Factors affecting the durability of selected weak and clay-bearing rocks from Turkey, with particular emphasis on the influence of the number of drying and wetting cycles

Weathering can induce a rapid change of rock material from initial rock-like properties to soil-like properties. The resistance of a rock to short-term weathering is described through a durability parameter called the slake durability index. As durability is an important engineering parameter, particularly for weak and clay-bearing rocks, it was assessed by a number of tests. The main purpose of this study is to assess the influence of the number of drying and wetting cycles and controls of mineralogical composition and strength on durability. For this purpose, 141 samples of different types of weak and clay-bearing rocks were selected from different parts of Turkey, and relationships between the above-mentioned rock characteristics were statistically investigated. The samples were subjected to multiple-cycle slake durability testing, X-ray diffraction (XRD) analysis and uniaxial compression testing. In addition, to assess the influence of mineralogical composition on durability, the mineral contents of the original material and the material passing from the drum of the slake durability apparatus after each cycle were also determined by XRD. The results indicate that the type and amount of clay minerals are the main factors influencing the variations of the slake durability index in all samples. The durability of the clay-bearing rocks studied correlates best with the amount of expandable clay minerals. A strong relationship between the uniaxial compressive strength and the fourth-cycle slake durability index is found only for the marls among the rock types studied. Assessment of gradation results of the spoil pile materials consisting of clay-bearing rocks also reveals that the increase in percentage of fines in old piles is indicative of material degradation, as is evident by multiple-cycle slaking. It is emphasized that two-cycle conventional slake durability testing did not appear to offer an acceptable indication of the durability of weak and clay-bearing rocks when compared with multiple-cyclic wetting and drying. Comments on the performance of the test are made that aim to make the testing process and interpretation of the results more reliable.     

Slake durability and mineralogical properties of some pyroclastic and sedimentary rocks

Slake durability of rocks is an important property of rock-mass and rock-materials in geotechnical practice. The slake durability of rocks is closely related to their mineralogical composition. In this paper, mineralogical examinations and slake durability tests for argillaceous clastic rocks, especially pyroclastic rocks, sandstones and mudstones of Neogene Tertiary age from Japan, were performed in order to assess the slake durability and rock alteration process of these rocks as well as to understand the relationship between mineralogy and durability.The mineral composition and textural features of the rocks were studied by means of optical microscopy (OM), X-ray diffractometry (XRD), electron microprobe analysis (EPMA), and scanning electron microscopy (SEM). In addition, the slake durability test was carried out by using the standard testing method of ISRM [Int. J. Rock Mech. Min. Sci. 16 (1979) 148] in distilled water and in the aqueous solutions with dissolved electrolytes of NaCl and CaCl₂.The pyroclastic rocks and tuffaceous sandstone, rich in di-octahedral and tri-octahedral Fe smectite, respectively, show distinctively different slaking behaviors. The pyroclastic rocks show relatively high slaking (Id₂=55.5% and Id₁₀=10.5%) than the tuffaceous sandstone (Id₂=94.1% and Id₁₀=87.8%, refer to text for Id₂ and Id₁₀). This difference in the slake durability observed in these rocks is due to the microscopic occurrences of smectite present in the interspaces between the particles (pyroclastic rocks) and zeolite cementing the interspaces (tuffaceous sandstone) as alteration minerals. In addition, the durability results of tuffaceous sandstone show that the slake durability decreases as the degree of weathering increases (weathered material Id₂=88.7% and Id₁₀=65.3%). Furthermore, two mudstones of Miocene and Pliocene ages, having different clay mineral compositions (smectite vs. illite+chlorite), show the lowest and the highest slake durability among the tested clastic rocks. Hard mudstone shows the highest (Id₂=98.1% and Id₁₀=95.5%) while the soft mudstone shows the lowest (Id₂=33.9% and Id₆=0.4%.) slake durability. Thus, the slake durability of pyroclastic and sedimentary rocks is greatly affected by their mineral composition and texture, and is closely related to their alteration history. Slake durability is also affected by the kind of dissolved electrolyte and its concentration in the aqueous solution, providing some useful information for geotechnical practice.     

Durability Characterization of Marls from the Region of Dalmatia,Croatia

Durability is one of the most important engineering properties of weak and clay-bearing rocks. Weathering can induce a rapid change in rock material from initial properties to soil-like properties. The sensitivity of a rock type against weatherability is usually described by a durability parameter, such as the slake durability index. However, marl resistance is not detected satisfactorily by the durability indices by using slake durability test as suggested by ISRM for two wetting–drying cycles. The results of this study are obtained from samples of compact or laminated eocene marls from region of Dalmatia, Croatia. The samples were subjected to 4 cycles of slake durability, point load tests, determination of dry density, determination of carbonate content and absorption of water. The scatter of data suggests that strength probably has no influence on the durability of marls. On the other hand a separate group of marl samples have a second-cycle slake durability index higher than approximately 85%, and the durability of these samples is classified as “medium-high” to “high”, although the visual inspection of samples after testing, suggests that they should have “medium” to “low” durability classification. According to obtained results these samples of marl fulfil the criterions for the durability classification: a carbonate content lower than approximately 65%, a dry density lower than 2.4 Mg/m³, and values of water absorption higher than 5%.     

The effect of pH of water and mineralogical properties on the slake durability (degradability) of different rocks from the Lesser Himalaya, India

Slake durability is an important geotechnical parameter and is a measure of degradability of rocks due to the process of mechanical and chemical breakdown. It is closely related to the mineralogical composition and the texture of the rocks. In this paper, mineralogical examination along with slake durability tests under variable pH conditions, both in acidic and alkaline environments, on the limestone, shale and siltsone were evaluated to understand the relationship between mineralogy and the degradability of rocks. The study revealed that rocks rich in calcium carbonate and or magnesium carbonate are adversely affected in the acidic environment, whereas, the rocks rich in quartz, feldspar and muscovite are independent of the pH of the slaking fluid, which in turn, is more influenced by the texture of the constituent minerals. It has also been observed that fine grained rocks are more susceptible to degrade in comparison to the coarse grained rocks.     

Assessment of Durability and Weathering State of Some Igneous and Metamorphic Rocks Using Micropetrographic Index and Rock Durability Indicators: A Case Study

Weathering and durability are the key factors of the rock in the suitability and usefulness of different construction materials, building materials and engineering structures. A single test never predicts the entire factor for suitability of rock stone and aggregate in different uses. Thus, variety of physical, mechanical and chemical tests and indices of rocks are widely used to estimate and evaluate the rocks for the suitability of the required purpose. In all the cases, knowledge of durability and weathering properties are the most important along with the strength of the rock. Micropetrographic index and rock durability indicators (dynamic and static) are the one of the best methods to evaluate the rock for weathering and durability. To estimate these indices, variety of tests are performed such as petrographic examination test, point load index, sulfate soundness test, water absorption test, modified aggregate impact value test and test for specific gravity. Slake durability index and impact strength index tests were also performed for correlation with static and dynamic rock durability indicators due to its application and usefulness in the durability and strength of the rock materials. Micropetrographic index was obtained by petrographic examination test and correlated with all the physical and mechanical properties used for find out the durability indicators. The present study is to express the usefulness of these three indices in the classification of weathering and durability classes and estimation of durability indices by slake durability index, impact strength index and micropetrographic index.     

Artificial neural networks and nonlinear regression techniques to assess the influence of slake durability cycles on the prediction of uniaxial compressive strength and modulus of elasticity for carbonate rocks

Understanding rock material characterizations and solving relevant problems are quite difficult tasks because of their complex behavior, which sometimes cannot be identified without intelligent, numerical, and analytical approaches. Because of that, some prediction techniques, like artificial neural networks (ANN) and nonlinear regression techniques, can be utilized to solve those problems. The purpose of this study is to examine the effects of the cycling integer of slake durability index test on intact rock behavior and estimate some rock properties, such as uniaxial compressive strength (UCS) and modulus of elasticity (E) from known rock index parameters using ANN and various regression techniques. Further, new performance index (PI) and degree of consistency (Cd) are introduced to examine the accuracy of generated models. For these purposes, intact rock dataset is established by performing rock tests including uniaxial compressive strength, modulus of elasticity, Schmidt hammer, effective porosity, dry unit weight, p‐wave velocity, and slake durability index tests on selected carbonate rocks. Afterward, the models are developed using ANN and nonlinear regression techniques. The concluding remark given is that four‐cycle slake durability index (I_d4) provides more accurate results to evaluate material characterization of carbonate rocks, and it is one of the reliable input variables to estimate UCS and E of carbonate rocks; introduced performance indices, both PI and Cd, may be accepted as good indicators to assess the accuracy of the complex models, and further, the ANN models have more prediction capability than the regression techniques to estimate relevant rock properties. Copyright © 2011 John Wiley & Sons, Ltd.     

Slake durability study of shaly rock and its predictions

More than 35% of the earths crust is comprised of clay-bearing rocks, characterized by a wide variation in engineering properties and their resistance to short term weathering by wetting and drying phenomenon. The resistance to short-term weathering can be determined by slake durability index test. There are various methods to determine the slake durability indices of weak rock. The effect of acidity of water (slaking fluid) on slake durability index of shale in the laboratory is investigated. These methods are cumbersome and time consuming but they can provide valuable information on lithology, durability and weather ability of rock. Fuzzy set theory, Fuzzy logic and Artificial Neural Networks (ANN) techniques seem very well suited for typical complex geotechnical problems. In conjunction with statistics and conventional mathematical methods, a hybrid method can be developed that may prove a step forward in modeling geotechnical problems. During this investigation a model was developed and compared with two other models i.e., Neuro-fuzzy systems (combination of fuzzy and artificial neural network systems) and artificial neural network system, for the prediction of slake durability index of shaly rock to evaluate the performance of its prediction capability.     

红层软岩崩解性路用控制方法研究

采用灰色关联度分析法对红层软岩的矿物成分、化学成分、崩解试验等数据进行了分析。分析表明, 水理特性不稳定的粘土矿物始终是影响软岩崩解的主要因素之一, 而不同的化学成分对红层软岩崩解性的影响程度不同。通过以纯水、MgCl2, FeCl3, NaCl, CaCl2盐溶液作为红层软岩岩块浸泡液的崩解试验, 说明纯水浸泡下软岩的崩解性最强, 而所选3种盐溶液对所选红层软岩样品的崩解性均有抑制作用, 其中又以CaCl2抑制作用最强。在此基础上提出公路施工中填筑前以浇水作为加快红层软岩崩解, 填筑压实中以掺入石灰作为抑制软岩崩解路用控制方法。     

Investigation of the effect of aggregate shape and surface roughness on the slake durability index using the fractal dimension approach

Argillaceous rocks cover about one thirds of the earth's surface. The major engineering problems encountered with weak- to medium-strength argillaceous rocks could be slaking, erosion, slope stability, settlement, and reduction in strength. One of the key properties for classifying and determining the behavior of such rocks is the slake durability. The concept of slake durability index (SDI) has been the subject of numerous researches in which a number of factors affecting the numerical value of SDI were investigated. In this regard, this paper approaches the matter by evaluating the effects of overall shape and surface roughness of the testing material on the outcome of slake durability indices.

For the purpose, different types of rocks (marl, clayey limestone, tuff, sandstone, weathered granite) were broken into chunks and were intentionally shaped as angular, subangular, and rounded and tested for slake durability. Before testing the aggregate pieces of each rock type, their surface roughness was determined by using the fractal dimension. Despite the variation of final values of SDI test results (values of I_d), the rounded aggregate groups plot relatively in a narrow range, but a greater scatter was obtained for the angular and subangular aggregate groups. The best results can be obtained when using the well rounded samples having the lowest fractal values. An attempt was made to analytically link the surface roughness with the I_d parameter and an empirical relationship was proposed. A chart for various fractal values of surface roughness to use as a guide for slake durability tests is also proposed. The method proposed herein becomes efficient when well rounded aggregates are not available. In such condition, the approximate fractal value for the surface roughness profile of the testing aggregates could be obtained from the proposed chart and be plugged into the empirical relation to obtain the corrected I_d value. The results presented herein represent the particular rock types used in this study and care should be taken when applying these methods to different type of rocks.     

Relative contribution of various climatic processes in disintegration of clay-bearing rocks

The climatic processes of heating and cooling, wetting and drying, and freezing and thawing affect the disintegration characteristics of clay-bearing rocks (shales, claystones, mudstones, and siltstones) to varying degrees. Although heating and cooling, wetting and drying, and freezing and thawing are known to be the main processes responsible for physical disintegration of rocks under natural conditions, most of the previous investigators have used methods based only on water content variations (e.g., jar slake, slake index, and slake durability index tests) to assess the disintegration of clay-bearing rocks. Such assessments may not be adequate to explain the field behaviour of clay-bearing rocks subjected to a full range of climatic processes. In order to evaluate the combined effects as well as relative contributions of various climatic processes on the disintegration behaviour, samples of selected clay-bearing rocks, consisting of 5–6 particles, each weighing 85–150 g, were subjected to multiple cycles of heating and cooling, wetting and drying, and freezing and thawing. These treatments resulted in fragmentation of samples with fragments ranging from 50 to 2 mm and finer in dimensions. A new approach, referred to as the disintegration ratio, and defined as the area under the grain size distribution curve of the disintegrated material to the total area encompassing all grain size distribution curves of the samples, was used to account for fragmentation into varying sizes. Statistical analyses were performed to investigate the relationship between fragmentation, mineralogical composition, and physical properties.     

泥质膨胀岩崩解物粒径分布与膨胀性关系试验研究

崩解性是膨胀岩最基本的特性之一,但在膨胀岩膨胀性的快速判别指标中少见关于崩解性及崩解物的定量指标。因此,有必要开展膨胀岩崩解物粒径分布特征和崩解性与膨胀性之间关系的研究,以对膨胀岩的快速判别进行补充。以浙江台州黑洞、蛇蟠岛和新疆大阪隧洞泥质岩样品为例,进行了干燥饱和吸水率和干燥饱和崩解试验,并分析了干燥崩解物粒径分布特征、耐崩解性指数及其与基于干燥饱和吸水率的膨胀性判别结果之间的关系。结果表明,膨胀岩膨胀性的强弱与其崩解物的最大含量粒组颗粒粒径、有效粒径和耐崩解性指数呈反相关关系。膨胀岩崩解物粒径分布的差异性对其膨胀性具有一定的指示意义。     

Estimation of Durability Aspects of Al Masjid Al-Haram Marble,Makkah City,Saudi Arabia

The durability is a measure of the rock’s ability to resist degradation during its working life. Rock durability is greatly related to the mineralogical composition of rocks, rock texture (crystal interlocking, crystal shape and size), and the nature of fluids that are in contact with rock. Marbles have been among the most important building materials since ancient times. The main aim of this study is to evaluate the durability of Al Masjid Al-Haram marble and Ordinary white marble “Carrara” (M₁ and M₂) and develop some correlations among the physical and mechanical properties such as P-wave velocity, slake durability index, dry uniaxial compressive strength (UCS_Dry), abrasion resistance, point load index, impact strength index, Brazilian tensile strength, and Shore hardness. After testing and the evaluation of the test results, strong statistical correlations were found between P-wave velocity and other rock properties. Statistical correlations between the UCS_Dry other tests were also carried out. The coefficients of regressions (R²) range from 0.6177 to 0.997. The study shows that the UCS_Dry values of M1 and M2 have positive relationship with P wave velocities. Concluding remark is that the rocks tested in the study have good durability characteristics and can be reliably used for construction projects. On the other hand, the derived empirical equations can be used for the estimation purposes for similar rock types.     

Provenance, Tectonic Setting and Geochemistry of Ahwaz Sandstone Member (Asmari Formation, Oligo-Miocene), Marun Oilfield, Zagros Basin, SW Iran

The Asmari Formation deposited in the Zagros foreland basin during the OligoceneMiocene. Lithologically, the Asmari Formation consists of limestone, dolomitic limestone, dolomite, argillaceous limestone, some anhydrite(Kalhur Member) and sandstones(Ahwaz Member). This study is based on the analysis of core samples from four subsurface sections(wells Mn-68, Mn-281, Mn-292 and Mn-312) in the Marun Oilfield in the Dezful embayment subzone in order to infer their provenance and tectonic setting of the Ahwaz Sandstone Member. Petrographical data reveal that the Ahwaz Sandstone comprises 97.5% quartz, 1.6% feldspar, and 0.9% rock fragments and all samples are classified as quartz arenites. The provenance and tectonic setting of the Ahwaz Sandstone have been assessed using integrated petrographic and geochemical studies. Petrographic analysis reveals that mono- and poly-crystalline quartz grains from metamorphic and igneous rocks of a craton interior setting were the dominant sources. Chemically, major and trace element concentrations in the rocks of the Ahwaz Sandstone indicate deposition in a passive continental margin setting. As indicated by the CIW′ index(chemical index of weathering) of the Ahwaz Sandstone(average value of 82) their source area underwent "intense" recycling but "moderate to high" degree of chemical weathering. The petrography and geochemistry results are consistent with a tropical, humid climate and low-relief highlands.     

An Empirical Correlation of Index Geomechanical Parameters with the Compressional Wave Velocity

The geomechanical strength of rockmass plays a key role in planning and design of mining and civil construction projects. Determination of geomechanical properties in the field as well as laboratory is time consuming, tedious and a costly affair. In this study, density, slake durability index, uniaxial compressive strength (UCS) and P-wave velocity tests were conducted on four igneous, six sedimentary and three metamorphic rock varieties. These properties are crucial and used extensively in geotechnical engineering to understand the stability of the structures. The main aim of this study is to determine the various mechanical properties of 13 different rock types in the laboratory and establish a possible and acceptable correlation with P-wave velocity which can be determined in the field as well as laboratory with ease and accuracy. Empirical equations were developed to calculate the density, slake durability index and UCS from P-wave velocities. Strong correlations among P-wave velocity with the physical properties of different rock were established. The relations mainly follow a linear trend. Student’s ‘t’ test and ‘F’ test were performed to ensure proper analysis and validation of the proposed correlations. These correlations can save time and reduce cost during design and planning process as they represent a reliable engineering tool.     

冷生风化作用对边坡稳定性影响

The experiment shows that considerable influence on density rock properties are subjected by nival weathering conditions. The main parameter defining the rock suitability for solution various engineering and geological problems is its firmness limit on single axis pressing. The firmness properties of sandstone being in absolutely dry condition for Kabakta suite at the beginning of investigation was 64.7 MPa, for Nerungri suite sandstones it was 48. 7 MPa. The investigations showed how much the nival conditions of cryohypergenesis of rock sandstones in Kabakta and Nerungri suites have destructive influence in comparison with aquale and more over aerale conditions. In the aerale conditions sedimentary rock firmness of Kabakta suite decreased to 23.2 MPa, in aquale conditions to 16.5, and in the nivale conditions to 8.9 MPa. In Nerungri suite sandstones are according to 17.7 MPa, 11.1 MPa, and 6 MPa after 300 freezing and thawing cycles. The common sandstone firmness decrease of Kabakta suite was 25 %,of Nerungri suite it was 23.8%. Marlstone samples after 400 FTC decrease to 62% in the nivale conditions and to 33 % in the aerale conditions. After 3～5 years of exploitation marlstone will destruct due to structural and textural inhomogenesis up to gruss, i.e. it will not meet the requirements of durability.Judging by the results of carried out experiment it should be concluded that by cryogenic weathering the sedimentary rocks (sandstones) and rocks with schistose lithogenic texture (marlstone) are subjected to disintegration. The primary rock samples firmness considerably influences on the disintegration rate.     

Comparison of three artificial neural network approaches for estimating of slake durability index

Slake durability index (I _d2) is an important engineering parameter to assess the resistance of clay-bearing and weak rocks to erosion and degradation. Standard test sample preparation for slake durability test is difficult for some rock types and the test is time-consuming. The paper reports an attempt to define I _d2 using other parameters that are simpler to obtain. In this study, three different artificial neural network approaches, namely feed-forward back propagation (FFBP), radial basis function based neural network (RBNN), and generalized regression neural networks (GRNN) were used for estimating I _d2. The determination coefficient (R ²), root mean square error and mean absolute relative error statistics were used as evaluation criteria of the FFBP, RBNN, and GRNN models. The experimental results were compared with these models. The comparison results indicate that the GRNN models are superior to the FFBP and RBNN models in modeling of the slake durability index (I _d2).     

Slaking durability and its effect on the doline formation in the gypsum

Texture and grain size is of great importance in understanding the mechanical properties of rocks. The aim of this study was to investigate textural and slaking durability characteristics, and correlate them with the gypsum types where the dolines occurred, with particular reference to the texture and crystal size. The investigation comprised two stages: field work and laboratory testing. Initially, rock samples were obtained from various representative karstified and non-karstified locations. Thereafter, mineralogical, physical and slaking durability characteristics of the gypsum samples were determined by means of laboratory testing. After the field and laboratory works, the geological, mineralogical and slaking durability characteristics of the study area gypsum were reviewed and discussed from the point of view of doline formation. Results showed that fine grain sized alabastrine gypsum tends to be karstified and leads to doline formation. This is closely related to the crystal size, texture and attributable to the slaking durability of the gypsum. Consequently, the results demonstrate that the texture, especially crystal size, and effective porosity are important parameters controlling the slake durability of the gypsum and doline formation.     

钻井液性能对火山碎屑岩崩解性的影响——以青海阿克楚克塞矿区火山碎屑岩为例

为解决火山碎屑岩在钻进中易剥落、易崩塌的问题,探讨钻井液性能对火山碎屑岩崩解性的影响,以青海阿克楚克塞矿区火山碎屑岩为例,分析了其岩石样品的矿物成分,进行了岩石样品烘干和浸水循环实验,采用多元线性回归分析法分析了原1^#、2^#钻井液的主要参数和耐崩解性指数之间的关系。结果表明,钻井液的动塑比、静切力、失水量和漏斗黏度4项性能指标与火山碎屑岩崩解性的相关性可达83.37%,其中动塑比对火山碎屑岩崩解性的影响尤为显著。通过调整水解聚丙烯酰胺和褐煤树脂质量分数提高了钻井液的动塑比和稳定性,从而获得优选钻井液配方：水+4%膨润土+3% Na₂CO₃+0.1% NaOH+0.15% MV-CMC（中黏钠羧甲基纤维素）+0.5% LV-CMC（低黏钠羧甲基纤维素）+2% SPNH（褐煤树脂）+0.08% PHP（水解聚丙烯酰胺）。现场应用表明,钻进至429.00 m深度时使用优选钻井液孔底沉渣厚度较1^#钻井液降低了89.7%,较2^#钻井液降低了80.3%。     

A new engineering-geological rock durability classification

The construction of the 5.3-m diameter, 82-km long Orange—Fish Tunnel in the Republic of South Africa, in sensibly horizontal beds of mudrocks, siltstones and sandstones of the Karoo Supergroup (Upper Carboniferous to Triassic age), revealed the paramount importance of rock durability. The presence of non-durable rock types was found to be one of the causes of the rock distress problems encountered in some tunnel sections during construction.

Geomechanical tests conducted on representative samples of potentially difficult rock types from the Orange—Fish Tunnel, indicated important limitations of international rock material classifications, such as the Deere—Miller Modulus—Strength and the Deere—Gamble Durability—Plasticity systems. The inadequacy of these classifications in the case of the Karoo sedimentary rocks, underlined the need for a new rock durability classification which could be used for the timely indication of the presence of non-durable rock material sections at tunnel level.

An account is given of the lithology, mineralogy and the postulated weathering mechanics of the Karoo rocks encountered, as well as the application of these parameters to the numerical methods used for the quantitative assessment of rock durability. It is considered that a reliable appraisal of this time-dependent parameter can be provided by the measurement of the strength and free swelling properties of the intact rock material.

A new rock durability classification, styled the Geodurability Classification, is discussed. This empirical system appears to be practical and simple as it depends on the minimum number of index rock properties, which can be measured fairly rapidly in a field laboratory by means of simple test apparatus and semi-skilled labour. It is based on different ranges of ratios of the uniaxial compressive strength, σ_c, and the “Duncan” free swelling coefficient, ε_D, as index parameters. The intact rock material is classified according to a rating system which varies from “excellent” (Class A) to “very poor” (Class F).

The extensive use of the Geodurability Classification indicated such a system to be particularly relevant to compacted and weakly cemented rocks, where the tendency of the rock material to deteriorate with time (and not the presence of rock discontinuities such as joints and bedding planes) dominates the time-dependent behaviour of tunnel rock masses.