Combined dendrochronological and radiocarbon dating of six Russian icons from the 15th–17th centuries

The results of dendrochronological and radiocarbon dating by means of accelerator mass spectrometry (AMS) of six medieval icons, originating from northern European Russia and painted on wooden panels made from Scots pine, dated to the 15th to 17th centuries are presented. The panels of each icon were studied using dendrochronology. Five to six AMS dates were obtained for four icons. Although five icons were dendro-dated successfully, one failed to be reliably cross-dated with the existing master tree-ring chronologies and it was dated by radiocarbon wiggle-matching. Dendrochronological dating and wiggle-matching of radiocarbon dates allowed us to determine the narrow chronological intervals of icon creation.

     

The pre-Holocene marine limit on Hopen, Svalbard

A pre-Holocene marine level is found at 109 m a.s.1. on Hopen. Fragments of Mya truncata and Hiatella arctica occurring on a raised coastal spit at that altitude have been radiocarbon dated to >45,000 BP. The amino acid epimerization of these shells, a clearly mixed sample, correlates with samples from Kongsøya that are of Eemian or Early Weichselian age (alloisoleucine/isoleucine ratios, hydrolysed fraction, between 0.084 and 0.213). No direct evidence, such as striations or roche moutonées, of overriding glacier ice has been found, and no erratics were found above the pre-Holocene marine limit. The existing Holocene shoreline displacement curve, with its upper limit at 60 m a.s.1., is supported by four new radiocarbon dates.     

Animals and humans in the European Russian Arctic towards the end of the last Ice Age and during the mid‐Holocene time

Here, we present and discuss results from geo‐archaeological and palaeo‐zoological investigations at the Palaeolithic site Pymva Shor, in the Russian Arctic. As many as 3324 vertebrate fauna remains were recovered during two excavations. This includes bones of mammals, birds and fish. Radiocarbon dates were obtained from 26 specimens. The results show ages in the range 30–3 cal. ka BP. Hare and reindeer are the best represented amongst the identified mammalian species, whilst ptarmigan and various wader species dominate the avian bones. The Pleistocene assemblage includes herbivorous herd animals such as horse, bison and musk ox. These species are typical of the treeless tundra‐steppe landscape that existed during the Lateglacial. Of particular interest is a cave lion specimen that has been radiocarbon dated to approximately 15.5 cal. ka BP. According to our knowledge, this is one of the latest dated examples of this species in Eurasia. The faunal composition in the Holocene assemblage is strikingly different and includes distinct forest taxa such as beaver and pine marten. The avifauna also supports a forested environment with the presence of black grouse. A few stone artefacts were found within the strata, and have been radiocarbon dated to 16–15 cal. ka BP, suggesting that there were humans in the Pymva Shore area at that time. We identified impact notches and cut marks on some radiocarbon‐dated reindeer and bison bones, showing that humans were present twice during the Younger Dryas period. A fourth occupation phase is identified during the mid‐Holocene (6–5 cal. ka BP). We also investigated river terraces and obtained a series of luminescence dates. These have been used to reconstruct the geological history and the relationship to the find‐bearing strata.     

Radiocarbon dating of quaternary loess deposits,Banks Peninsula,Canterbury, New Zealand

Quaternary loess deposits containing charcoal and in situ organic matter constituents from Banks Peninsula, New Zealand, were subjected to various physical and chemical treatments before radiocarbon assay. A stepwide procedure was used in which each component was radiocarbon dated before and after the treatments were applied. The criterion adopted for judging the effectiveness of a treatment is an increase in the radiocarbon age of loess layer. On this basis the oldest and therefore the most reliable date was obtained from the intra-loess charcoal and its humic acid extract. By comparison, the radiocarbon ages of organic matter constituents of the whole or partitioned loess were much younger, and are considered to represent only average ages for the particular layers concerned. No advantage was gained by dating the carbon-enriched clay-humus fraction as opposed to whole loess samples. There is an apparent conflict between our dates and current interpretation of loess stratigraphy and chronology in the South Island of New Zealand, which requires further investigation. This uncertainty apart, the upper layers of multiple loess deposits are clearly much older than earlier reports indicate, and it follows that the correlation of these deposits with late-glacial events both within and beyond New Zealand is even more tenuous and unreliable than previously thought to be the case.     

Long‐term spruce budworm outbreak dynamics reconstructed from subfossil trees

We reconstructed the long‐term spruce budworm (SBW) (Choristoneura fumiferana Clem.) outbreak dynamics in the boreal forest of Quebec (Canada) using a dendrochronological approach with subfossil trees. Although the majority of the excavated wood belonging to the genus Picea could potentially reveal the past activity of spruce budworms in the tree rings, very few were cross‐dated due to a lack of marker rings. All cross‐dated trees were found within a particular zone of the peat bogs and the floating chronology was radiocarbon dated to ca. 5.1 cal ka BP. The results presented in this study suggest that the dynamics of SBW outbreaks in the studied area fluctuated during the last millennia and that severe outbreaks as observed during the 20th century seldom occurred in that part of the boreal forest since the end of the last glaciation. These results are in agreement with observations from other parts of eastern North America. Copyright © 2011 John Wiley & Sons, Ltd.     

The first dating of strong Holocene earthquakes in Gorny Altai using long-term tree-ring chronologies

We present the first results of application of long-term tree-ring chronologies for dating seismically triggered rockfalls and determining the upper age of Holocene rockfalls in southeastern Altai. Based on the results of seismic dendrochronological analysis, dating of penetrating wood injuries is proposed and tested, and the criterion for the distinguishing of seismically triggered rockfalls among slope processes of climatic nature is formulated. An earlier unknown strong earthquake of 1532 has been recognized; its traces are dated by the radiocarbon method. Based on the new data and calibration of earlier radiocarbon dates, the recurrence period of strong earthquakes in the southeastern Altai is refined.     

Depositional and soil history along the Lower Macleay River,New South Wales

Extensive terrace and flood plain deposits occur along the Lower Macleay River. A sequence of terraces from oldest to youngest was named: Madron, Corangula, Mungay, Mooneba, Belgrave and Macleay deposits (contemporary). Basal sediments in the Mooneba terrace were dated by radiocarbon analysis at 3,280 ± 55 years; basal sediments of the Mungay terrace were dated at 6,425 ± 105 years. The Madron and Corangula terraces are considered very much older than the Mungay. The flood plain consists of two early cycles of aggradation buried under 23m of estuarine sediment, which in turn is overlain by up to 6m of alluvium. The estuarine sediments were dated at 8,530 ± 200 years at elevation —4m relative to mean sea level. The base of the overlying Smithtown alluvium was dated at 3,295 ± 95 years. A general chronology is presented for the Lower Macleay valley, and a sequence of terrace soils is discussed.     

A revised chronology of the lowest occupation layer of Pedra Furada Rock Shelter,Piauı́, Brazil: the Pleistocene peopling of the Americas

The present work revisits the chronology of the archaeologically controversial Pedra Furada Rock Shelter of Southeast Piauı́, Brazil, using an improved radiocarbon laboratory pre-treatment and measurements on charcoal samples. The procedure, known as ABOX-SC (acid–base–wet oxidation followed by stepped combustion), has previously been used to secure radiocarbon dates of >40 ka for the antiquity of human occupation of Australia and South Africa, and now has been applied to charcoal from the previously dated oldest occupation layer of the Pedra Furada site. Previous radiocarbon dating had obtained only lower limits of 40–45 ka BP for the Pedra Furada basal layer. Nine charcoal samples from well-structured hearths were subjected to the ABOX-SC procedure and their radiocarbon content determined by accelerator mass spectrometry. Measurements on five of the samples returned ages of greater than 56 ka BP, from graphites produced from ABOX pre-treated charcoal combusted at 910°C. Two other samples were greater than 50 ka BP. The remaining two samples were essentially completely combusted at 650°C, with no material surviving to make a 910°C CO₂ fraction. Their ages were 41.3 and 47.2 ka BP. Ages obtained from graphites generated from the 650°C combusted fraction are considered minimum ages.     

Chronology of late wisconsinan glaciation in middle North America

We propose a chronology of late Wisconsinan glacial fluctuations in middle North America, from Alberta to Wisconsin, based on radiocarbon dates derived solely from wood. Previous chronologies of the southwestern margin of the North American Continental Ice Sheet have depended to a considerable degree on radiocarbon dates from fine-grained organic sediment. This material is commonly contaminated with older carbon, resulting in chronologic confusion. By using only dates from wood, much of the confusion disappears. However, because of the scarcity of wood dates, only four of the sixteen identified fluctuations are accurately dated: an advance into Iowa about 14,000 to 13,500 BP, an advance into South Dakota and Iowa about 12,300 BP, an advance into the Lake Michigan basin about 11,700 BP, and an advance into the Lake Superior basin about 9900 BP. In addition, the beginning of late Wisconsinan glaciation, before 20,000 BP, is fairly well documented. None of the fluctuations in the western part of the region are accurately dated.     

An insect assemblage of early Flandrian age from Lea Marston, Warwickshire, and its bearing on the contemporary climate and ecology

An extensive insect fauna is described from an organic deposit occurring in a gravel pit at Lea Marston, Warwickshire, England. This organic deposit was lying beneath approximately 2.5 m of alluvial clay and directly above gravels which had provided organic material ¹⁴C dated at 11,700 ± 200 yr BP. The insect fauna was indicative of a temperate oceanic climate similar to that found today in southern England or south Sweden and suggested the presence of deciduous woodland. The six radiocarbon dates, however, agreed in giving the deposit an age of around 9500 yr BP which is earlier than the arrival of the principal broad-leaved trees. The pollen assemblage was consistent with the radiocarbon dates in showing, in addition to herbaceous pollen, only the presence of Betula, Salix, and small amounts of Pinus. As the insect faunas known from midland Britain at the close of the Devensian period, barely 500 yr before, are aretic in aspect and entirely devoid of thermophilous species a very rapid climatic amelioration is postulated which permitted the immigration of the very mobile insect fauna well in advance of the more slowly migrating trees.     

The deglaciation of Norway after 10,000 B.P.

Several distinctive marginal moraines of Preboreal age have been observed in Norway. They are grouped into three major morainal zones that are radiocarbon dated at about 9900±100, 9600±100 and 9300±100 B.P. respectively. The following deglaciation of central Norway was rapid and most likely completed about 8500 B.P. Evidence of glacier fluctuations up to recent time is discussed. The results are based partly on observations by the field parties of the I.G.C.P. project 'Quaternary Glaciations in the Northern Hemisphere'.     

Dating prehistoric bog-fires in northern England to calendar years by long-distance cross-matching of pine chronologies

The ages of prehistoric fires can be approximated by radiocarbon dating of charcoal or associated material, but such dating is often inaccurate and at best imprecise. Pine trunks preserved in British and Irish peats occasionally show firescars, which might be dated through dendrochronology to yield calendar-year dates. However, unlike oak, there is no master pine chronology to provide absolute dates, so dating is dependent on interspecies cross-matching; for sites in the British Isles with no dated oaks, calendar-year dating of prehistoric pines has hitherto proved impossible. We present a first success in dating, accurately and precisely, prehistoric fire events recorded in subfossil bog-pine trunks, using long-distance cross-matching of pine chronologies between White Moss, Cheshire, and the Humberhead Levels, England. Results demonstrate a bog-fire in Cheshire in spring 2800 BC, and again in 2710 BC, between spring and summer. Further successful long-distance cross-matching of pine would permit international climatological comparisons. © 1997 John Wiley & Sons, Ltd.     

Thermoluminescence dating of the eruption at Mt Schank,South Australia

Mount Schank, a young volcano in southeastern South Australia, has been dated by thermoluminescence. The dated material was quartz from a former beach dune overlain by the lava flow. Disequilibrium in the uranium decay series required a detailed analysis of the isotopic concentrations in the sand. The samples dated yielded an average age of 4930 ± 540 years BP which is consistent with palaeomagnetic measurements. Combined thermoluminescence, palaeomagnetic and radiocarbon evidence leave unresolved the relative chronologies of Mt Schank and nearby Mt Gambier.     

Building cultural chronology in Eastern Washington: The influence of geochronology,index fossils,and radiocarbon dating

Until the early 1950s, it was believed that the archaeological record of eastern Washington state did not exceed 4000 years. That belief changed in the middle 1950s after discovery of the Lind Coulee site (45GR97), originally dated to the Holocene on the basis of geochronological data and subsequently dated via radiocarbon to 8700 B.P. Geochronology and geoarchaeology provided temporal control and resulted in archaeological time being measured discontinuously as stratigraphically associated sets of artifacts were stacked one upon the other. Percentage stratigraphy and frequency seriation played no role in the measurement of time or the construction of cultural chronologies. Local cultural chronologies originally constructed on the basis of chronostratigraphic marker horizons were not significantly altered in the 1960s and 1970s because few radiocarbon ages were run and the chronological validity of the ages was questioned. The increased intensity of cultural resource management in the 1980s witnessed a marked increased in the production of radiocarbon ages, but extant cultural chronologies have not been significantly altered in structure or appearance. © 2000 John Wiley & Sons, Inc.     

OSL dating and luminescence characteristics of aeolian deposits and their source material in Dalarna,central Sweden

Aeolian dunes, coversands, glacifluvial deltas and paraglacial mass‐movement deposits in Bonäsheden and Skattungheden in Dalarna, central Sweden were dated by optically stimulated luminescence (OSL) on quartz. The OSL ages confirm that the majority of the dunes started forming directly after deglaciation, as suggested by previous investigators. Dune formation seems to have lasted at least 1500 years, until c. 9 ka. Four younger episodes of sand drift resulting in coversand deposition were dated by OSL and/or radiocarbon to 4100±200 a, 1569–1412 cal. a BP, 970±60 a and 150±10 a. The youngest one is related to changes in land use, while the older ones may be due to regional climatic changes. The dated quartz had excellent luminescence characteristics; the luminescence was bright and dominated by the fast signal component, which made it possible to successfully analyse even untreated material, so‐called range‐finder dating. These characteristics are most likely inherited from one of the source rocks of the Quaternary deposits – the Mesoproterozoic Dala sandstone, which we show to also have very good luminescence properties.     

The racemization rate constant for protein-bound aspartic acid in woodrat middens

The racemization rate constant for aspartic acid has been determined from the d/l isomeric ratio in four strata of radiocarbon dated woodrat midden in Arizona. Two different methods of stereospecifically deaminating l-aspartic acid prior to the assay are compared. It is found that pure l-amino acid oxidase pretreatment of the dl aspartic acid mixture requires one less step than treatment with crude, dialyzed venom (Crotalus viridis) but that the two methods give the same results. Application of the theory of amino acid racemization dating is discussed in the context of the steric properties ofthe protein environment in which the racemization actually occurs.     

Fluctuations of the South Patagonian Ice-field during the last glaciation and the Holocene

Mapping along a transect from the southeastern margin of the South Patagonian Ice-field in Torres del Paine National Park (Chile) to the limits of fresh moraines of the last glacial cycle indentified eight glacier advances. The four younger ones have been dated by dendrochronology, tephrochronology and radiocarbon dating. Although the bases of 10 m deep bogs were sampled, close limiting radiocarbon dates were not obtained because bog formation in this rain-shadow area appears not to have commenced until ca.12000 yr ago. The outermost Little Ice Age moraine formed during the seventeenth century and three inner ones were deposited around ad 1805, 1845 and after 1890. Densely vegetated older moraines contiguous with Little Ice Age deposits are possibly of late Holocene age. Tephra from the eruption of Reclus volcano at ca. 11 880 yr BP was incorporated by a readvance that deposited large multiple moraines 10–16 km from the modern ice-front; the oldest basal peat found inside the moraine has been dated to ca. 9200 yr BP. These bracketing dates indicate that some eastern outlet glaciers of the ice-field advanced at a time when some western tidewater outlet glaciers terminated inside their modern limits. This questions the view of J. H. Mercer and other that Patagonian glaciers did not readvance during the late-glacial interval. A stadial event also occurred when the glaciers were some 18–20 km from their modern positions and is closely dated to ca. 11880 yr BP because Reclus pumice flushed down-glacier forms thick upper beds in outwash deltas deposited in proglacial lakes. The four older moraines pre-date the late-glacial eruption of Reclus but are not dated closely. Comparison of their spatial extent with well-dated moraines in the Chilean Lakes Region suggests that they may mark advances culminating at ca. 14000 yr BP, ca. 20000 yr BP and earlier.     

An outline tephrochronology for the Holocene of the north of Ireland

Geochemically typed thin layers of Icelandic Holocene tephras form a tephrochronology for the north of Ireland. Tephrochronology construction is based on geochemical linkage with dated historic Icelandic eruptions and high-precision multisample radiocarbon dating. Comparison with geochemically typed Holocene layers at sites throughout Scotland and northern England shows that some layers are widespread throughout much of the northern British Isles. Other layers of known historic date have so far been detected only in Ireland.     

Chronologies of sedimentary changes in the south Bohai Sea,China: constraints from luminescence and radiocarbon dating

The alternation of terrestrial and marine deposits is an indicator of past environmental and sea‐level changes. The age of deposition is usually dated by means of radiocarbon. However, radiocarbon dates of molluscan shells from coastal areas may be complicated by various sources of carbon, and problematic for deposits of 40–50 ka or older. Herein, we apply the Optically Stimulated Luminescence (OSL) dating method to date samples from terrestrial and marine/coastal sediments extracted from three cores in the south Bohai Sea, China. Multiple‐ and single‐aliquot regenerative‐dose procedures using OSL signals from fine‐silt (4–11 μm), coarse‐silt (38–63 μm) and fine‐sand (63–90 or 90–125 μm) quartz were employed to determine the equivalent dose (D _e). The results showed that: (i) OSL ages from quartz of different grain sizes and different protocols are consistent with each other; (ii) for Holocene samples, most of the radiocarbon dates agree well with OSL ages; (iii) for pre‐Holocene samples, radiocarbon dates cluster at 40–50 ¹⁴ C ka BP, whereas OSL ages are in stratigraphic order from 11 ka to 176 ka. Because of the self‐consistency of the quartz OSL ages, the stratigraphic agreement in the three cores, and the clustering of the radiocarbon dates, we suggest that the quartz OSL ages are more reliable with respect to dating the samples from the south Bohai Sea. Finally, the four marine strata identified in the south Bohai Sea are likely to have formed during the Holocene, Marine Isotopic Stage (MIS) 3–5, MIS 6 and probably MIS 7, respectively.     

Rockfalls triggered by the ad 1356 Basle Earthquake

In the Basle region of Switzerland we demonstrate that rockfall blocks can be dated accurately using the radiocarbon method. Soil beneath rockfall blocks containing organic macro‐remains was sampled at four cliff sites in the Tabular Jura south‐east of Basle. A lightweight drilling rig drills a 101‐mm‐diameter hole through rockfall blocks up to 6 m in height. A downhole sampler is used to recover soil samples from below the blocks. Eighteen radiocarbon dates on charcoal, wood, needles of conifers and organic macro‐remains from 11 blocks gave dates between 970 and 440 bp . Calibrated ages range between ad 1210 and ad 1450. These results, along with field observations and historical research, suggest that a large number of blocks toppled as rockfalls within a short time interval in the epicentral area of the ad 1356 Basle earthquake.