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1.
Abstract Five whole-rock 40Ar/39Ar plateau ages from low-grade sectors of the Sambagawa belt (Besshi nappe complex) range between 87 and 97 Ma. Two whole-rock phyllite samples from the Mikabu greenstone belt record well-defined 40Ar/39Ar plateau ages of 96 and 98 Ma. Together these ages suggest that a high-pressure metamorphism occurred in both the Sambagawa and Mikabu belts at c. 90–100 Ma. The northern Chichibu sub-belt may consist of several distinct geochronological units because metamorphic ages increase systematically from north ( c. 110 Ma) to south ( c. 215 Ma). The northern Chichibu sub-belt is correlated with the Kuma nappe complex (Sambagawa belt). Two whole-rock phyllite samples from the Kurosegawa terrane display markedly older metamorphic ages than either the Sambagawa or the Chichibu belts.
Accretion of Sambagawa-Chichibu protoliths began prior to the middle Jurrasic. Depositional ages decrease from middle Jurassic (Kuma-Chichibu nappe complex) to c. 100 Ma (Oboke nappe complex) toward lower tectonostratigraphic units. The ages of metamorphic culmination also decrease from upper to lower tectonostratigraphic units. The Kurosegawa belt and the geological units to the south belong to distinctly different terrances than the Sambagawa-Chichibu belts. These have been juxtaposed as a result of transcurrent faulting during the Cretaceous.  相似文献   

2.
Abstract 40Ar/39Ar data collected from hornblende, muscovite, biotite and K-feldspar constrain the P-T-t history of the Cordillera Darwin metamorphic complex, Tierra del Fuego, Chile. These data show two periods of rapid cooling, the first between c. 500 and c. 325° C at rates ≥25° C Ma-1, and the second between c. 250 and c. 200°C. For high-T cooling, 40Ar/39Ar ages are spatially disparate and depend on metamorphic grade: rocks that record deeper and hotter peak metamorphic conditions have younger 40Ar/39Ar ages. Sillimanite- and kyanite-grade rocks in the south-central part of the complex cooled latest: 40Ar/39Ar Hbl = 73–77 Ma, Ms = 67–70 Ma, Bt = 68 Ma, and oldest Kfs = 65 Ma. Thermobarometry and P-T path studies of these rocks indicate that maximum burial of 26–30 km at 575–625° C may have been followed by as much as 10 km of exhumation with heating of 25–50° C. Staurolite-grade rocks have intermediate 40Ar/39Ar ages: Hbl = 84–86 Ma, Ms = 71 Ma, Bt = 72–75 Ma, and oldest Kfs = 80 Ma. Thermobarometry on these rocks indicates maximum burial of 19–26 km at temperatures of 550–580° C. Garnet-grade rocks have the oldest ages: Ms = 72 Ma and oldest Kfs = 91 Ma; peak P-T conditions were 525–550° C and 5–7 kbar. Regional metamorphic temperatures for greenschist facies rocks south of the Beagle Channel did not exceed c. 300–325° C from 110 Ma to the present, although the rocks are only 2 km from kyanite-bearing rocks to the north. One-dimensional thermal models allow limits to be placed on exhumation rates. Assuming a stable geothermal gradient of 20–25° C km-1, the maximum exhumation rate for the St-grade rocks is c. 2.5 mm yr-1, whereas the minimum exhumation rate for the Ky + Sil-grade rocks is c. 1.0 mm yr-1. Uniform exhumation rates cannot explain the disparity in cooling histories for rocks at different grades, and so early differential exhumation is inferred to have occurred. Petrological and geochronological comparisons with other metamorphic complexes suggest that single exhumation events typically remove less than c. 20 km of overburden. This behaviour can be explained in terms of a continental deformation model in which brittle extensional faults in the upper crust are rooted to shallowly dipping ductile shear zones or regions of homogeneous thinning at mid- to deep-crustal levels. The P-T-t data from Cordillera Darwin (1) are best explained by a ‘wedge extrusion’model, in which extensional exhumation in the southern rear of the complex was coeval with thrusting in the north along the margin of the complex and into the Magallanes sedimentary basin, (2) suggest that differential exhumation occurred initially, with St-grade rocks exhuming faster than Ky + Sil-grade rocks, and (3) show variations in cooling rate through time that correlate both with local deformation events and with changes in plate motions and interactions.  相似文献   

3.
The Yinshan deposit in the Jiangnan tectonic belt in South China consists of Pb‐Zn‐Ag and Cu‐Au ore bodies. This deposit contains approximately 83 Mt of the Cu‐Au ores at 0.52% Cu and 0.8 g/t Au, and 84 Mt of the Pb‐Zn‐Ag ores at 1.25% Pb, 1.02% Zn and 33.3 g/t Ag. It is hosted by low‐grade metamorphosed sedimentary rocks and mafic volcanic rocks of the lower Mesoproterozoic Shuangqiaoshan Group, and continental volcanic rocks of the Jurassic Erhuling Group and dacitic subvolcanic rocks. The ore bodies mainly consist of veinlets of sulfide minerals and sulfide‐disseminated rocks, which are divided into Cu‐Au and Pb‐Zn‐Ag ore bodies. The Cu‐Au ore bodies occur in the area close to a dacite porphyry stock (No. 3 stock), whereas Pb‐Zn‐Ag bodies occur in areas distal from the No. 3 stock. Muscovite is the main alteration mineral associated with the Cu‐Au ore bodies, and muscovite and chlorite are associated with the Pb‐Zn‐Ag ores. A zircon sensitive high‐resolution ion microprobe U‐Pb age from the No. 3 dacite stock suggests it was emplaced in Early Jurassic. Three 40Ar‐39Ar incremental‐heating mineral ages from muscovite, which are related to Cu‐Au and Pb‐Zn‐Ag mineralization, yielded 179–175 Ma. These muscovite ages indicate that Cu‐Au mineralization occurred at 178.2±1.4 Ma (2σ), and Pb‐Zn‐Ag mineralization at 175.4±1.2 Ma (2σ) and 175.3±1.1 Ma (2σ), which supports a restricted period for the mineralization. The Early Jurassic ages for the mineralization at Yinshan are similar to that of the porphyry Cu mineralization at Dexing in Jiangnan tectonic belt, and suggest that the polymetallic mineralization occurred in a regional transcompressional tectonic regime.  相似文献   

4.
Abstract. Ages for thirty adularia samples collected from various veins were in the Hishikari gold deposit determined by 40Ar/39Ar dating to constrain the timing of adularia‐quartz vein formation and to determine the temporal change in temperature of hydrothermal fluid. Plateau ages were obtained from all adularia samples, and significant excess 40Ar is not recognized from inverse isochrones. The duration of mineralization within individual veins was determined by adularia ages from the early and late stages of mineralization within the same vein. The durations of mineralization in the Daisen‐1, Daisen‐3, Hosen‐2 and Keisen‐3 veins in the Honko‐Sanjin zone were 7,000, 140,000, 160,000 and 170,000 years, respectively. The durations of mineralization in the Seisen‐2 and Yusen‐1–2 veins in the Yamada zones were 360,000 and 320,000 years, respectively. Mineralization lasted for a relatively longer period in individual veins at the Yamada zone. Mineralization ages from the Honko‐Sanjin zone range from 1.04 to 0.75 Ma, and most mineralization ages are concentrated in a short period from 1.01 to 0.88 Ma. In contrast, mineralization ages for the Yamada zone range from 1.21 to 0.64 Ma. These results indicate that fracturing and subsequent vein formation lasted for a longer period in the Yamada zone (about 570,000 years) compared with those events in the Honko‐Sanjin zone (about 290,000 years). The homogenization temperatures of liquid‐rich fluid inclusions in columnar adularia used for age determination were determined to be 223°C on average, and most of these temperatures range from 180 to 258d?C. No significant temporal change in homogenization temperature is recognized in this study. However, adularia in the Keisen veins indicated higher homogenization temperatures compared with elsewhere in the deposit, suggesting that the principal ascent of mineralizing hydrothermal fluid was via the Keisen veins.  相似文献   

5.
Abstract Petrological, oxygen isotope and 40Ar/39Ar studies were used to constrain the Tertiary metamorphic evolution of the lower tectonic unit of the Cyclades on Tinos. Polyphase high-pressure metamorphism reached pressures in excess of 15 kbar, based on measurements of the Si content in potassic white mica. Temperatures of 450–500° C at the thermal peak of high-pressure metamorphism were estimated from critical metamorphic assemblages, the validity of which is confirmed by a quartz–magnetite oxygen isotope temperature of 470° C. Some 40Ar/39Ar spectra of white mica give plateau ages of 44–40 Ma that are considered to represent dynamic recrystallization under peak or slightly post-peak high-pressure metamorphic conditions. Early stages in the prograde high-pressure evolution may be documented by older apparent ages in the high-temperature steps of some spectra. Eclogite to epidote blueschist facies mineralogies were partially or totally replaced by retrograde greenschist facies assemblages during exhumation. Oxygen isotope thermometry of four quartz–magnetite pairs from greenschist samples gives temperatures of 440–470° C which cannot be distinguished from those deduced for the high-pressure event. The exhumation and overprint is documented by decreasing ages of 32–28 Ma in some greenschists and late-stage blueschist rocks, and ages of 30–20 Ma in the lower temperature steps of the Ar release patterns of blueschist micas. Almost flat parts of Ar–Ar release spectra of some greenschist micas gave ages of 23–21 Ma which are assumed to represent incomplete resetting caused by a renewed prograde phase of greenschist metamorphism. Oxygen isotope compositions of blueschist and greenschist facies minerals show no evidence for the infiltration of a δ18O-enriched fluid. Rather, the compositions indicate that fluid to rock ratios were very low, the isotopic compositions being primarily controlled by those of the protolith rocks. We assume that the fundamental control catalysing the transformation of blueschists into greenschists and the associated resetting of their isotopic systems was the selective infiltration of metamorphic fluid. A quartz–magnetite sample from a contact metamorphic skarn, taken near the Miocene monzogranite of Tinos, gave an oxygen isotope temperature of 555° C and calculated water composition of 9.1%. The value of δ18O obtained from this water is consistent with a primary magmatic fluid, but is lower than that of fluids associated with the greenschist overprint, which indicates that the latter event cannot be directly related to the monozogranite intrusion.  相似文献   

6.
Abstract 40Ar/39Ar step-heating and single-grain laser fusion ages from phengites from the polydeformed and polymetamorphosed blueschist-greenschist facies Nome Group fall into two groups. Samples from the upper part of the structural section that have experienced a relatively weak metamorphic and deformational post-blueschist facies overprint and one sample from the Cape Nome orthogneiss yield plateau ages of 116-125 Ma. More intensely overprinted samples yield hump-shaped spectra with minimum ages of 123 Ma and maximum ages of 334 Ma. Samples with hump-shaped spectra are derived from a greater structural depth than most samples with plateau ages. Unreasonably old maximum ages from some of the disturbed spectra suggest that the hump-shaped spectra result from the incorporation of excess 40Ar. This interpretation conflicts with previous interpretations of similarly disturbed spectra from the Brooks Range, which have been argued to provide minimum ages for blueschist facies metamorphism. Since the maximum temperatures achieved by all samples were probably above the blocking temperature of Ar in phengite, the 116-125 Ma plateau ages are a minimum age for blueschist facies metamorphism on the Seward Peninsula, Alaska.  相似文献   

7.
Abstract The Sambagawa metamorphic belt exposed in central Shikoku records a high-P–T metamorphic event. It is represented by the Oboke nappe and structurally overlying, internally imbricated, Besshi nappe complex. These major structural units are in ductile thrust contact. A melange is developed along a ductile internal tectonic contact within the Besshi nappe complex. Tectonic emplacement of a high-T enclave (Sebadani eclogite) in the melange zone resulted in the development of a contact metamorphic aureole within the host Sambagawa rocks. 36Ar/40Ar versus 39Ar/40Ar isotope correlation ages recorded by hornblende from the Sambagawa basic schists which surround the Sebadani enclave are 83.4 ± 0.3 Ma (within contact aureole) and 83.6 ± 0.5 Ma (outside aureole). 40Ar/39Ar plateau ages recorded by muscovite from the same samples are 87.9 ± 0.3 and 89.3 ± 0.4 Ma. Amphibole from the amphibolite within the Sebadani enclave records isotope correlation ages of 93.7 ± 1.1 and 96.5 ± 0.7 Ma (massive interior) and 84.6 ± 1.2 Ma (marginal shear zone). Amphibole within the massive amphibolite is significantly higher in XMg than that within the host Sambagawa basic schists. The older ages recorded by amphibole within the Sebadani enclave are interpreted to date cooling through somewhat higher closure temperatures than which characterize the more Fe-rich amphibole in surrounding schists. The younger amphibole age recorded within the marginal shear zone probably indicates that crystallization of amphibole continued until cooling through the relatively lower amphibole closure temperatures. These results, together with the previously published 40Ar/39Ar ages of the Sambagawa schists, suggest: (i) metamorphic culmination occurred in the Besshi nappe complex at c. 100–90 Ma; (ii) at c. 95 Ma the Besshi nappe complex was internally imbricated and tectonic enclaves were emplaced; (iii) at c. 85 Ma, the composite Besshi nappe was rapidly exhumed and tectonically emplaced over the Oboke nappe (which attained peak metamorphic conditions at c. 75 Ma); (iv) the Besshi and Oboke nappe complexes were further exhumed as a coherent tectonic unit and unconformably overlain by the Eocene Kuma Group at c. 50 Ma.  相似文献   

8.
Abstract 40Ar/39Ar age spectrum analysis of phengite separates from Naxos, part of the Attic Cycladic Metamorphic Belt in Greece, indicates that cooling following high-pressure, low- to medium-temperature metamorphism, M1, occurred about 50 Ma ago. Phengite has 40Ar* gradients that suggest that part of the scatter observed in conventional K–Ar ages was caused by diffusion of radiogenic argon from the minerals during a younger metamorphism, M2. In central Naxos, this metamorphism (M2) has overprinted the original mineral assemblages completely, and is associated with development of a thermal dome. Excellent 40Ar/39Ar plateaus at 15.0 ± 0.1 Ma, 11.8 ± 0.1 Ma, and 11.4 ± 0.1 Ma, obtained on hornblende, muscovite and biotite, respectively, from the migmatite zone, indicate that relatively rapid cooling followed the M2 event, and that no significant thermal overprinting occurred subsequent to M2. Toward lower M2 metamorphic grade, 40Ar/39Ar plateau ages of hornblendes increase to 19.8 ± 0.1 Ma; concomitantly the proportion of excess 40Ar in the spectra increases as well. We propose that the peak of M2 metamorphism occurred beween 15.0 and 19.8 Ma ago. K–Ar ages of biotites from a granodiorite on the west coast are indistinguishable from those found in the metamorphic complex, and hornblende K–Ar ages from the same samples are in the range 12.1–13.6 Ma. As the latter ages are somewhat younger than most ages obtained from the metamorphic complex, intrusion of the granodiorite most likely followed the peak of the M2 metamorphism. The metamorphic evolution of Naxos is consistent with rapid crustal thickening during the Cretaceous or early Tertiary, causing conditions at which supracrustal rocks experienced pressures in the range 900–1500 MPa. Transition to normal crustal thicknesses ended the M1 metamorphism about 50 Ma ago. The M2 metamorphism and granodiorite intrusion occurred during a period of heat input into the crust, possibly related to the migration of the Hellenic volcanic ar°C in a southerly direction through the area.  相似文献   

9.
Abstract The St Malo region in north-west France contains migmatites and anatectic granites derived by partial melting of metasedimentary protoliths during Cadomian orogenesis at c. 540 Ma. Previously reported Rb–Sr model ages for muscovite and biotite range from c. 550 to c. 300 Ma, and suggest variable resetting of mineral isotopic systems. These rocks display microscopic evidence for variably intense Cadomian intracrystalline plastic strain but record no obvious evidence of penetrative Palaeozoic regional deformation. 40Ar/39Ar mineral ages have been determined to evaluate better the extent, timing and significance of Palaeozoic overprinting. Eleven muscovite concentrates and one whole-rock phyllite have been prepared from various units exposed in the St Malo and adjacent Mancellian regions. In the Mancellian region, muscovite from two facies of the Bonnemain Granite Complex record 40Ar/39Ar plateau ages of c. 527 and 521 Ma. An internally discordant 40Ar/39Ar release spectrum characterizes muscovite from protomylonitic granite within the Cadomian Alexain-Deux Evailles-Izé Granite Complex, and probably records the effects of Variscan displacement along the North Armorican Shear Zone. Muscovite concentrates from anatectic granite and from Cadomian mylonites along ductile shear zones within the north-western sector of the St Malo region exhibit internally discordant 40Ar/39Ar release spectra which suggest variable and partial late Palaeozoic rejuvenation. By contrast, muscovite concentrates from samples of variably mylonitic Brioverian metasedimentary rocks exposed within the south-eastern sector of the St Malo region display internally concordant apparent age spectra which define plateaux of 326–320 Ma. A whole-rock phyllite sample from Brioverian metasedimentary rocks exposed along the eastern boundary of the St Malo region displays an internally discordant argon release pattern which is interpreted to reflect the effects of a partial late Palaeozoic thermal overprint. Muscovite from the Plélan granite, part of the Variscan Plélan-Bobital Granite Complex, yields a 40Ar/39Ar plateau age of c. 307 Ma. The 40Ar/39Ar results indicate that Cadomian rocks of the St Malo region have undergone a widespread and variable Palaeozoic (Carboniferous) rejuvenation of intracrystalline argon systems which apparently did not affect the Mancellian region. This rejuvenation was not accompanied by penetrative regional deformation, and was probably of a static thermal–hydrothermal origin. The heat source for rejuvenation was probably either the result of heating during Variscan extension or advection from Variscan granites which are argued to underlie the St Malo region.  相似文献   

10.
In the Caledonide orogen of northern Sweden, the Seve Nappe Complex is dominated by rift facies sedimentary and mafic rocks derived from the Late Proterozoic Baltoscandian miogeocline and offshore-continent–Iapetus transition. Metamorphic breaks and structural inversions characterize the nappe complex. Within the Sarek Mountains, the Sarektjåkkå Nappe is composed of c. 600-Ma-old dolerites with subordinate screens of sedimentary rocks. These lithological elements preserve parageneses which record contact metamorphism at shallow crustal levels. The Sarektjåkkå Nappe is situated between eclogite-bearing nappes (Mikka and Tsäkkok nappes) which underwent high-P metamorphism at c. 500 Ma during westward subduction of the Baltoscandian margin. 40Ar/39Ar mineral ages of c. 520–500 Ma are recorded by hornblende within variably foliated amphibolite derived from mafic dyke protoliths within the Sarektjåkkå Nappe. Plateau ages of 500 Ma are displayed by muscovite within the basal thrust of the nappe and are consistent with metamorphic evidence which indicates that the nappe escaped crustal depression as a result of detachment at an early stage of subduction. Cooling ages recorded by hornblende from variably retrogressed eclogites in the entire region are in the range of c. 510–490 Ma and suggest that imbrication of the subducting miogeocline was followed by differential exhumation of the various imbricate sheets. Hornblende cooling ages of 470–460 Ma are recorded from massive dyke protoliths within the Sarektjåkkå Nappe. These are similar to ages reported from the Seve Nappe Complex in the central Scandinavian Caledonides. Probably these date imbrication and uplift related to Early Ordovician arrival of outboard terranes (e.g. island-arc sequences represented by structurally lower horizons of the Köli Nappes). Metamorphic contrasts and the distinct grouping of mineral cooling ages suggest that the various Seve structural units are themselves internally imbricated, and were individually tectonically uplifted through argon closure temperatures during assembly of the Seve Nappe Complex. The cooling ages of 520–500 Ma recorded within Seve terranes and along terrane boundaries of the Sarek Mountains provide evidence of significant accretionary activity in the northern Scandinavian Caledonides in the Late Cambrian–Early Ordovician.  相似文献   

11.
Abstract 40Ar/39Ar ages from white mica in rocks of the internal zone of the Brooks Range contractional orogen indicate that the Nanielik antiformal duplex developed at about 120 Ma and was remobilized on its southern boundary at c . 108 Ma. Blueschist facies metamorphism accompanied development of the antiform. The timing of the blueschist facies event and creation of the antiform overlap the period of shallow-seated deformation in the foreland fold and thrust belt and sedimentation in the foreland basin of the Brooks Range. Blueschist facies P-T conditions may therefore characterize the thicker parts of orogenic wedges in some orogenic systems; ancient blueschists need not necessarily be interpreted as indicators of active subduction or continent-continent collision.
Microprobe analysis using quantitative wavelength-dispersive and electron backscattered electron imaging methods was used to characterize the composition of white micas in the dated samples. None of the samples was compositionally homogeneous; many contained 2-3 populations of white mica, including both potassic and sodic varieties. Samples which had undergone (in sequence) amphibolite, albite-epidote amphibolite and blueschist facies metamorphic events retained muscovites relict of the amphibolite facies event. Samples that had undergone only the blueschist facies event also contained multiple populations of mica, some probably from detrital sources.  相似文献   

12.
The Schistes Lustrés (SL) suture zone occupies a key position in the Alpine chain between the high‐pressure (HP) Brianconnais domain and the ultrahigh‐pressure (UHP) Dora Maira massif, and reached subduction depths ranging from c. 40–65 km (Cottian Alps). In order to constrain the timing of HP metamorphism and subsequent exhumation, several phengite generations were differentiated, on the basis of habit, texture, paragenesis and chemistry, as belonging to the first or second exhumation episode, respectively, D2 or D3, or to earlier stages of the tectono‐metamorphic evolution. Ten carefully selected samples showing D2, D3 (D2 + D3), or earlier (mostly peak temperature) phengite population(s) were subjected to laser probe 40Ar/39Ar analysis. The data support the results of the petrostructural study with two distinct age groups (crystallization ages) for D2 and D3 phengite, at 51–45 and 38–35 Ma, respectively. The data also reveal a coherent age cluster, at 62–55 Ma, for peak temperature phengite associated with chloritoid which were preserved in low strain domains. The age of the D3 event in the SL complex appears very similar to ages recently obtained for greenschist facies deformation on the border of most internal crystalline massifs. Exhumation rates of the order of 1–2 mm yr?1 are obtained for the SL complex, which are compatible with velocities documented for accretionary wedge settings. Similarly, cooling velocities are only moderate (c.5 °C Myr?1), which is at variance with recent estimates in the nearby UHP massifs.  相似文献   

13.
The alkalic Scituate Granite was emplaced into crystalline sequences within the New England Esmond–Dedham terrane in the Late Devonian ( c. 370 Ma). Variably recrystallized amphibole (iron-rich, hastingsite–hastingsitic hornblende) from four variably deformed samples of the pluton record south-westerly younging 40Ar/39Ar plateau ages ranging between 276 and 263 Ma. These are interpreted to date diachronous cooling through temperatures appropriate for intracrystalline retention of argon following late Palaeozoic orogenic activity. Iron-rich biotite concentrates from the samples record only slightly younger ages, and therefore suggest relatively rapid post-metamorphic cooling. The 40Ar/39Ar ages indicate that the late Palaeozoic tectonothermal overprint was much more regionally pervasive than was previously considered. The apparent timing of this activity is similar to previous estimates for the chronology of high-grade metamorphism throughout the adjacent Hope Valley terrane and for phases of ductile movement on the intervening Lake Char–Honey Hill fault system.  相似文献   

14.
桑海清  王非  龚俊峰  周晶 《岩石学报》2013,29(8):2759-2774
为了满足Ar-Ar快中子活化法定年的需要,经过十几年的连续测定与检验,一个用于早前寒武纪矿物定年的K-Ar法年龄标准物质——ZMT04白云母已被研制成功。它采自内蒙古自治区卓资县天皮山。40Ar-39Ar定年结果表明,40Ar*在矿物晶格中保存均匀稳定,年龄谱平坦,39Ar析出量为99.1%,40Ar/39Ar坪年龄为1823±15Ma,说明该白云母结晶以来未受热扰动,40K-40Ar*同位素计时体系封闭良好。40Ar/39Ar等时年龄为1824±15Ma,与坪年龄一致,代表了伟晶岩中白云母的结晶时间。(40Ar/36Ar)0初始值为288±16,此值与(40Ar/36Ar)a大气氩丰度比(295.5±0.5)处于同一范围,表明该白云母不含过剩氩。根据国家一级标准物质技术规范(JJG1006-1994)的有关规定,对ZMT04白云母进行了一系列分析检验。均匀性检验结果表明,在0.05显著性水平下,K和40Ar*的F分布值小于F临界值,证明该白云母是均匀的。t检验法和稳定性检验与分析表明,ZMT04白云母完全满足国家一级标准物质技术规范对稳定性的要求。国内8个实验室参加了ZMT04白云母K和40Ar*含量的定值分析,正态性和等精度检验结果显示,全部定值分析数据服从正态分布并具等精度。当置信概率为0.95时,该白云母40Ar*和K含量的相对标准偏差都小于1%。经过严格计算最后获得40Ar*和K含量及年龄的认定值和不确定度分别为:40Ar*=4.449±0.060×10-8mol/g(2σ),K=8.28±0.04%(2σ),K-Ar年龄=1804±21Ma(2σ)。此标准物质纯度达100%,总重量为1080g,缩分为196瓶,每瓶5.51g。可供我国K-Ar和Ar-Ar法年代学实验室至少使用54年。此标准物质于2009年3月4日被国家质量监督检验检疫总局审核批准为国家二级标准物质(见国质检量函[2009]89号文),国家质检总局认定的ZMT04白云母制造计量器具许可证编号为GBW(E)040019。  相似文献   

15.
内蒙古东乌珠穆沁旗奥尤特铜-锌矿床位于西伯利亚板块南缘的查干敖包—奥尤特—朝不楞早古生代构造岩浆带。为了获得该矿床的形成年龄,笔者首次对奥尤特矿床铜-锌矿石中的绢云母进行了40Ar-39Ar同位素年代学研究。所测样品的有效坪年龄值为(286.5±1.8)Ma(2σ),等时线年龄为(287±10)Ma(2σ),MSWD=0.45,40Ar/36Ar的初始值为284±74,等时线年龄与坪年龄在误差范围内完全一致,该结果可能代表绢云母的形成时代。详细的野外地质调查和系统的室内岩(矿)相学研究结果表明,奥尤特绢云母和铜-锌硫化物矿具有密切的成因联系,可以推测奥尤特铜-锌矿床形成于海西晚期,属海西晚期构造—岩浆活动的产物。  相似文献   

16.
New 40Ar/39Ar ages are presented from the giant Sulu ultrahigh-pressure (UHP) terrane and surrounding areas. Combined with U-Pb ages, Sm-Nd ages, Rb-Sr ages, inclusion relationships, and geological relationships, they help define the orogenic events before, during and after the Triassic collision between the Sino–Korean and Yangtze Cratons. In the Qinling microcontinent, tectonism occurred between 2.0 and 1.4 Ga. The UHP metamorphism occurred in the Yangtze Craton between 240 and 222 Ma; its thermal effect on the Qinling microcontinent was limited to partial resetting of K-feldspar 40Ar/39Ar ages. Subsequent unroofing at rates of 5–25 km Myr−1 brought the UHP terrane to crustal levels where it underwent a relatively short amphibolite facies metamorphism. The end of that metamorphism is marked by 40Ar/39Ar ages in the 219–210 Ma range, implying cooling at crustal depths at rates of 50–200 °C Myr−1. Ages in the 210–170 Ma range may reflect protracted cooling or partial resetting by Jurassic or Cretaceous magmatism. Jurassic 166–149 Ma plutonism was followed by cooling at rates of c. 15 °C Myr−1, suggesting relatively deep crustal conditions, whereas Cretaceous 129–118 Ma plutonism was succeeded by cooling at rates of c. 50 C Myr−1, suggesting relatively shallow crustal depths.  相似文献   

17.
The phonolitic Limberg t3 tephra (Kaiserstuhl Volcanic Complex, Germany) was previously dated by the conventional K/Ar method yielding inconsistent results. We have re-dated this tephra layer with three independent methods. Fission Track (FT) external detector analyses on single apatite crystals (16.8 ± 1.3 Ma, 2s) and (U-Th)/He measurements on titanite and apatite (16.5 ± 1.0 Ma, 2s and 16.8 ± 1.0 Ma, 2s, respectively) are in close agreement with laser Ar/Ar dates on incrementally heated single crystals of sanidine (16.3 ± 0.4 Ma, 2s). Due to very rapid cooling, the He, FT and Ar thermochronometers provide one single age representing the eruption event. The different minerals are characterised by favourable properties with respect to their chemical composition, grain size and shape. In particular for the t3 sanidine, homogeneity has been demonstrated by electron microprobe analysis and on a grain-to-grain and grain-internal scale by single crystal incremental laser heating. Based on the agreement between independent methods and the mineral yield of this unit, the Limberg t3 tephra is proposed as multi-method age reference material for single grain laser Ar/Ar, FT and (U-Th)/He dating.  相似文献   

18.
尼雄矿田位于隆格尔-工布江达断隆带,是措勤-申扎铁铜多金属成矿带的重要组成部分.滚纠铁矿位于矿田西北端,矿体主要产于花岗闪长岩和二长花岗岩与二叠系敌布错组的接触带及敌布错组层间破碎带中.矿区主要金属矿物有磁铁矿、穆磁铁矿、赤铁矿、磁赤铁矿及少量的褐铁矿、针铁矿等,夕卡岩矿物有石榴石、透辉石、金云母、蛇纹石、绿帘石、阳起石等,其中金云母与磁铁矿密切伴生,本文对其进行电子探针成分分析和40Ar-39Ar同位素测年.电子探针成分分析表明金云母富镁贫铁,Mg/(Fe+Mg+Mn+Ti)介于0.90~0.94之间;金云母40Ar- 39Ar同位素测年获得总气体年龄(Total age)为112.3 Ma,与成矿相关的花岗闪长岩(113.6±1.6 Ma)和二长花岗岩(112.6±1.6 Ma)年龄在误差范围内一致,指示矿床形成于早白垩世晚期(113Ma).与铁矿化时代不同,矿田内铜矿化主要发生在晚白垩世早期(87 Ma).结合区域地质资料,认为滚纠铁矿的形成与班公湖-怒江洋壳的向南俯冲关系密切,冈底斯陆壳和羌塘陆壳在约113Ma对接碰撞,已俯冲的班公湖-怒江洋壳在俯冲惯性和/或重力拖拽作用下发生板片回转,导致软流圈地幔流体上涌,热的软流圈地幔流体携带的巨大热能引发岩石圈地幔和上覆地壳发生部分熔融,形成以壳源为主的壳幔混源岩浆,在弧后拉张区上侵形成花岗闪长岩和二长花岗岩.同时,遭遇下拉组和敌布错组地层,与之发生接触交代作用并形成磁铁矿床.  相似文献   

19.
Ar/Ar thermochronology on 24 hornblendes, 3 biotites, 2 muscovites and 2 K-feldspars, collected along a 400 km-long NW-SE geotraverse through the Grenville Province in western Québec, is employed to provide time constraints on the intermediate and low temperature stages of cooling of part of the Grenville orogen. In the Grenville Front zone, the c. 1000 Ma time of exhumation previously established from thermobarometric and isotopic studies, is supported by the hornblende age data presented here. From 60 km to 160 km SE of the Front, reworked Archaean migmatites of the parautochthonous Réservoir Dozois terrane (RDT; 1004 Ma-old metamorphic monazites) contain hornblendes with 972– 950 Ma cooling ages. Assuming metamorphic geotherms between 25 and 30 °C km?1, calculated cooling and unroofing rates are about 6 °C Ma?1 and 0.33 km Ma?1 in the P–T range 725 °C–800 MPa and 450 °C–400 MPa. Hornblendes from monocyclic rocks of the Mont-Laurier and Morin terranes (MLT and MT; monazite ages c. 1165 Ma) give ages of about 1040 and 1010 Ma, respectively. Calculation of cooling-unroofing rates from peak metamorphic conditions in this area is hampered by thermal perturbations associated with the still poorly dated Grenville collision which took place approximately between 1060 and 1020 Ma. Cooling ages of c. 900 Ma for muscovite and biotite and 860–810 Ma for K-feldspar, show that cooling rates decreased to around 1.5 °C Ma?1 under retrograde greenschist facies conditions in the MLT. On a time vs. distance diagram, the hornblende data define several distinct age ranges, suggesting that each terrane had a characteristic thermal history. Thus, cooling was diachronous and probably non-homogeneous throughout this segment of the Grenville orogen. The time-lag between the cooling history of the parautochthon (972–950 Ma) and the allochthons (1040–1010 Ma) is compatible with an earlier (pre-1040 Ma) peak of metamorphism in the allochthons. The Réservoir Cabonga allochthon was transported toward the NNW from its probable root zone in the MLT during the 1060–1020 Ma Grenvillian collision as a partially cooled slab. The remobilization of the Archaean parautochthon is attributed to this collision. In the Grenville Front zone, slightly older cooling ages and cooling rates initially faster than in the remaining part of the parautochthon are probably as a result of rapid (tectonic?) exhumation shortly after collision. The minor delay (20–30 Ma) in unroofing of the MT compared to the adjacent MLT is most likely related to post-1040 Ma extensional displacement along the Labelle shear zone. In terranes like those described above where metamorphism is diachronous, determination of cooling rates and the history of exhumation may be meaningless without a firm control on the regional structure. However, identification of contrasting cooling histories contributes to unravelling the independent movement of terranes.  相似文献   

20.
利用特别研制的纯化装置有效地除弃有机杂质气体,松辽盆地下白垩统泉头组四段砂岩储层伊利石40Ar-39Ar激光阶段加热分析获得了逐渐上升的阶梯型年龄谱.低温阶段伊利石的年龄小于地层年龄,大于但可能接近于油气成藏最早的年龄;高温阶段坪年龄明显老于地层年龄,反映了陆源碎屑伊利石的年龄,用于探讨盆地沉积物的物源.松辽盆地北部下...  相似文献   

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