in permafrost environments.  相似文献   

12.
The standardised growth curve (SGC) for quartz OSL has recently been developed as a practical means to reduce measurement times when determining palaeodoses using quartz of aeolian sediments, especially loess and desert sand from the same section or the same geographical area. In the present study, we test the performance of SGCs for lacustrine sediments of three cores in the Qaidam Basin of the Qinghai-Tibetan Plateau (QTP) in China. A total of nine samples were collected (three samples from each of the three cores), and silt-sized (38–63 μm) quartz was extracted for the experiment. The results demonstrated that: (a) Nine samples display similar dose–response curves up to a regeneration dose of 600 Gy using single aliquot regenerative-dose (SAR) protocol, suggesting the existence of a standardised growth curve for lacustrine sediments in the Qaidam Basin; (b) For samples with Des of up to ~400 Gy, the Des determined by the SGC are in agreement with the Des by the SAR protocol, suggesting that the SGC approach could be used for De determination up to a dose of ~400 Gy for lacustrine samples from the Qaidam Basin of the Qinghai-Tibetan Plateau in China; (c) The saturation dose for these samples is more than 600 Gy, and in the growth curve a linear growth part was observed in the high dose range of >200 Gy.  相似文献   

13.
The growth of vertically laminated calcium-sulphate wedges in the Atacama Desert is assumed to be driven by the interaction of moisture supply and salt dynamics in the subsurface. Geochronological data of these wedge laminations is yet sparse but indispensable to resolve wedge-growth phases and episodes of moisture supply and to use these deposits as a palaeoclimate archive in the hyperarid environment. Our pilot study presents a first approach of dating a calcium-sulphate wedge from the Atacama Desert using coarse-grain feldspar luminescence dating. Our results show a widespread and clustered equivalent-dose distribution of two wedge samples from ∼20 Gy up to saturation. Optically stimulated luminescence (OSL) of quartz revealed unsuitable properties for dating wedge deposits. Consequently, we applied post-infrared infrared stimulated luminescence (post-IR IRSL) to coarse-grained feldspars. Since feldspar single-grain measurements yielded a low number of luminescent grains, we used 1 mm aliquots as reliable single-grain proxies for genuine single-grain measurements. Data from energy-dispersive x-ray spectroscopy (EDX) showed that the feldspar single grains have large differences in their internal K content, resulting in an averaged internal K content of 3.9 ± 1.0 % for all luminescent grains. This result was subsequently used for dose rate and age calculations. Our results of equivalent-dose distributions and palaeodoses derived from the minimum age model reveal most recent wedge-growth activities at 10.6 ± 2.2 ka and 7.9 ± 1.8 ka for the two wedge samples.  相似文献   

14.
The Late Quaternary hydroclimatic evolution of lake systems in Mongolia remains unclear. Here we present a record of lake level variations at Orog Nuur in the Valley of Gobi Lakes in southern Mongolia, since the last interglaciation, based on paleo-shoreline dating using quartz optically stimulated luminescence (OSL) and K-feldspar post-infrared infrared stimulated luminescence (pIRIR) signals. Due to feldspar contamination that could not be eliminated, the OSL signals of quartz single-aliquots (SA), except for two Holocene samples, were unsuitable for dating and a double SA regenerative-dose (SAR) protocol was used for the quartz fraction of these two samples. The pIR50IR170 and pIR200IR290 signals of K-feldspar SA were used to date Holocene samples and old samples (>100 ka), respectively, with the SAR protocol. To determine the bleaching condition of the pIR200IR290 signals, the first pIRIR dating of K-feldspar single-grains of lake shoreline sediments in Mongolia was performed. The equivalent doses of K-feldspar grains show normal distributions, suggesting that the pIR200IR290 signals are well-bleached. Overall, the results, combined with those of previous studies, show that a mega-lake developed at 56 m above the modern lake level (a.m.l.) during MIS 5e (124.2 ± 6.8114.7 ± 8.0 ka). Holocene high-stands occurred in the last deglaciationearly Holocene (11.1 ± 1.0 ka) at 23 m a.m.l. and in the mid-Holocene (6.7 ± 0.83.3 ± 0.4 ka) at 2014 m a.m.l. The dimensions of the paleo-lakes were recovered, and a hydrological index indicates that the effective moisture during MIS 5e and the mid-Holocene was 10.7 times and 3.65.0 times larger than today, respectively. Finally, the possible mechanisms behind the lake level history are discussed based on correlation with independent paleoclimatic records.  相似文献   

15.
The Wulanmulun site found in 2010 is an important Paleolithic site in Ordos (China), from which lots of stone and bone artifacts and mammalian fossils have been recovered. It was previously dated by radiocarbon and optically stimulated luminescence (OSL) techniques on quartz. To further confirm the reliability of the chronology constructed based on OSL ages and test the applicability of the recently developed pIRIR procedure on sediments from northern China, twenty-four sediment samples (including eolian, lacustrine and fluvio-eolian sands) from the site were determined using the multi-elevated-temperature post-IR IRSL (MET-pIRIR or pIRIR) procedure on potassium feldspar. The results show that the studied samples have two MET-pIRIR De preheat plateaus (280–320 and 340–360 °C), and the bleaching rates of the luminescence signals are associated with sample ages and stimulation temperatures. All the pIRIR ages (7–155 ka) corrected for anomalous fading and residual dose obtained after solar bleaching for 15 h are larger than the corresponding quartz OSL ages (4–66 ka) previously determined, even for the young eolian samples (<10 ka). But the corrected IRSL(50 °C) ages (6–85 ka) are broadly consistent with the quartz ages. It appears that the IRSL(50 °C) ages are more reliable, although this contradicts the previously results obtained by other people. On the other hand, we also obtained an extended age plateau between the stimulation temperatures of 50 and 290 °C in the plot of age versus stimulation temperature (A-T plot) by subtracting different residual doses obtained after different bleaching times. The reliability of the plateau ages requires further investigation. For the sediment samples from this site, quartz should be more suitable for dating than K-feldspar, and the quartz OSL ages of 50–65 ka for its cultural layer should be reliable.  相似文献   

16.
The Mu Us Desert, located in the northwestern fringe of the East Asian monsoon region, is sensitive to climate variability. The desert is characterized by mobile, semi-fixed and fixed sand dunes. Alternating units of dune sands and sandy palaeosols in the Mu Us Desert imply multiple episodes of dune building and stabilization, in response to the ebb and flow of the East Asian monsoon. Desert evolution and climatic change of high-resolution in the Mu Us Desert are still poorly understood due to limited numerical dating results. In the present study, 19 samples collected from five sand dune sections along a northwest–southeast transect in the Mu Us Desert were dated using quartz optically stimulated luminescence (OSL) and single aliquot regenerative-dose (SAR) protocol. Internal checks of the OSL dating indicate that the SAR protocol is appropriate for equivalent dose (De) determination for the samples under study. Combined with the lithologic stratigraphy and the luminescence chronology, the sand dune development in the Mu Us Desert during the Late Pleistocene is discussed. Our results indicate that the sand was mobilized approximately at 91 ka, 71 ka, 48–22 ka, 5 ka, 1 ka, and 0.44 ka; the sand was fixed approximately at 65 ka and Holocene Optimum period in the interior Mu Us Desert. The Mu Us Desert formed at least before ~144 ka, and has shown increasing aridity in the Late Pleistocene.  相似文献   

17.
Debris flows in the mountainous regions south west of Beijing, China occur frequently and often result in considerable mass movements with disastrous consequences for human life, infrastructure and agriculture. Obtaining chronological information on such events is important for the prediction of the return frequency of these debris flows, risk assessment and climate change research. In this project, we use quartz single-grain optically stimulated luminescence (OSL) methods to determine the burial ages of five debris flow samples from the Zhai Tang region ∼60 km west of Beijing. OSL characteristics were found to be acceptable despite the low inherent brightness of quartz extracted from these samples. Single-grain thermal transfer was determined to be negligible and beta dose recovery experiments were satisfactory. The quartz single-grain dose distributions strongly indicate that the samples were poorly bleached prior to deposition; relative over-dispersions are larger than 60%. Minimum age modelling indicates that all five samples were deposited within the past few hundred years, indicating that catastrophic debris flows are occurring under the historically-recent land-use pattern.  相似文献   

18.
Identification of past tsunamis is important for risk assessment and management of coastal areas. Obtaining accurate and precise ages of sediments originating from such extreme marine coastal floods is crucial for a reliable estimation of the recurrence interval of these often devastating events. We present here the results of quartz optical dating and 14C dating of two sites (Boca do Rio and Martinhal) on the Algarve coast (southern Portugal). These sites contain deposits of the great tsunami of November 1, 1755. The sections were described using sedimentological techniques; at both sites tsunami-laid sands and gravels were identified, intercalated between estuarine muds. Quartz luminescence ages from these sedimentary successions were derived using standard SAR-OSL dating using multi-grain sub-samples. A multiple sampling strategy was employed with several samples taken from the AD 1755 tsunami deposit and from the sediments bracketing the tsunami layer. Our SAR-OSL protocol was shown to be appropriate using dose recovery measurements (measured/given dose ratio of 1.004 ± 0.007, n = 165). The several OSL ages from the 1755 tsunamigenic deposits are internally reproducible but yield age overestimates of between 20 and 125% (60–310 years respectively); this is in agreement with values reported in the literature for similar deposits. The age overestimation of the tsunami-laid sands is presumably due to the rapid erosion and deposition of older sediments, with insufficient light exposure for complete bleaching during the tsunami event itself. The absence of significant bleaching during the tsunami is also suggested by the shape of the dose distributions based on sub-samples made up of only about 100 grains. Analysis of the distributions with the minimum-age model seems to yield the expected age for two of the three distributions. It is important to note that age offsets of a few tens of years to a few hundred years rapidly become insignificant when dating older (>1 to few ka) tsunami layers.  相似文献   

19.
Fluvial, colluvial, and aeolian sediments were dated by optically stimulated luminescence (OSL) on quartz to improve the chronological framework for Quaternary sedimentation and landscape evolution in the forelands of the Vértes Hills (central Hungary). The separated quartz was suitable for age determination based on an OSL SAR protocol. Most samples have asymmetric equivalent dose distributions and OSL ages were calculated by the mean, central, and minimum De values. Considering geomorphology and earlier age data from the area, the central De values seem most appropriate for age calculation. A fan on the geomorphological level QV in the western foreland of the Vértes Hills was deposited 79–75 (±8) ka ago. In the south-eastern foreland an alluvial fan on level QIIb is at most 42 ± 4 ka old. Fluvial incision and aggradation occurred 16–10 (±1) ka ago on the geomorphic surface QIIa. Loess is 14 ± 1 ka old, and slope sedimentation was active 11–9 (±1) ka ago. Our OSL data demonstrate that in the north-western foreland of the Vértes Hills wind remained an important agent after the last glacial times, into the early Holocene (9–8 ± 1 ka) and was able to accumulate large aeolian dunes.  相似文献   

20.
The Starmoen dune field is part of a larger aeolian system in the Jømna and Glomma river valleys in southeastern Norway. It is believed to have formed just after the last deglaciation in the area, but no absolute ages have been available to support this. Here, we present a set of quartz optically stimulated luminescence (OSL) ages from the aeolian sediments and the underlying glacifluvial deposits. The results show that the main dune-building phase was a short-lived event ∼10 ka ago, likely with a duration less than a few hundred years. This suggests a rapid stabilisation of an initially unstable environment in newly deglaciated terrain. A much younger event with limited and surficial reworking of sand is dated to 770 ± 110 years ago, and the modern age of an active dune provide additional OSL quality control. Age overestimation is found for glacifluvial sediments, probably due to incomplete bleaching as indicated by e.g. scattered dose distributions from small aliquots. OSL measurements were conducted using coarse quartz grains (180–250 m), which show a dominance of a fast signal component.  相似文献   

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