辽宁后仙峪硼矿区古元古代电气石岩: 锆石特征及SHRIMP定年

为了确定辽东硼矿含硼岩系中电气石岩的形成时代, 对后仙峪硼矿区电气石岩首次进行了锆石SHRIMP U-Pb年龄测定.阴极发光图像显示, 锆石具核-边结构, 锆石核部多具振荡环带, 为高Th/U值的岩浆碎屑锆石; 锆石边部无明显结构变化, 为变质成因.岩浆碎屑锆石和变质锆石的年龄分别为2 171~2 175 Ma和1 894~1 906 Ma.结合野外地质和岩相学研究, 认为后仙峪硼矿区电气石岩原岩为古元古代克拉通裂谷环境中源于地壳再循环组分混染的亏损地幔的中酸性岩浆活动引发海底喷流作用的产物, 其原岩形成时代为古元古代中期(2 171~2 175 Ma), 并在稍后(1 894~1 906 Ma)遭受变质作用叠加改造.      

U‒Pb age of detrital zircons from Upper Precambrian deposits of the Sredni and Rybachi peninsulas (northern margin of the Kola Peninsula)

The first U?Pb dates are obtained for detrital zircons from Upper Precambrian deposits of the Sredni (Zemlepakhtinskaya and Kuyakan formations) and Rybachi (Lonskii Formation) peninsulas. The spectra of ages of detrital zircons in sandstone samples from the Zemlepakhtinskaya and Kuyakan formations are similar to a significant extent to each other, which implies the dominant role of the same provenances. Most zircon grains are the Paleoproterozoic and Mesoproterozoic in age; some of them are characterized by Mesoarchean and Neoarchean ages. Zircons dated back to 1.0?2.0 Ga with maxima at approximately 1.8, 1.5, 1.3, and 1.1 Ga are the most abundant. The youngest zircon grains are the Mesoproterozoic in age: 1050 ± 21Ma (i.e., close to the Mesoproterozoic?Neoproterozoic boundary) and 1028 ± 21 Ma from the Zemlepakhtinskaya and Kuyakan formations, respectively. The distribution spectrum of ages obtained for zircons from sandstones of the Lonskii Formation significantly differs from that characteristic of zircons from sandstones of the Zemlepakhtinskaya and Kuyakan formations. The zircon population from the Lonskii Formation is dominated by detrital zircons with Neoarchean and Paleoproterozoic ages (2.8?1.6 Ga); Paleoarchean and Mesoarchean grains are scarce. Their age maxima are registered at levels of approximately 2.7 and 1.8 Ga. The minimum age obtained for zircons from sandstones of the Lonskii Formation (1349 ± 35 Ma) allows the Rybachi block to be considered as being older as compared with the Sredni bock. Crystalline complexes of the Baltic Shield served as a main provenance for the Upper Precambrian deposits of the peninsulas under consideration. The dates obtained for detrital zircons from the Upper Precambrian deposits of the Sredni and Rybachi peninsulas are compared with similar data on the Upper Precambrian sequences of the Timan and Varanger Peninsula areas to reveal differences and similarities in the distribution of ages.     

胶东谭格庄地区奥长花岗质片麻岩和斜长角闪岩的野外地质和锆石SHRIMP定年

对胶东谭格庄地区一地质剖面进行了详细野外观察和锆石SHRIMP年代学研究.剖面主要是由奥长花岗质片麻岩和斜长角闪岩组成,两者互层产出并一起发生褶皱变形,在强变形域两者完全平行化.所以,在强变形地区,不同成分岩性的薄层状互层产出不能作为变质沉积岩的识别标志.奥长花岗质片麻岩(S1105)形成于2496±10Ma,遭受了古元古代早期和晚期变质.两个斜长角闪岩样品(S1238和S0812)都只发育变质锆石,年龄分别为1842±3Ma和1833±13Ma.该剖面岩石记录的两期变质作用在胶东地区具有普遍意义.结合前人研究,作者指出该地区太古宙末存在区域性变质深熔作用,早期地壳受到了强烈的再造;古元古代末的变质作用具有带状分布特点,与造山作用有关.     

U-Pb SHRIMP zircon dating of andesite from the Dolomite area (NE Italy): geochronological evidence for the early onset of Permian Volcanism in the eastern part of the southern Alps

The Athesian Volcanic District (AVD), a thick sequence of andesitic to rhyolitic lava and ignimbrite, overlies both the Variscan basement of the Dolomites and, where present, the continental basal conglomerate of Upper Carboniferous(?) to Early Permian age. This volcanic activity is known to mark the margin of the intra-Pangea megashear system between Gondwana and Laurasia, the onset age of which is determined in this study.SHRIMP U-Pb dating on zircon from Ponte Gardena/Waidbruck (Isarco/Eisack valley) basaltic andesite yields an age of 290.7 ± 3 Ma, providing the oldest record of andesite volcanic activity yet documented in the AVD. Two younger dates (279.9 ± 3.3 and 278.6 ± 3.1 Ma) obtained for the andesitic necks of M. dei Ginepri (Eores/Aferer valley) and Col Quaternà (western Comelico), respectively, probably represent a second pulse of andesite magmatic activity.Near Chiusa/Klausen, the volcanoclastic deposits at the bottom of the Funes/Villnöss valley volcano-sedimentary complex only contain detrital zircons, dated at 469 ± 6 Ma; these probably derive from erosion of Paleozoic porphyroids. Other zircons from the same sediments and inherited cores of magmatic andesite crystals give Paleoproterozoic (1953.6 ± 22.1, 1834.6 ± 69.3, 1773.6 ± 25.1 Ma), Early Neoproterozoic (1015 ± 14 Ma) and Late Neoproterozoic (728.4 ± 9.6, 687.6 ± 7.6 Ma) ages. These ancient detrital and inherited zircon ages fit the model that envisages the Dolomite region as being tectonically coherent with Africa, at least until the Lower Permian.     

SHRIMP Dating and Recrystallization of Metamorphic Zircons from a Granitic Gneiss in the Sulu UHP Terrane

An unusual zircon SHRIMP dating result of a granitic gneiss from the Qinglongshan eclogite-gneiss roadcut section is presented in this paper. The very peculiar and complicated internal structures, as well as the very low Th/U ratios (0.01-0.08) of the zircons indicate that they were formed by metamorphic recrystallization. Strongly in contrast with previously published zircon U-Pb ages of the Dabie-Sulu UHP metamorphic rocks where protolith ages of 600-800 Ma are commonly recorded, only metamorphic age of 218±5 Ma, defined by 18 analytical spots either in rim or in core of zircons, are recorded in this granitic gneiss. This age represents the time of the complete metamorphic recrystallization overprint on primary magmatic zircons. The recrystallization was derived by the UHP metamorphism, and was strengthened by the early stage of retrograde metamorphic fluid activity.     

Zircon U‐Pb/Lu‐Hf and monazite chemical dating of the Tirodi biotite gneiss: implication for latest Palaeoproterozoic to Early Mesoproterozoic orogenesis in the Central Indian Tectonic Zone

In this investigation, we reconstruct the latest Palaeoproterozoic to Early Mesoproterozoic orogenic events along the southern margin of the Central Indian Tectonic Zone (CITZ), using sensitive high resolution ion microprobe (SHRIMP) U‐Pb zircon dating and Lu‐Hf isotope analyses of zircon and Th‐U‐Pb chemical dating of monazite from samples of the Tirodi biotite gneiss (TBG) unit in the Sausar Mobile Belt (SMB), the latter constituting the southernmost litho‐tectonic component of the CITZ. U‐Pb zircon dating of one migmatitic gneiss sample from the type locality of the Tirodi biotite gneiss in the northern domain of the SMB has yielded an age of 1618 ± 8 Ma, which is considered to be the time of magmatic crystallization of its protolith. Combined U‐Pb zircon and monazite chemical dating of two granite gneiss samples from the southern domain of the SMB broadly constrain magmatic crystallization between 1603 ± 23 Ma and 1584 ± 17 Ma and an overprinting metamorphic recrystallization event at 1572 ± 7 Ma. Monazites from the granite gneiss samples also record a terminal metamorphic event at 1415 ± 23 Ma. Lu‐Hf isotopic analyses of zircons reveal fundamentally different source rock reservoirs for the protoliths of these magmatic rocks across the SMB. While the type TBG from the northern domain was derived from an Early Palaeoproterozoic source T(Hf) from 2093 to 2523 Ma, with a mean value at 2379 Ma) of essentially juvenile material with minor crustal components (εHf(t) from −3.3 to + 3.7), the granite from the southern domain had a mature crustal source (εHf(t) from −12.5 to −21.9) of Palaeoarchaean age T(Hf) from 3051 to 3630 Ma, with a mean value at 3218 Ma). When integrated with metamorphic information previously obtained from the 1.6 Ga ultra‐high temperature granulite facies metamorphic event in the SMB, the discrete magmatic and metamorphic events between 1.62/1.60 Ga and 1.42 Ga can be correlated with the formation of an Early Mesoproterozoic accretionary orogen in the CITZ. Copyright © 2011 John Wiley & Sons, Ltd.     

鄂尔多斯盆地西北缘晚三叠世早期物源组成

利用碎屑锆石LA?ICP?MS U?Pb测年方法,对鄂尔多斯盆地西缘北部贺兰山炭井沟、插旗沟和中部磁窑堡3个地区晚三叠世早期的物源进行分析。结果表明:研究区部分碎屑锆石阴极发光（CL）图像具有环带结构,大部分锆石Th/U值大于0.4,极少部分小于0.1,表明锆石来源以岩浆为主,变质为次。3个地区锆石年龄分布均有三组年龄峰值:古元古代早期—新太古代（2 204.3~2 610.1 Ma）、古元古代（1 667~2 171.8 Ma）和晚古生代（245.1~322.6 Ma）,这3组年龄分别与新太古代末华北克拉通化的基本完成、古元古代晚期华北克拉通三大陆块（阴山陆块、鄂尔多斯陆块和东部陆块）之间的相互碰撞拼合以及晚古生代古亚洲洋向华北板块俯冲而形成的构造岩浆事件相对应。结合锆石年龄对比和岩相古地理分析得知,鄂尔多斯盆地西北缘晚三叠世早期物源来自北部和西北部地区,主要为古元古代孔兹岩带和阿拉善地块的变质岩和岩浆岩,其次为华北板块西部基底的岩浆岩和阿拉善地块海西期的岩浆岩。     

Zirconology of ultrabasic rocks of the Karabash massif (Southern Urals)

Dating of zircon (SHRIMP) from dunite and harzburgite of the Karabash massif was carried out for the first time. Relics of ancient crystals (1940 ± 30 Ma in harzburgite, 1860 ± 16 Ma in dunite) provide evidence for the Paleoproterozoic age of the protolith. The morphological peculiarities of zircon crystals allow us to assume differentiation of the magmatic source 1720 m. y. ago. The major variety of zircons indicates stages of metamorphic evolution in the Neoproterozoic (530–560 Ma) and Early–Late Ordovician (440–480 Ma).     

胶北早前寒武纪变质基底多期岩浆-变质热事件:来自TTG片麻岩和花岗质片麻岩中锆石U-Pb定年的证据

本文采用LA-ICP-MS技术,对胶北地体TTG片麻岩和花岗质片麻岩中锆石进行系统原位U-Pb定年和稀土、微量元素的分析,发现研究区早前寒武变质结晶基底存在多期岩浆-变质热事件。4件TTG片麻岩和2件花岗质片麻岩锆石样品记录了2909±13Ma、2738±23Ma、2544±15~2564±12Ma和2095±12Ma 4组岩浆事件年龄,以及2504±16~2513±32Ma和1863±41Ma 2组变质事件年龄。结合以往TTG片麻岩和花岗质片麻岩的地球化学及Nd同位素研究发现,约2738Ma的TTG岩浆事件可能代表胶北地体地壳最主要的生长事件,而2544~2564Ma的岩浆事件则可能代表古老地壳重熔的最强烈岩浆事件,约2095Ma岩浆事件则反映了胶-辽-吉构造带内部在该时期与地壳拉张作用有关的岩浆活动。2504~2513Ma是研究区以及华北克拉通早前寒武基底最主要的一期变质热事件,可能与地幔柱(热点)岩浆的底侵作用有关,而TTG片麻岩记录的约1863Ma的变质年龄与研究区基性和泥质高压麻粒岩相岩石记录的麻粒岩相变质时代一致,暗示TTG片麻岩可能也经历了古元古代高压麻粒岩相变质作用,上述研究进一步表明胶北地体在古元古代的确存在一期陆-陆碰撞的重要造山事件。该项研究成果对于进一步深入探讨胶北乃至华北克拉通早前寒武纪变质基底的形成演化、岩浆-变质热事件序列及其构造背景具有重要的科学意义。     

东阿拉善地块叠布斯格杂岩的形成与变质时代:来自黑云斜长片麻岩锆石LA-ICP-MS U-Pb定年的新证据

叠布斯格杂岩作为阿拉善地块变质程度最高、形成时代最老的变质岩系,是进一步深入认识阿拉善地块形成、演化与构造亲缘性的最佳对象.本文对叠布斯格杂岩中黑云斜长片麻岩开展了系统的野外地质调查、岩相学观察和锆石U-Pb年代学研究.碎屑锆石U-Pb定年和野外地质调查表明,叠布斯格杂岩中黑云斜长片麻岩碎屑锆石年龄介于2 177~2 010 Ma,最小年龄峰值为2 050 Ma,结合变质锆石年龄数据,限定其沉积时代在2 050~1 969 Ma之间.区域对比研究表明,阿拉善地块叠布斯格杂岩中黑云斜长片麻岩与西阿拉善地块龙首山杂岩、华北克拉通孔兹岩带（尤其是孔兹岩带西部）中的变沉积岩系在沉积时代与源区特征上具有高度的一致性.此外,变质锆石U-Pb定年和微量元素分析表明,叠布斯格杂岩中黑云斜长片麻岩记录了古元古代晚期1 969~1 811 Ma连续的变质年龄.对比分析阿拉善地块与孔兹岩带变沉积岩系的碎屑锆石年龄谱系-变质时代表明,阿拉善地块与孔兹岩带在古元古代可能具有相同的沉积-变质演化历史,在古元古代期间阿拉善地块应是华北克拉通孔兹岩带的西延部分.      

Unusual Uranium‐rich Fluid Flow During Exhumation of Deeply Subducted Continental Crust

In‐situ SIMS analyses of O and U‐Pb isotopes were carried out for zircons from a quartz vein hosted by ultrahigh‐pressure metagranite (UHP) in the Dabie orogen. The results are integrated to decipher the property of unusual U‐rich aqueous fluids and their effects on both metamorphic and magmatic zircons during exhumation of the UHP metagranite. In CL images, most zircon grains show distinct core‐rim structures. Relict cores are bright and exhibit oscillatory or patchy zonation, giving Neoproterozoic upper‐intercept ages of 795 ± 26 Ma. Newly grown rims are dark and exhibit no zoning, yielding Triassic concordant ages of 215 ± 5 Ma. The cores give Th contents of 59 to 463 ppm and U contents of 98 to 558 ppm, with Th/U ratios of 0.263 to 1.423. The rims yield reduced Th contents of 11 to 124 ppm but significantly elevated U contents of 1051 to 3531 ppm, with Th/U ratios of 0.010 to 0.035. Comparison with the cores of magmatic origin, the unusual enrichment in U but depletion in Th in the rims of metamorphic origin are interpreted as zircon growth from Cl‐rich oxidized vein‐forming aqueous fluids that were produced by dehydration reactions of the wallrock during continental exhumation. The cores have variably positive δ¹⁸O values with concordant or discordant Neoproterozoic U‐Pb ages, suggesting their solid‐state modification of both O and U‐Pb isotopes through interaction with the fluids. The rims yield negative δ¹⁸O values, indicating their growth from the negative δ¹⁸O fluids. Taken together, the proposed Cl‐rich oxidized negative‐δ¹⁸O vein‐forming aqueous fluids have such an ability to not only cause variable metamorphic recrystallization in the relict magmatic zircons but also produce dramatic fractionation of U over Th in the metamorphic zircons during quartz veining, and potentially impact on the overlain metasomatite in the mantle wedge.     

华北克拉通北缘化德群中碎屑锆石的LA-ICP-MS U-Pb年龄及其构造意义

化德群出露地区位于华北克拉通北缘中部,紧邻中亚造山带南缘,呈近东西向展布。在它的西边是早-中元古代的白云鄂博裂谷和渣尔泰—狼山裂谷,东南面是由长城系、蓟县系和青白口系组成的早-新元古代的燕辽裂陷槽,南边分布着1.9~1.8Ga麻粒岩相变质的丰镇群（孔兹岩系）,北边出露有代表中亚造山带的古生代岩石。化德群由一套浅变质和未变质的沉积岩组成,无火山岩夹层。地层序列包含多个沉积旋回,每个旋回自下而上为含砾砂岩、砂岩、碳酸盐岩和泥质岩。岩石组合反映了从河流—滨海—浅海相的沉积环境。化德群的地层序列可以和白云鄂博群及渣尔泰群相对比。本文对化德群四个变质砂岩样品中的碎屑锆石进行了LA-ICP-MS U-Pb年龄测定,年龄主要集中在1800±50Ma和1850±50Ma,另外还有~2500Ma和~2000Ma的次要峰值。化德群底部变质含砾云母长石石英砂岩中碎屑锆石的最小谐和年龄是1758±7Ma,限定了化德群沉积时代的下限。碎屑锆石的CL图像显示,1800±50Ma和1850±50Ma的锆石主要是变质成因,少量岩浆成因,说明化德群的源区主要是古元古代的变质岩,少量岩浆岩。~2500Ma和~2000Ma的碎屑锆石代表了更为古老的源区。碎屑锆石的U-Pb年龄限制了化德群的沉积时代为古元古代晚期—中元古代,年龄峰值对应华北克拉通的重要构造热事件,而无与中亚造山带地质事件相关的年龄信息。沉积组合特征表明化德群属于稳定的浅水—半深水沉积盆地。化德盆地、渣尔泰—狼山盆地和白云鄂博盆地共同构成华北克拉通北缘的被动陆缘裂谷系,该裂谷系的形成可能与燕辽及熊耳裂陷槽的打开是同时期的。因此,华北克拉通的北界应该置于化德群出露区域以北。基于锆石特征的详细分析及对比,我们认为化德群以南的孔兹岩系可能是化德群的主要源区。     

贺兰山孔兹岩系的变质时代及其对华北克拉通西部陆块演化的制约

贺兰山孔兹岩系作为华北克拉通西部孔兹岩带的重要组成部分,其变质时代问题一直悬而未决.利用SHRIMP锆石U-Pb定年技术,对贺兰山孔兹岩系中3个代表性富铝片麻岩(石榴堇青钾长片麻岩、石榴堇青二长片麻岩与石榴黑云斜长片麻岩)样品进行了精确定年.发现这3种岩石虽处不同层位,但其碎屑锆石年龄却非常集中,各测点207Pb/206Pb年龄总体变化在2.0～2.1Ga之间,加权平均年龄则在2017～2040Ma之间.这些碎屑锆石都具有岩浆结构特征,反映当时曾存在大规模花岗质岩浆活动,所成岩体为孔兹岩系沉积提供了充足物源.另有少量大于2.5Ga的碎屑锆石(2520～2949Ma),表明本区存在太古代岩浆活动记录.本区石榴堇青二长片麻岩中发育典型的变质增生锆石,其成因很可能与黑云母的脱水熔融反应有关.利用该锆石确定贺兰山孔兹岩系的变质时代为1950±8Ma.该时代与东部大青山、乌拉山孔兹岩系变质时代相同,表明华北克拉通西部的阴山地块与鄂尔多斯地块大体是以平行的方式正面拼贴到一起的,形成了目前的孔兹岩带.     

小兴安岭“晚古生代”地层的时代与物源：地质与碎屑锆石 U-Pb 年代学证据

本文对出露于小兴安岭的"晚古生代"红山组和黑龙宫组进行了碎屑锆石LA-ICP-MS U-Pb定年,旨在准确限定红山组和黑龙宫组的沉积时限,并揭示其物源组成。样品中大多数锆石呈自形—半自形,显示典型的岩浆生长环带或条痕状吸收,暗示其岩浆成因。研究结果显示,采自红山组标准剖面泥板岩中的碎屑锆石42个分析点产生以下年龄峰值:747、807、849、903、956、1 167和1 811 Ma,表明红山组沉积于747 Ma之后;采自伊春地区黑龙宫组泥板岩中的碎屑锆石97个分析点产生以下年龄峰值:700(发生Pb丢失)、805、902、1 764、2 446和2 467Ma,确定黑龙宫组沉积于805Ma之后。近年来在该地区"晚古生代"地层中碎屑锆石的定年结果显示普遍存在561 Ma年龄,鉴于红山组和黑龙宫组中缺乏上述锆石年龄组合,认为研究区的红山组和黑龙宫组的形成时代分别为747~561 Ma和805~561 Ma,时代置于新元古代。基于两组碎屑锆石的年龄频数和区域地质年代学资料的对比分析,两个地层单元中出现大量新元古代岩浆锆石,证明研究区可能存在新元古代岩浆事件,岩浆产物为两组地层提供物源;而中—古元古代碎屑锆石的存在,同时暗示该区沉积时地表或地表浅部应存在更为古老的前寒武纪残片。     

浙西南八都群古元古代和三叠纪变质和岩浆事件的年代学证据

本文对华夏地块浙西南八都群片麻岩和侵入其中的花岗岩进行了系统的岩石学、地球化学、LA-ICP-MS锆石U-Pb年代学以及Lu-Hf同位素研究。结果表明,八都群片麻岩中的碎屑锆石普遍发育~1882 Ma的(变质)增生边,而侵入八都群花岗岩的结晶时代集中在1861~1841 Ma。综合本文及前人获得的岩石学和同位素年代学数据可知,华夏地块在古元古代晚期(1890~1850Ma)发生了一次强烈的造山事件,该期造山很可能与Columbia超大陆的聚合作用密切相关,华夏地块可能为Columbia超大陆的一个陆块。除此之外,本研究还在八都杂岩中获得了三叠纪变质锆石年龄(235±1)Ma,综合前人发表资料可知,这些古元古代基底岩石遭受了强烈的印支期改造,可能与华南大陆印支期造山作用相关。然而,关于古元古代基底的三叠纪变形变质、抬升和出露过程及其与印支期构造演化的内在联系,仍有待进一步研究。     

大兴安岭中段乐平统-中三叠统沉积物源分析:来自重矿物组合及碎屑锆石年代学证据

黑龙江西部龙江地区位于中亚造山带东段,黑河-贺根山缝合带与西拉木伦缝合带之间,地层记录了两大古板块之间古亚洲洋闭合过程的信息。本文对龙江地区乐平统林西组和下-中三叠统老龙头组的砂岩样品进行碎屑重矿物和碎屑锆石U-Pb同位素年代学研究。碎屑重矿物组合以锆石+磷灰石+金红石+角闪石+绿帘石+重晶石的组合为特征,表明物源主要来自于中酸性岩浆岩,并有少量变质岩及沉积岩组分。林西组样品最年轻的锆石年龄为278±3Ma,老龙头组样品最年轻的锆石年龄为247±3Ma、243±4Ma及237±3Ma,结合前人的研究,限定了林西组沉积于乐平世,老龙头组沉积于早三叠世-中三叠世。碎屑锆石年龄谱明显分为五组:237～258Ma、270～329Ma、357～558Ma、680～1633Ma及1893～1966Ma。其中237～258Ma的碎屑锆石主要来自与古亚洲洋洋壳消亡前的俯冲增生过程相关的火山活动,270～329Ma的碎屑锆石主要来自大石寨组火山岩及其同期侵入岩,357～558Ma的碎屑锆石来自早古生代-晚古生代早期岩浆弧,680～1633Ma的碎屑锆石可能来自兴安及额尔古纳地块的变质基底,而较古老的～1800Ma的锆石年龄暗示了华北克拉通基底的物源信息。通过研究发现林西组及老龙头组样品前30%年轻的碎屑锆石年龄与地层沉积年龄之差都小于100Ma,结合对砂岩碎屑组成、重矿物组合及盆地与火山弧位置关系的研究,认为研究区乐平世-中三叠世沉积盆地具有汇聚背景,为弧前盆地。     

西南天山科桑溶洞新元古代-早奥陶世花岗岩锆石U-Pb年代学研究

在新疆西南天山科桑溶洞地区,新厘定出一套斜长角闪岩-花岗岩地质单元:侵入斜长角闪岩中的新元古代白云母花岗岩(片麻状构造)、以及侵入上述古老岩石单元的早奥陶世花岗岩(块状构造)。片麻状白云母花岗岩中锆石具有热液锆石边、岩浆锆石幔和碎屑锆石核(边-幔-核结构),剔除被热液锆石和碎屑锆石混染的SHRIMP测点,获得岩浆锆石幔的加权平均年龄752.3±5.1Ma(MSWD=0.95),代表岩浆的结晶年龄。块状花岗岩的锆石具有边-核结构,热液锆石边的U-Pb年龄(419.5±5.7Ma)明显偏低。剔除热液锆石和碎屑锆石,获得岩浆锆石的平均U-Pb年龄481.1±4.4Ma(MSWD=0.88),代表花岗岩的结晶年龄。早奥陶世早期,岩浆侵入新元古代片麻状白云母花岗岩中。在晚志留世或者更晚时期,两类花岗岩共同经受了变质热液改造,变质流体交代岩浆锆石,导致锆石溶蚀再生长。     

黑龙江省东部早古生代地层的确定:地质与碎屑锆石U-Pb年代学证据

通过研究黑龙江省东部早古生代地层晨明组和宝泉组碎屑锆石的U-Pb定年结果,讨论了晨明组和宝泉组的所属时代和物源.大多数锆石呈自形-半自形晶,显示出典型的岩浆生长环带或条痕状吸收,暗示其岩浆成因,极少数的锆石具有经变质作用形成的暗色增生边.定年结果表明:采自晨明组上部长石石英砂岩中碎屑锆石59个分析点产生了以下年龄组:561 Ma、621 Ma、683 Ma、752 Ma、803 Ma、822 Ma、851 Ma、900 Ma、922 Ma、954 Ma、1 781 Ma、1 865 Ma和1 933 Ma,这表明晨明组沉积于561 Ma之后.而以不整合接触关系覆盖于晨明组之上的宝泉组底部泥质板岩中碎屑锆石60个分析法点产生了425 Ma、450 Ma、485 Ma、900 Ma和1 750 Ma年龄众数.由上述地质关系和年代学测定结果,结合晚古生代地层中碎屑锆石的年龄组合,可以判定位于黑龙江省东部地区晨明组的形成时代介于561~510 Ma之间,这是首次在黑龙江省东部确定的具有确切年代学证据的早古生代地层.上述年龄组碎屑锆石的存在,表明其物源主要为该区新元古代和古元古代的地质体,这进一步揭示在早古生代期间,松嫩-张广才岭地块东缘可能存在前寒武纪残片.      

辽东弓长岭—岫岩地区古元古界辽河群变沉积岩的物源及构造背景

辽东弓长岭—岫岩地区位于胶—辽—吉造山带东段,区内发育厚层古元古代变质沉积岩系,本文对这些变质沉积岩进行了岩相学和U-Pb年代学等方面的研究。岩相学特征显示这些岩石变质程度普遍偏低,多为绿片岩相变质条件,未发现高级特征变质矿物。岩石中主要矿物颗粒为石英,其中北辽河群碳酸盐矿物较为发育。根据辽东弓长岭-岫岩地区古元古代变沉积岩碎屑锆石阴极发光（CL）图像,这些锆石普遍具有清晰的振荡环带和较高的Th/U值（>0.3）,表明其原岩来自岩浆岩。结合LA-ICP-MS U-Pb年代学,得到里尔峪组、高家峪组、大石桥组和盖县组碎屑锆石分别呈现出2 159、2 500、2 189/2 530和2 044/2 197 Ma的年龄峰值,表明其沉积物来源于古元古代花岗质岩石和相邻的太古宙杂岩。结合前人资料,本文认为南、北辽河岩群形成于相同的环境并经历了相同的构造演化过程,古元古代弧-陆碰撞模式可能更适用于胶—辽—吉造山带的构造演化。     

阿尔金江尕勒萨依榴辉岩和围岩锆石LA-ICP-MS微区原位定年及其地质意义

阿尔金江尕勒萨依榴辉岩及其直接围岩——石榴子石黑云母片麻岩锆石的阴极发光图像、微区原位LA-ICP-MS微量元素分析研究表明,榴辉岩锆石内部结构比较均匀,少数颗粒保留斑杂状残核;位于锆石斑杂状残核测点的重稀土相对富集,Th/U比值多大于0.4,为岩浆锆石的特征;位于锆石边部与内部结构均匀颗粒上的测点显示HREE近平坦型或弱亏损型的稀土配分模式,显示了与石榴石平衡共生的变质锆石特征;而石榴子石黑云母片麻岩的锆石具有核-幔-边结构,核部为碎屑锆石,幔部则为与石榴石平衡共生的变质锆石。LA-ICP-MS微区定年获得榴辉岩的变质年龄为(493±4.3)Ma,其原岩形成年龄为(754±9)Ma;石榴子石黑云母片麻岩的变质年龄为(499±27)Ma。榴辉岩的变质年龄滞后于其原岩的形成年龄约250Ma,并且榴辉岩与其直接围岩副片麻岩的变质年龄几乎完全一致,充分表明该超高压榴辉岩的形成是陆壳深俯冲作用的产物。