Comparison of SAR techniques for luminescence dating of sediments derived from volcanic tuff

In this investigation we evaluate several proposed optically stimulated luminescence single-aliquot regeneration (OSL SAR) procedures to determine which technique has the greatest potential to yield accurate ages for samples collected from tuff-derived alluvial sediments within the narrow, sharply incised canyon systems of the Pajarito Plateau of northern New Mexico. The SAR data collection methods evaluated are: infrared-stimulated luminescence (IRSL), post-IR blue-OSL, IRSL with TL annealing cycles on polymineral fine-grains, and blue-OSL on quartz fine sand. A single-grain laser luminescence (SGLL) procedure for quartz sand is also evaluated. Age estimates obtained from these methods are compared with radiocarbon, soil PDI (profile development index), and IRSL multi-aliquot additive dose (MAAD) age constraints. Our results indicate that the modal D_e of quartz sand SGLL dose distributions yield ages that are consistent with radiocarbon and PDI age constraints for the tuff derived sediments in this investigation and appears to be the most promising method for studies in this area. Additionally, two fine-grained polymineral methods, IRSL SAR and traditional IRSL MAAD, produced ages that were generally in agreement with the SGLL ages and with available ¹⁴C and PDI age constraints. At the present stage of research, we advocate using quartz sand SGLL in conjunction with IRSL SAR or even IRSL MAAD for polymineral fine-grains to provide the most robust and reliable luminescence age data sets for tuff-derived sediments.     

旧石器遗址强烈化学风化沉积物细粒混合矿物的光释光信号特征及其测年应用

从湖南省北部赤山岛枫树嘴旧石器遗址剖面第2、第3和第4考古层位采集的3个沉积物样品中提取的细粒混合矿物,尝试对其红外释光(IRSL)信号进行研究。实验表明,虽然长石IRSL信号很弱,但仍可以测得信噪比足够高的红外激发后高温红外激发释光(post-IR IRSL)信号。与此同时,样品存在明显的红外激发后蓝光释光(post-IR OSL)信号,并且样品的IRSL与post-IR OSL信号均以快组分为主,这为该地区沉积物利用长石光释光信号定年提供了新的可能。鉴于长石IRSL信号较弱,根据剂量恢复实验结果,本研究采用post-IR IRSL SAR法(50℃红外激发后270℃高温红外激发,pIRIR270℃)进行等效剂量测量,同时也应用post-IR OSL SAR法定年进行比较。实验结果表明,细粒混合矿物的pIRIR270℃等效剂量分别为418.8±13.2 Gy、562.3±18.2 Gy和694.8±17.9 Gy,相对应的post-IR OSL SAR等效剂量结果为345.0±29.4 Gy、409.6±33.7 Gy和424.7±32.2 Gy。假设强烈化学风化未对沉积物的剂量率造成很大影响,基于长石pIRIR270℃信号的释光年龄为89±6 ka、118±8 ka和152±9 ka,比前人所得的石英OSL SAR法年龄老30%~55%(约20~55 ka)。通过对比不同测量条件下获得的等效剂量值来评估长石IRSL信号是否存在晒退问题,没有发现长石post-IR IRSL信号存在晒退不完全的证据。根据本研究post-IR IRSL SAR法测年结果,赤山岛枫树嘴旧石器遗址似阿舍利技术类型的石器出现在倒数第二次冰期(MIS 6)后期至末次间冰期(MIS 5)前期,比湖南道县福岩洞现代人类牙齿化石年龄(80~120 ka)稍老。作为似阿舍利技术石器制造者的赤山岛古人与福岩洞现代人的关系将是我国旧石器时代考古学和古人类学研究的一个重要课题。     

Dust deposition and climate in the Carpathian Basin over an independently dated last glacial–interglacial cycle

Loess in the Carpathian Basin is some of the thickest and most complete in Europe. Located in the Vojvodina region of the southern Carpathian Basin the Crvenka loess-palaeosol section appears to preserve a detailed climate proxy archive of the last glacial–interglacial cycle. Central to the interpretation of the site is a detailed and independent age model. Here, the results of detailed optically stimulated luminescence (OSL) dating and elevated temperature post-IR infrared stimulated luminescence (post-IR IRSL) dating are presented. Quartz OSL ages appear accurate to about 50–60 ka, where 2D₀ values are reached, while elevated temperature post-IR IRSL yields more accurate ages below this. In line with recent results, the latter signal appears to show negligible fading rates. Two age models are developed that combine (a) OSL and post-IR IRSL ages and (b) OSL ages and ‘expected’ ages from tying unit boundaries to the marine record. If the luminescence model is regarded as accurate, differences between this and the OSL/marine age model raise questions over the accuracy of the latter, as well as the processes controlling the zeroing of luminescence dates. The luminescence based age model is then used to derive the first fully independent reconstruction of climate proxies and accumulation rates from Carpathian loess. Such reconstructions can be used to compare to other independent records without assumptions inherent in correlation-based approaches. The findings demonstrate how variable accumulation rate is at the site, and compared to other independently dated Carpathian loess records. Average values vary north–south but are of similar order throughout the basin. Accumulation rate was highest during the later part of the last glacial, but variation on millennial timescales does not always match shifts in grain-size, suggesting diverse and complex influences. Environmental reconstructions using grain-size and magnetic susceptibility show that no one atmospheric system or air mass can explain the changes in the Carpathian Basin and that millennial-scale variability can only intermittently be tied to North Atlantic Heinrich events. Expanded ice sheets during the peak last glacial, combined with other atmospheric teleconnections, may have served to develop a strong anticyclone in the region. It was likely windier during earlier parts of the last glacial, but Atlantic and Mediterranean moisture was probably less abundant than during more humid interglacials.     

Infrared stimulated luminescence dating of an Eemian (MIS 5e) site in Denmark using K‐feldspar

Buylaert, J.‐P., Huot, S., Murray, A.S. & Van den haute, P.: Infrared stimulated luminescence dating of an Eemian (MIS 5e) site in Denmark using K‐feldspar. Boreas, 10.1111/j.1502‐3885.2010.00156.x. ISSN 0300‐9483. Infrared stimulated luminescence (IRSL) dating of K‐feldspars may be an alternative to quartz optically stimulated luminescence (OSL) dating when the quartz OSL signal is too close to saturation or when the quartz luminescence characteristics are unsuitable. In this paper, Eemian (MIS 5e) coastal marine sands exposed in a cliff section on the coast of southern Jutland (Denmark) are used to test the accuracy and precision of IRSL dating using K‐feldspars. This material has been used previously to test quartz OSL dating ( Murray & Funder 2003 ): a small systematic underestimation of <10% compared to the expected age of ～130 ka was reported. In our study, a single‐aliquot regenerative‐dose (SAR) IRSL protocol is used to determine values of equivalent dose (D_e) and the corresponding fading rates (g values). A significant age underestimation (of up to ～35%) is observed; this is attributed to anomalous fading. Using a single site‐average fading rate of 3.66 ± 0.09%/decade to correct the IRSL ages for all samples provides good agreement between the average fading‐corrected K‐feldspar age (119 ± 6 ka) and the independent age control (132–125 ka). This is despite the reservations of Huntley & Lamothe (2001) that their fading correction method is not expected to work on samples older than ～20–50 ka. This fading‐corrected feldspar result is not significantly different from the overall revised quartz age (114 ± 7 ka) also presented here. We conclude that fading‐corrected IRSL ages measured using K‐feldspar may be both precise and accurate over a greater age range than might be otherwise expected.     

Stability of fine‐grained TT‐OSL and post‐IR IRSL signals from a c. 1 Ma sequence of aeolian and lacustrine deposits from the Nihewan Basin (northern China)

We tested the suitability of the fine‐grained quartz (4–11 μm) Optical Stimulated Luminescence (OSL) and thermally‐transferred OSL (TT‐OSL), and the fine‐grained polymineral (4–11 μm) post‐infrared IRSL (post‐IR IRSL or pIRIR) signals for dating samples from aeolian‐lacustrine deposits from the Xiaochangliang archaeological profile in the Nihewan Basin, China; these deposits include material from the Jaramillo subchron (c. 1.0 Ma). In the upper aeolian section, the OSL and pIRIR₂₉₀ ages are consistent with each other, and show that the upper 8.8 m was deposited between c. 0.3 and c. 140 ka. The luminescence ages indicate a major discontinuity in deposition between the aeolian and the older lacustrine deposits. Below this hiatus at 9.4 m (i.e. in the lacustrine sediments) all three signals are found to be in field saturation (no further systematic increase in burial dose with depth) despite the TT‐OSL signal (apparent mean burial dose ~880 Gy) being well below saturation on the laboratory growth curve. This is in contrast to the pIRIR₂₉₀ signal, which saturates in the field at a level consistent with laboratory saturation. This results in a practical upper limit to the measured burial dose of ~900 Gy (2D₀). Thus for the TT‐OSL and pIRIR₂₉₀ signals, the upper limits for dating lacustrine deposits are <260 ka and c. 240 ka, respectively. These results have major implications for the appropriate future application of these signals. The ages of our lacustrine samples cannot be regarded as necessarily accurate ones; nevertheless, these ages provide the first long series absolute chronology for study of local palaeolithic and geomorphic evolution history aside from the magnetostratigraphical results available before this research.     

洛川黄土细颗粒混合矿物红外释光信号 异常衰减的初步研究*

对洛川末次冰期的黄土细颗粒混合矿物红外释光(IRSL)信号异常衰减行为的初步研究结果表明: 1)预加热只能部分消除异常衰减对等效剂量测定的影响,不能完全消除这种影响,IRSL异常衰减过程也许存在着热效应和非热效应两种组分; 2)对16个已知年龄的马兰黄土(15~70ka)样品细颗粒混合矿物天然IRSL信号的ED值与期望ED值的比较初步显示,马兰黄土细颗粒混合矿物IRSL信号异常衰减不断发生,导致混合矿物IRSL的年龄测定值可能被低估达20 ％ 以上。     

Timing of fluvial sedimentation in the Upper Rhine Graben since the Middle Pleistocene: constraints from quartz and feldspar luminescence dating

The Heidelberg Basin (HDB) hosts one of the thickest Quaternary sediment successions in central Europe. To establish a reliable Middle and Upper Pleistocene chronology for a recently drilled core from the depocentre of the Heidelberg Basin, we applied multiple luminescence dating approaches, including quartz optically stimulated luminescence (OSL), two feldspar post‐IR IRSL protocols using second IR stimulation temperatures of 225 °C (pIRIR₂₂₅) and 290 °C (pIRIR₂₉₀), and two fading correction models. Relatively high anomalous fading was observed for both the pIRIR₂₂₅ and pIRIR₂₉₀ signals, with mean fading rates of 2.13±0.27 and 2.08±0.49%/decade, respectively. Poor dose recovery behaviour of the pIRIR₂₉₀ signal suggests that the pIRIR₂₉₀ ages are not reliable. The comparison of two fading correction methods for the K‐feldspar ages indicates that the correction method proposed by Kars et al. (2008) Radiation Measurements 43, 786, yields reliable ages, whereas the dose‐rate correction method proposed by Lamothe et al. (2003) Radiation Measurements 37, 493, does not. A chronology for the HDB is established using the quartz ages and reliable fading corrected feldspar pIRIR₂₂₅ ages. Our chronology shows that the sediments in the upper Mannheim Formation were deposited during Marine Isotope Stage (MIS) 4 (c. 70 ka), constrained by two quartz ages in the upper 20 m of the core. Four fading corrected pIRIR₂₂₅ ages of c. 400 ka show that the upper Ludwigshafen Formation was deposited during MIS 12–11, correlated with the Elsterian‐Holsteinian stage. Two ages of 491±76 and 487±79 ka indicate that the Middle and Upper Ludwigshafen Formation were probably deposited during the Cromerian Complex. This luminescence chronology is consistent with palynological results. It also indicates that the IR‐RF ages reported earlier are probably underestimated due to anomalous fading.     

Age limit and age underestimation using different OSL signals from lacustrine quartz and polymineral fine grains

As part of a systematic palaeohydrological reconstruction of lake level fluctuations during the Last Glacial Maximum, a transect of cores from ancient Lake Xinias in central Greece has already been studied with respect to pollen, sediment and mineral magnetic analyses. The chronology was based on ¹⁴C AMS dating of terrestrial plant macrofossil remains from peat and clayey peat (Palaeogeog. Palaeoclimatol. Palaeoecol. 158 (2000) 65). This site thus provides an opportunity for the comparison of fine grain optically stimulated luminescence (OSL) ages of water–lain sediments with an independent chronology. We present here infrared (IR), post-IR blue and blue OSL characteristics of the fine grain sediments from Lake Xinias and a preliminary comparison with independent ages. The equivalent doses based on the IR results are about 40% of those based on post-IR blue stimulation, which in turn are 10–15% below those based on quartz OSL. We discuss the ages derived from the 3 signals in terms of the independent chronology, and draw conclusions about initial bleaching of the quartz and feldspar components, and the reliability of the post-IR blue signal as a chronometer.     

Testing polymineral post-IR IRSL and quartz SAR-OSL protocols on Middle to Late Pleistocene loess at Batajnica,Serbia

The loess–palaeosol sequence of Batajnica (Vojvodina region, Serbia) is considered as one of the most complete and thickest terrestrial palaeoclimate archives for the Middle and Late Pleistocene. In order to achieve a numerical chronology for this profile, four sets of ages were obtained on 18 individual samples. Equivalent doses were determined using the SAR protocol on fine (4–11 μm) and coarse (63–90 μm) quartz fractions, as well as on polymineral fine grains by using two elevated temperature infrared stimulation methods, pIRIR₂₉₀ and pIRIR₂₂₅. We show that the upper age limit of coarse quartz OSL and polymineral pIRIR₂₉₀ and pIRIR₂₂₅ techniques is restricted to the Last Glacial/Interglacial cycle due to the field saturation of the natural signals. Luminescence ages on coarse quartz, pIRIR₂₂₅ and pIRIR₂₉₀ polymineral fine grains are in general agreement. Fine quartz ages are systematically lower than the coarse quartz and pIRIR ages, the degree of underestimation increasing with age. Comparison between natural and laboratory dose response curves indicate the age range over which each protocol provides reliable ages. For fine and coarse quartz, the natural and laboratory dose response curves overlap up to ~150 and ~250 Gy, respectively, suggesting that the SAR protocol provides reliable ages up to c. 50 ka on fine quartz and c. 100 ka on coarse quartz. Using the pIRIR₂₂₅ and pIRIR₂₉₀ protocols, equivalent doses up to ~400 Gy can be determined, beyond which in the case of the former the natural dose response curve slightly overestimates the laboratory dose response curve. Our results suggest that the choice of the mineral and luminescence technique to be used for dating loess sediments should take into consideration the reported limited reliability.     

The luminescence dating chronology of a deep core from Bosten Lake (NW China) in arid central Asia reveals lake evolution over the last 220 ka

The lacustrine deposits of lakes in arid central Asia (ACA) potentially record palaeoclimatic changes on orbital and suborbital time scales, but such changes are still poorly understood due to the lack of reliable chronologies. Bosten Lake, the largest freshwater inland lake in China, is located in the southern Tianshan Mountains in central ACA. A 51.6‐m‐deep lacustrine succession was retrieved from the lake and 30 samples from the succession were used for luminescence dating to establish a chronology based on multi‐grain quartz OSL and K‐feldspar post‐IR IRSL (pIRIR₂₉₀) dating. Quartz OSL ages were only used for samples from the upper part of the core. The K‐feldspar luminescence characteristics (dose recovery test, anomalous fading test, first IR stimulation temperature plateau test) are satisfactory and from the relationship amongst the quartz OSL, IR₅₀ and pIRIR₂₉₀ doses we infer that the feldspar signals are likely to be well bleached at deposition. Bacon age‐depth modelling was used to derive a chronology spanning the last c. 220 ka. The chronology, lithology and grain‐size proxy record indicate that Bosten Lake formed at least c. 220 ka ago and that lake levels fluctuated frequently thereafter. A stable deep lake occurred at c. 220, 210–180, c. 165, 70–60, 40–30 and 20–5 ka, while shallow levels occurred at c. 215, 180–165, 100–70, 60–40 and 30–20 ka. Bosten Lake levels decreased by at least ~29 m and possibly the lake even dried up between c. 160 and c. 100 ka. We suggest that the water‐level fluctuations in the lakes of ACA may not respond directly to climatic changes and may be affected by a number of complex factors.     

钾长石矿物在全新世样品光释光测年中的应用与校正问题

使用钾长石进行释光测年时,由于长石的释光信号存在异常衰减,会导致沉积事件年龄的低估。对中国北方4个全新世样品分别使用石英和钾长石矿物组分释光测年,通过测量钾长石的衰退系数(g值)对钾长石使用再生剂量法获得的表征年龄进行了校正。发现对于本文所研究的年轻样品钾长石表征年龄与石英年龄相比系统偏小约2％～9％,钾长石校正年龄与石英年龄相比则严重偏大约16％～40％,表明使用g值无法校正年轻样品的钾长石年龄。对于年轻样品,钾长石IRSL信号异常衰减现象对测年结果的影响是可以忽略的。     

Advances and Issues in Luminescence Dating of Loess Deposits in Arid Central Asia

High-resolution loess deposits are widely distributed in Arid Central Asia (ACA) and provide important records associated with dust transportation, paleoenvironmental and paleoclimatic evolution. The chronology is the foundation of the research into loess deposits as an environmental archive. In recent decades, the gradually developed optical dating method has been increasingly matured and become an important approach to establishing the loess-paleosol sequences. Here, we summarized and discussed previous work on loess chronology mainly based on optical dating approach in ACA. The following understandings have been listed: ① In comparison with optical dating method, the suitable material for ¹⁴C dating is uncommon in ACA. However, the dating range of luminescence dating is more extensive, and the dating materials are accessible. Thus, the optical dating is widely applicable in the establishment of loess framework in this area. ② Until now, the quartz Single Aliquot Regeneration (SAR) method can be applied to the establishment of loess-paleosol sequence since last glacial period. But several issues remain unaddressed. For example, the Optically Stimulated Luminescence (OSL) signal sensitivity of quartz grains are low in some areas. Furthermore, the results of OSL dating of different grain sizes within a single sample are inconsistent in some areas. The solution of these problems still requires more methodological research. ③ The post-IR IRSL (pIRIR) and multiple elevated temperature stimulation (MET-pIRIR) protoCols of feldspar have basically overcome the anomalous fading issue in the traditional IRSL dating process. In ACA, the framework since MIS 7 can be established with K-feldspar luminescence dating method. Compared with quartz luminescence characteristics, the K-feldspar luminescence signals are more sensitive and exhibit a high saturation level. In specific applications, it is necessary to establish the age frame according to the luminescence sensitivity, the age of samples or other factors.     

A detailed post‐IR IRSL dating study of the Niuyangzigou loess site in northeastern China

In this study, we report standard quartz SAR OSL and post‐IR infrared (IR) stimulated luminescence (post‐IR IRSL; pIRIR₂₉₀) measurements made on sand‐sized quartz and K‐feldspar extracts from the loess‐palaeosol sequence at Niuyangzigou in northeastern China. The quartz OSL characteristics are satisfactory. Extensive pIRIR_50,290 dose recovery tests were performed by adding doses on top of the natural dose. We found that dose recovery ratios improve significantly when the test dose ranges between ~15 and ~80% of the total dose, and good dose recovery (within ±5% of unity) can be obtained up to ～800 Gy. Otherwise, the dose recovery ratio deviates from unity. The D_e values also depend on the test dose size and so we conclude that the effect of test dose size should be routinely considered in pIRIR dating. First IR stimulation plateau pIRIR₂₉₀ results are compared with multiple elevated temperature ‐pIRIR (MET‐pIRIR) data. It appears that the low temperature MET‐pIRIR data are strongly affected by poor dose recovery, but this is not the case for the pIRIR₂₉₀ results. Natural signal measurements at the highest (first IR) stimulation temperature on a sample expected to be in field saturation suggest that ~10% signal loss occurs in pIRIR signals. Long‐term laboratory bleaching experiments (>80 days) show that a constant (or very difficult to bleach) residual pIRIR₂₉₀ signal is reached after ~300 h, corresponding to a dose of 6.2±0.7 Gy. Quartz OSL and feldspar pIRIR_50,290 ages are in good agreement at least back to c. 70 ka. Beyond this the quartz ages begin to underestimate but the feldspar ages are in agreement with the expected Last Interglacial age palaeosol.     

Luminescence evidence for two Middle Pleistocene interglacial events at Tourville, northwestern France

The infrared stimulated luminescence (IRSL) dating method is applied to alkali feldspar coarse grains from the two distinct Middle Pleistocene interglacial estuarine deposits of Tourville, located along the Seine Valley. The upper deposit (unit D), previously dated at 200 ka by ESR on in situ shells and correlated with a stage 7 high sea-level stand (186–245 ka), yields a measured IRSL age of 176 ± 21 ka. The lower deposit (unit B) assigned to a distinctly older high sea-level event (stage 9: 303–339 ka) yields a measured IRSL age of 273 ± 28 ka. The nearby stage 7 raised beach of Sangatte, in Northwestern France, previously dated by TL on quartz (229 ± 18 ka) yields a measured IRSL age of 186 ± 19 ka. These IRSL age estimates systematically underestimate the expected geological ages. This could be due to the long-term fading or instability of the luminescence signal in alkali feldspars. The correction for long-term fading has been tested on these samples. At Tourville, it yields corrected IRSL ages of 196 ± 23ka and 314 ± 32ka, for the upper and lower units respectively and, at Sangatte, a corrected IRSL age of 206 ± 20 ka. These corrected IRSL age estimates are in better agreement with the expected geological ages. This study demonstrates the potential of the feldspar luminescence dating method to provide chronological information on Middle Pleistocene interglacial estuarine sediments within the North Sea-English Channel Basin.     

Hebei loess section in the Anyemaqen Mountains,northeast Tibetan Plateau: a high‐resolution luminescence chronology

The extensive aeolian deposits of the Tibetan Plateau (TP) represent important environmental archives, recording information about the past interplay between the Asian monsoon and Westerlies and the link between dust accumulation and Quaternary glaciations. In the northeast TP, mantles of sandy loess form a distinct belt lying between 3500 and 4500 m a.s.l. on the east‐facing slopes of the Anyemaqen Mountains. However, there is little chronological information about the loess deposits in this region. This study provides a detailed chronology for loess formation in the region using luminescence dating. A total of 29 samples were collected from an 8‐m‐thick homogeneous loess section at Hebei (HB) in order to date sand‐sized (63–90 μm) quartz and K‐feldspar fractions using optically stimulated luminescence (OSL) and infrared stimulated luminescence (IRSL and pIRIR) signals, respectively. The resulting quartz and feldspar ages are in good agreement over the last 40 ka; beyond this (i.e. D_e >120 Gy), the quartz age is underestimated, and the pIRIR₁₇₀ feldspar ages are considered more reliable. The HB loess section records continuous environmental information from c. 50 to c. 30 ka, i.e. throughout Marine Isotope Stage (MIS) 3. Mass accumulation rates (MARs) varied considerably over this period with increased dust accumulation around c. 38 ka and after c. 32 ka; in between, and at the beginning of MIS 3 (50–40 ka), the dust accumulation rate was ~50% lower. Finally, the HB section also records a MIS 2 hiatus of c. 17 ka duration, probably resulting from deflation. This study implies that loess deposition on the TP is predominantly an interglacial/interstadial phenomenon and the TP may be deflating at the same time as the Chinese Loess Plateau is accumulating, at least during MIS 2.     

OSL signal resetting in young deposits determined with a pulsed photon‐stimulated luminescence (PPSL) unit

Optical Stimulated Luminescence (OSL) is a technique that can be used for dating geological materials deposited within the last half‐million years, including sediments transported by air, water or gravity, as well as rocks heated at high temperatures. Recently, several studies have shown that OSL can also provide information on sediment transport. The pulsed photon‐stimulated luminescence (PPSL) unit (also known as a portable OSL reader) developed by the Scottish Universities Environmental Research Centre is an instrument designed to read luminescence signals from bulk (untreated) sediment samples comprising poly‐mineral and poly‐grain fractions. In this contribution, we evaluate the potential of the PPSL unit to assess the degree of OSL signal resetting in 27 young deposits (<2 ka) transported by different geomorphic agents in volcanic, coastal and fluvial depositional settings located in Mexico. Our results are in agreement with previous findings that used the Risø TL/OSL reader, confirming that sediments transported by debrisflows contain the highest inherited luminesce signals. Infrared stimulation (IRSL) values in volcanic ash, lavas, and sand beach and dune deposits exhibit low scatter. However, with blue stimulation (BLSL) these samples reveal a large degree of scattering, attributed to charge transfer in the case of the coastal deposits and to the low sensitivity of quartz in the case of volcanic material. The luminescence signals of fluvial sediments exhibit a highly scattered distribution in both IRSL and BLSL. We conclude that the use of a PPSL unit is a simple approach to assess the degree of OSL signal resetting in deposits sourced from different geological environments. This research contributes to previous studies that have investigated new applications of the PPSL unit to assist in OSL dating of geological materials.     

甘肃玉门地区第四纪晚期构造阶地的红外释光测年

光释光（ＯＳＬ）测年是近几年从热释光（ＴＬ）测年基础工起来的测定第四纪沉积物年龄的一种新技术，其原理与ＴＬ测年类似。不同的是：ＯＳＬ是单色光束激发品体中储存的电离辐射能使其以光的形式释放出来。当用近红外线束作为激光光源时称之为红外释光测年。与ＴＬ测年相比，ＩＳＬ测年可以不考虑残留的ＯＳＬ信号，而且测量具有简便，迅速且准确等优点。本文用细颗粒红外释放技术对玉门地区的构造阶地进行了年龄测定，初步结果表     

Chronology and the upper dating limit for loess samples from Luochuan section in the Chinese Loess Plateau using quartz OSL SAR protocol

Luminescence dating of loess older than 100 ka has long been a challenge. It has been recently reported that, using optically stimulated luminescence (OSL) of fine-grained quartz (4–11 μm) extracted from loess, the range of luminescence dating could be pushed to 0.6 Ma with OSL ages being in agreement with independent ages [Watanuki, T., Murray, A.S., Tsukamoto, S., 2005. Quartz and polymineral luminescence dating of Japanese loess over the last 0.6 Ma: comparison with an independent chronology. Earth and Planetary Science Letters 240, 774–789]. The aim of this study is to provide a luminescence chronology (20 samples) for the standard Luochuan loess section, and to further examine the upper limit of quartz OSL dating for Chinese loess. The growth curve does not saturate at 700 Gy, and should allow reliable equivalent dose (D_e) determination up to at least 400 Gy. However, when compared with independent chronological control, the D_e that could be treated as reliable is less than 230 Gy (corresponding to 70 ka in age for Chinese loess), and the D_e larger than 230 Gy should be underestimated. Ages for samples from the lower part of palaeosol S1 are severely underestimated, with the maximum age of 95 ka for a sample from the bottom of this palaeosol, much younger than the expected age of 128 ka. The maximum D_e obtained for sample L9/M, collected from loess layer L9 which is below the Matuyama–Brunhes (B/M) boundary whose age is 780 ka, is only 403 Gy which corresponds to an age of 107 ka. The cause of underestimation is not yet clear. The previous results by Watunuki et al. (2005) on the extension of OSL dating of loess to 0.6 Ma is not confirmed. When evaluating the validity of OSL ages in S1, another possibility is to question the already established chronological frame for Luochuan section, which is based on the hypothesis of continuous dust deposition. The assumption of an erosion hiatus between L2 and S1 could make the OSL ages look reasonable. However, if this is the case, then it is difficult to explain why the age of sample L9/M is only 107 ka which could be treated as a saturation age, while the OSL can provide a correct age for loess as old as 94.9 ka for sample LC22 collected from the bottom of S1. Much work is required to clarify these confusions.     

Luminescence dating of lacustrine sediments from Tangra Yumco (southern Tibetan Plateau) using post‐IR IRSL signals from polymineral grains

Radiocarbon dating of bulk organic matter is the most commonly used method for establishing chronologies of lake sediments for palaeoclimate reconstructions on the Tibetan Plateau. However, this method is likely to be problematic because the dated material often suffers from old carbon contamination. Recently, advances in luminescence‐based chronological techniques have provided new options for dating lacustrine sediments. In the current study, we tested for the first time the applicability of a new post‐IR IRSL (pIRIR) measurement protocol for dating fine‐grained polymineral material from a deep‐lake sediment core from the central part of Tangra Yumco, on the southern Tibetan Plateau. Our results show that: (i) radioactive disequilibria in the uranium decay chain were observed in the studied lake sediments, and thus taken into account for dose rate calculation by using a dynamic modelling approach; (ii) the suitability and robustness of the pIRIR protocol measured at 150°C (pIRIR₁₅₀) for our samples are confirmed by a set of luminescence characteristic tests as well as the agreement with an independent age control; (iii) turbidite deposition partly caused an insufficient resetting of luminescence signals and thus apparent overestimation in luminescence dating; (iv) compared with the luminescence‐based age‐depth model, the ¹⁴C ages of bulk organic matter from the studied core generally yielded an age difference of ～2 ka, which is attributed to hardwater reservoir effects in Tangra Yumco. This study highlights the need for multi‐dating approaches of lake sedimentary archives on the Tibetan Plateau.     

A robust feldspar luminescence dating method for Middle and Late Pleistocene sediments

Luminescence dating is used extensively to provide absolute chronologies for Late Pleistocene sediments. Nowadays, most optical dates are based on quartz optically stimulated luminescence (OSL). However, the application of this signal is usually limited to the last ～100 ka because of saturation of the quartz luminescence signal with dose. In contrast, the feldspar infrared stimulated luminescence (IRSL) dose–response curve grows to much higher doses; this has the potential to extend the datable age range by a factor of 4–5 compared with quartz OSL. However, it has been known for several decades that this IRSL signal is unstable, and this instability often gives rise to significant age underestimation. Here we test against independent age control the recently developed feldspar post‐IR IRSL approach to the dating of sediments, which appears to avoid signal instability. A physical model explaining our observations is discussed, and the method is shown to be accurate back to 600 ka. The post‐IR IRSL signal is reduced by exposure to daylight more slowly than that from quartz and low‐temperature IRSL, preventing its general application to young (e.g. Holocene) sediments. Nevertheless, this new approach is widely applicable (feldspar of appropriate luminescence behaviour is even more ubiquitous than quartz). These characteristics make this a method of great importance for the dating of Middle and Late Pleistocene deposits.