Applicability of a quartz OSL standardised growth curve for De determination up to 400 Gy for lacustrine sediments from the Qaidam Basin of the Qinghai-Tibetan Plateau

The standardised growth curve (SGC) for quartz OSL has recently been developed as a practical means to reduce measurement times when determining palaeodoses using quartz of aeolian sediments, especially loess and desert sand from the same section or the same geographical area. In the present study, we test the performance of SGCs for lacustrine sediments of three cores in the Qaidam Basin of the Qinghai-Tibetan Plateau (QTP) in China. A total of nine samples were collected (three samples from each of the three cores), and silt-sized (38–63 μm) quartz was extracted for the experiment. The results demonstrated that: (a) Nine samples display similar dose–response curves up to a regeneration dose of 600 Gy using single aliquot regenerative-dose (SAR) protocol, suggesting the existence of a standardised growth curve for lacustrine sediments in the Qaidam Basin; (b) For samples with D_es of up to ～400 Gy, the D_es determined by the SGC are in agreement with the D_es by the SAR protocol, suggesting that the SGC approach could be used for D_e determination up to a dose of ～400 Gy for lacustrine samples from the Qaidam Basin of the Qinghai-Tibetan Plateau in China; (c) The saturation dose for these samples is more than 600 Gy, and in the growth curve a linear growth part was observed in the high dose range of >200 Gy.     

Decoupled warming and monsoon precipitation in East Asia over the last deglaciation

Our understanding of the continental climate development in East Asia is mainly based on loess–paleosol sequences and summer monsoon precipitation reconstructions based on oxygen isotopes (δ¹⁸O) of stalagmites from several Chinese caves. Based on these records, it is thought that East Asian Summer Monsoon (EASM) precipitation generally follows Northern Hemisphere (NH) summer insolation. However, not much is known about the magnitude and timing of deglacial warming on the East Asian continent. In this study we reconstruct continental air temperatures for central China covering the last 34,000 yr, based on the distribution of fossil branched tetraether membrane lipids of soil bacteria in a loess–paleosol sequence from the Mangshan loess plateau. The results indicate that air temperature varied in phase with NH summer insolation, and that the onset of deglacial warming at ~ 19 kyr BP is parallel in timing with other continental records from e.g. Antarctica, southern Africa and South-America. The air temperature increased from ~ 15 °C at the onset of the warming to a maximum of ~ 27 °C in the early Holocene (~ 12 kyr BP), in agreement with the temperature increase inferred from e.g. pollen and phytolith data, and permafrost limits in central China.Comparison of the tetraether membrane lipid-derived temperature record with loess–paleosol proxy records and stalagmite δ¹⁸O records shows that the strengthening of EASM precipitation lagged that of deglacial warming by ca. 3 kyr. Moreover, intense soil formation in the loess deposits, caused by substantial increases in summer monsoon precipitation, only started around 12 kyr BP (ca. 7 kyr lag). Our results thus show that the intensification of EASM precipitation unambiguously lagged deglacial warming and NH summer insolation, and may contribute to a better understanding of the mechanisms controlling ice age terminations.     

Quartz OSL dating of sand dunes of Late Pleistocene in the Mu Us Desert in northern China

The Mu Us Desert, located in the northwestern fringe of the East Asian monsoon region, is sensitive to climate variability. The desert is characterized by mobile, semi-fixed and fixed sand dunes. Alternating units of dune sands and sandy palaeosols in the Mu Us Desert imply multiple episodes of dune building and stabilization, in response to the ebb and flow of the East Asian monsoon. Desert evolution and climatic change of high-resolution in the Mu Us Desert are still poorly understood due to limited numerical dating results. In the present study, 19 samples collected from five sand dune sections along a northwest–southeast transect in the Mu Us Desert were dated using quartz optically stimulated luminescence (OSL) and single aliquot regenerative-dose (SAR) protocol. Internal checks of the OSL dating indicate that the SAR protocol is appropriate for equivalent dose (D_e) determination for the samples under study. Combined with the lithologic stratigraphy and the luminescence chronology, the sand dune development in the Mu Us Desert during the Late Pleistocene is discussed. Our results indicate that the sand was mobilized approximately at 91 ka, 71 ka, 48–22 ka, 5 ka, 1 ka, and 0.44 ka; the sand was fixed approximately at 65 ka and Holocene Optimum period in the interior Mu Us Desert. The Mu Us Desert formed at least before ～144 ka, and has shown increasing aridity in the Late Pleistocene.     

Optical dating of Chinese loess using sand-sized quartz: Establishing a time frame for Late Pleistocene climate changes in the western part of the Chinese Loess Plateau

The Chinese Loess Plateau (CLP) is of major interest to Quaternary geologists because it represents an important terrestrial archive of palaeoclimatic fluctuations. Previous multiple-aliquot luminescence dating studies of Chinese loess mainly used thermoluminescence (TL) and infrared stimulated luminescence (IRSL) signals of polymineral fine-grains; these are known to be subject to anomalous fading and thus will tend to yield age underestimations. In this paper we investigate whether the blue-light stimulated luminescence (BLSL) signals from 63 to 90 μm quartz grains extracted from three western Chinese loess sites (Zhongjiacai, Le Du and Tuxiangdao) can be used to establish a reliable chronology. The single-aliquot regenerative-dose (SAR) procedure is used for the equivalent dose (D_e) determinations and the suitability of our measurement protocol is confirmed by dose recovery tests. The influence of an IRSL signal on the quartz D_e measurements derived from BLSL has been investigated. From these results we conclude that an IRSL contamination, expressed as an IRSL/BLSL ratio, of up to 10% can be accepted before the values of D_e are significantly affected. All three sites yield stratigraphically consistent and spatially highly reproducible optical ages up to about 50–70 ka. At the Tuxiangdao site a marked hiatus in the record is identified between ∼20 and ∼30 ka; this remained undetected in previous studies and clearly highlights the importance of high-resolution optical dating in Chinese loess research. The optical ages presented in this work provide more evidence for episodic loess deposition and varying loess accumulation rates in the western part of the CLP. Our study seems to confirm the potential of optically stimulated luminescence (OSL) dating using the SAR procedure applied to the very fine sandy quartz fraction in Chinese loess back to ∼40–50 ka (∼120–150 Gy).     

Two extraterrestrial dust horizons found in the Dome Fuji ice core,East Antarctica

Two silicate-rich dust layers were found in the Dome Fuji ice core in East Antarctica, at Marine Isotope Stages 12 and 13. Morphologies, textures, and chemical compositions of constituent particles reveal that they are high-temperature melting products and are of extraterrestrial origin. Because similar layers were found ～ 2000 km east of Dome Fuji, at EPICA (European Project for Ice Coring in Antarctica)-Dome C, particles must have rained down over a wide area 434 and 481 ka. The strewn fields occurred over an area of at least 3 × 10⁶ km². Chemical compositions of constituent phases and oxygen isotopic composition of olivines suggest that the upper dust layer was produced by a high-temperature interaction between silicate-rich melt and water vapor due to an impact explosion or an aerial burst of a chondritic meteoroid on the inland East Antarctic ice sheet. An estimated total mass of the impactor, on the basis of particle flux and distribution area, is at least 3 × 10⁹ kg. A possible parent material of the lower dust layer is a fragment of friable primitive asteroid or comet. A hypervelocity impact of asteroidal/cometary material on the upper atmosphere and an explosion might have produced aggregates of sub-μm to μm-sized spherules. Total mass of the parent material of the lower layer must exceed 1 × 10⁹ kg. The two extraterrestrial horizons, each a few millimeters in thickness, represent regional or global meteoritic events not identified previously in the Southern Hemisphere.     

Optical dating of Romanian loess using fine-grained quartz

Romanian loess -palaeosol sequences are amongst the thickest and most complete available in Europe. These deposits represent an extended continental record of environmental and climatic change during at least five glacial/interglacial cycles. Their chronology, however, is mainly based on relative methods. In this paper, we investigate whether SAR–OSL dating of fine-grained quartz can be used to establish a reliable chronology for Romanian loess.The samples were collected from the loess–palaeosol sequence near Mircea Vod? (Dobrogea, SE Romania). The luminescence characteristics of the fine-grained quartz extracts are investigated to some extent, and indicate that the applied laboratory measurement procedure (SAR) is reliable. An internally consistent set of optical ages is obtained for the loess deposited up to ～70 ka, and evidence is presented for a varying loess accumulation rate during the Last Glacial. Comparison with independent age control (pedostratigraphy and a newly-developed palaeomagnetic time–depth model) indicates that the optical dating procedure underestimates the true burial age from the penultimate glacial period onwards (i.e. for samples below the last interglacial S1 palaeosol). These results indicate that an apparently reliable laboratory measurement procedure not necessarily yields accurate sedimentation ages. We suggest that quartz-based SAR–OSL ages obtained using the high dose linear region of the growth curve are interpreted with caution.     

OSL chronology of Lynch's Crater,the longest terrestrial record in NE-Australia

Lynch's Crater on the Atherton Tablelands in NE-Australia formed about 230,000 years ago during an explosive eruption, creating a maar more than 80 m deep. Since the eruption, the maar has been filled with lake sediments that are topped by peat material. A 64 m long core was recovered and an OSL dating project was undertaken to extend the chronology beyond 16 m depth, which according to ¹⁴C age control represents ～60 ka. The predominantly organic lake sediments contained abundant fine quartz of aeolian origin, and the Single Aliquot Regenerative Method (SAR) provided satisfactory equivalent dose (D_E) estimates. However, the determination of the dose rate proved both critical and difficult. Extremely low radionuclide contents led to cosmic radiation being the dominant dose rate contribution for most samples. The OSL chronology presented in this paper thus relies on modelling the changing cover by sediments and lake water over the burial time.     

High resolution OSL dating back to MIS 5e in the central Sea of Okhotsk

Marine sediments contain important archives of past ocean and climate changes, but at high latitudes the absence of carbonate has prevented the construction of accurate chronological models. We have begun a study to (1) determine the accuracy of luminescence ages in deep-sea marine sediments, e.g. by comparison with marine oxygen isotope stratigraphy where possible, (2) describe changes in sedimentation rate through time, and (3) test whether it is possible to date back to marine isotope stage 5e (MIS 5e). We show here that optical dating of fine grains of quartz from the central Sea of Okhotsk is able to provide an accurate and precise chronology for the reconstruction of the palaeoceanic and palaeoclimatic environment at our site. The upper 6.5 m of the 18.42 m long core MR0604-PC07A is believed, based on its magnetic susceptibility and the oxygen isotope (δ¹⁸O) records to contain the last ～150 ka. Forty OSL samples were taken from this upper part of the core. The single-aliquot regenerative-dose (SAR) procedure is used for equivalent dose (D_e) determination. The luminescence characteristics of fine-grained quartz (4–11 μm) extracted from the core are described. The OSL signal is dominated by the fast component and a dose recovery test shows that we can accurately measure a known dose given in the laboratory prior to any heat treatment. Dose rates were determined using high-resolution gamma spectrometry, and vary between 0.4 and 1.6 Gy/ka. The OSL ages from this section lie between ～140 ka and ～15 ka and are in very good agreement with the δ¹⁸O stratigraphy up to MIS 5e. A clear change in sedimentation rate is identified: between ～139 and 110 ka, the sedimentation rate was ～0.09 m/ka, but then from ～110 to 15 ka, the sedimentation rate decreases to a constant value of ～0.04 m/ka. Our data confirm that OSL dating using widely distributed fine-grain quartz has great potential for dating deep-sea sediments. Because luminescence methods use clastic materials, they do not depend on the presence of biogenic carbonate. As a result it is now likely that we can establish a chronology in regions of the ocean that were previously undatable.     

Optical dating of a hyperconcentrated flow deposit on a Yellow River terrace in Hukou,Shaanxi, China

A sand layer, interpreted as a hyperconcentrated flow deposit, was found interbedded between loess on a Yellow River terrace in Hukou, Shaanxi, China. The site is known as the Longwangchan Palaeolithic site. The deposits from the terrace were dated using optically stimulated luminescence (OSL). Two samples from the sand layer were dated to 30 ± 2 and 33 ± 3 ka using coarse-grained (CG) quartz, and to 82 ± 7 and 94 ± 5 ka using fine-grained (FG) quartz, respectively. The CG quartz OSL ages are believed to be reliable on the basis of the OSL ages of the bracketing loess samples. The overestimation of the FG quartz OSL ages of the sand samples is explained in terms of hyperconcentrated flow processes during sediment transport and deposition. The large difference between the CG and FG quartz OSL ages of the sand samples helps to better understand the formation of the hyperconcentrated flow deposit. The hyperconcentrated flow deposit in this study indicates an extreme river flood occurring at ～30 ka in this area. In addition, the stone artifacts found in the lower loess layer overlying the bedrock of the terrace were dated to ～47 ka.     

Quartz luminescence dating of Anglian Stage (MIS 12) fluvial sediments: Comparison of SAR age estimates to the terrace chronology of the Middle Thames valley,UK

Quartz optically stimulated luminescence (OSL) is increasingly being used to constrain the depositional age of fluvial and glaciofluvial sequences over orbital (Milankovitch) timescales within the British Isles. Few of these previous studies have had any age control; however there is some evidence that OSL ages based on the single aliquot regenerative dose (SAR) protocol may be subject to systematic age underestimation as samples approach saturation. In this study, the age of 12 luminescence samples from a chronologically well-constrained site dating to 450 ka from the Thames terrace sequence, southern Britain, was measured using SAR in order to test the performance of the method close to its upper age limit. The characteristics, dose response and thermal stability of the OSL signal in these samples were assessed by investigating equivalent dose (D_e) as a function of stimulation time and component-resolved pulse annealing. Despite the fact that the samples are dominated by the quartz fast component, these results showed that both the medium and slow components have lower stabilities than the fast component, but with the unstable medium component most affecting the initial part of the OSL signal used in dating. Based on isolating the fast component either through curve fitting or eliminating the medium component using the early background subtraction method, OSL ages up to 450 Gy were found to compare well with the expected age of the site of 450 ± 23 ka. In contrast, a systematic age underestimation of 10% was manifested at lower doses when using the initial part of the OSL signal, contaminated by the medium component. These results suggest that the early background subtraction method should be used when dating in the non-linear part of the growth curve as it provides a better separation of thermally unstable signals and represents a more convenient approach than curve fitting in well-behaved samples.     

Observations of narrow bipolar events in East China

Narrow bipolar events (NBEs) are a distinct class of intra-cloud lightning discharge. In this paper we present observations of 10 negative and 67 positive such events in East China. Positive NBEs occurred at 7–12 km altitude above mean sea level (MSL) with a mean altitude of 9.5 km, and negative NBEs occurred at 14–16 km altitude. Electrical/channel characteristics of these events were derived from NBE pulse waveforms based on the transmission-line model. On average, the peak current moment and the charge moment change of a NBE event is 15 kA km, and 0.12 C km, respectively. The mean time for the propagation of current front along the channel is 2.2 μs. The upper limit on channel length for NBEs in this study is 510–1060 m, the lower limit on discharge current amplitude is 12.5–43.2 kA, and the minimum charge transfer is 0.1–0.3 C.     

Luminescence dating of baked earth and sediments from the Qujialing archaeological site,China

The Qujialing site is a representative Neolithic archaeological site in the middle reaches of the Yangtze River, China. Absence of suitable material for radiocarbon dating in this region makes the timing of the similar sites difficult. Here we applied optically stimulated luminescence (OSL–SAR) and thermoluminescence (TL–SAR) techniques to date the archaeological and natural deposits from the Qujialing site with known age, testing the techniques on samples at archaeological sites in this region. The results showed that the luminescence properties of quartz from sediment and baked earth samples are very similar. The quartz OSL ages obtained for a sediment sample and a baked earth sample from the cultural layer are 5.4 ± 0.3 and 5.1 ± 0.3 ka, respectively. The quartz TL age of the baked earth sample is 5.6 ± 0.5 ka. These dates are consistent with the calibrated radiocarbon ages (4.9 ± 0.1 and 5.1 ± 0.1 ka cal BP (±1σ)) of the two charcoal samples from the cultural layer at a nearby locality, and are also in agreement with the age of Qujialing culture period. The results indicate that the OSL dating techniques can be applied to date similar archaeological sites in the middle reaches of the Yangtze River, China.     

The equivalent dose of different grain size quartz fractions from lakeshore sediments in the arid region of north China

Equivalent dose (D_e) values were measured by using medium aliquots of different grain size quartz fractions of five lakeshore sediments from the arid region of north China. There are two different relationships between D_e values and grain sizes of these five samples. The first relationship is that the D_e values obtained from various grain sizes are in agreement within 1 delta errors. The second relationship is that D_e values are similar to each other for fractions between 125 and 300 μm, while the D_e value of the 63–90 μm fraction is 40～55% smaller than others. For example, the D_e values obtained for sample #3 are 20.15 ± 1.19 Gy, 19.80 ± 0.83 Gy and 20.93 ± 1.06 Gy for fractions of 90–125, 125–150 and 250–300 μm respectively, but are 10.79 ± 0.84 Gy for the 63–90 μm fraction. The second relationship can't be interpreted by previous studies of both dosimetry and heterogeneous bleaching. It is deduced for sample #2, #3 and #6 that fine particles (<90 μm) intruded after the dominant sedimentation. Comparison of OSL ages from different grain size fractions of sample #2 with a radiocarbon age from the same lithologic layer supports that fractions coarser than 125 μm yield more reliable burial ages, while the fraction finer than 90 μm yields underestimated ages for some lakeshore sediments from this arid region.     

Optically stimulated luminescence dating of loess in South-Eastern China using quartz and polymineral fine grains

Loess deposits distributed in southeastern China play an important role for paleoclimate reconstruction of the subtropical regions. These loess-paleosol deposits are mainly spread within the middle and lower reaches of the Yangtze River as well as in the drainage area of the Huai River. The ages of loess paleosol sequences that are distributed along the Huai River are not well constrained. In this study, the standard single-aliquot regenerative dose (SAR) optically stimulated luminescence (OSL) protocol and two elevated temperature post infrared-infrared stimulated luminescence SAR protocols (pIRIR₂₂₅ and pIRIR₂₉₀) were applied on 4–11 μm quartz and polymineral fine grains, respectively, in order to obtain the first numerical luminescence chronology for a loess-paleosol sequence in northern Jiangsu Province. Our results show a good agreement between quartz SAR-OSL and polymineral pIRIR ages up to ~70 ka. These findings confirm that Xiashu loess accumulated during the Last Glaciation. For samples older than this, the ages increasingly deviate with depth. Fine quartz ages beyond 70 ka are interpreted as underestimates, as previous studies reported that quartz ages >70 ka from various sedimentary origins worldwide may underestimate even if they pass rejection criteria and dose recovery tests. On the other hand, the pIRIR ages are most likely overestimating the true depositional ages as indicated by the results of dose recovery tests, where a 30–60% overestimation of the recovered dose is reported for values larger than ~400 Gy. The overestimation of pIRIR protocols was also confirmed by the results obtained when large beta doses were added on top of the natural accrued dose. Moreover, our dating results suggest that L1/S1 transition (corresponding to MIS 5/4 boundary) occurred much higher in the stratigraphic sequence than may have been interpreted from the magnetic susceptibility enhancement. This inconsistency can be assigned to invalidity of magnetic susceptibility as a chronostratigraphical proxy due to ferrimagnetic minerals dissolution or transformation during paedogenesis processes in this humid subtropical region in the southeastern China.     

Luminescence chronology for late Quaternary lake levels of enclosed Huangqihai lake in East Asian monsoon marginal area in northern China

Lake level fluctuations of closed lakes in monsoonal regions are direct indicators of regional moisture variability related to the intensity of monsoon activities. In the current study, quartz OSL dating was applied to construct the chronology of two sedimentary sequences from the east and west shores of Huangqihai Lake in the East Asian monsoon area, and the history of lake level fluctuations during the late Quaternary was established. In the current study, we present field investigation findings of highstands of >87 m above the modern lake in enclosed Huangqihai Lake in northern China, and also use luminescence dating to establish the timing for the highstands. We conclude that: (1) Lake highstands occurred during both MIS 5 (>87 m above the modern lake) and early Holocene (∼9–8 ka, >54 m above the modern lake), (2) No highstands were observed for MIS 3 and MIS 2 during which loess has accumulated indicative of much drier climate; (3) The evolution of lakes in East Asian monsoon marginal area (e.g. Huangqihai Lake) is linked with the monsoon variation.     

Optically stimulated luminescence dating of sediments from the Yellow River terraces in Lanzhou: Tectonic and climatic implications

The stratigraphic chronology of Yellow River terraces was investigated and studied in Lanzhou Basin, western Chinese Loess Plateau. The optically stimulated luminescence (OSL) dating results show that terraces T₁, T₂ and T₃ formed at 8 ka, 20 ka and 70 ka, respectively. Lateral accretion of the riverbed facies gravel sediments occurred during interglacial periods while vertical aggradations of the terrace sediments deposited predominantly under cold and dry glacial period. A thick layer of aeolian loess with a basal age about 35 ka indicates a remarkable drop of air temperature and a dry, cold climate. The temporal correlation between terrace formation and tectonic movement has not yet been established in this research, but the stratigraphic chronology of the terrace sections provides the timing of the terrace formation, the incision rate of the Yellow River, and the slip rate of the fault horizon.     

Optical dating of the upper 22 m of cored sediments from Daihai Lake,northern China

Daihai Lake is one of the largest lakes in the mid-latitude of northern China. Previous environmental change investigations using the sediments from the lake have been mainly focused on the last 13 ka. In 2006, we drilled an 80-m borehole on the southwest coast of the lake. Here we report the results of initial optical dating of the upper 22-m sediments from the core. Most of the samples allow separation of the 4–11 μm fine-grained and 45–63 μm medium-grained quartz, both of which were used for equivalent dose (D_e) determination. Dose recovery test experiments with the single-aliquot regeneration-dose (SAR) protocol indicate that a preheat at 240 °C for 10 s combined with a cut-heat of 240 °C is suitable for these samples. The D_e values show marked discrepancy between the two grain size fractions with the fine-grained quartz yielding up to over 50% higher D_e values than the medium ones for some samples. We consider the OSL ages for the samples from upper ～10 m to be overestimated. The main cause of the overestimation is attributed to the incomplete bleaching of the sediment grains at deposition. The OSL ages for the lower part of the sequence are considered to be reasonable age estimates which provide useful temporal constrains on the deposition of the sediments for the period of 20–40 ka.     

Recuperated optically stimulated luminescence dating of middle-size quartz grains from the Palaeolithic site of Bonneval (Eure-et-Loir,France)

The site of Bonneval (France) exhibits a 6 m thick stratigraphical sequence in which Middle and Lower Palaeolithic artefacts were discovered. The stratigraphy of the site consists of an alternation of loess-like silt layers deposited along glacial stages, and paleosoil horizons corresponding to the vegetal stabilization of the area during interglacials. These layers hence provide past environmental informations and can be used as stratigraphical markers and compared with well dated sequences of Northern France. Eight sediment samples from this Middle and Upper Pleistocene sequence were dated using the recuperated optically stimulated luminescence (Re-OSL) signal of quartz grains. The middle-size fraction (40–63 μm) shows a good reproducibility of the OSL signals which allows the application of a multiple-aliquot additive-dose approach for D_e determination. For all samples, the growth curves are linear up to an accumulated dose of 3000 Gy. The Re-OSL ages range from ～100 to ～450 ka and are in good agreement with the independent chronological information; they establish when handaxe industries have been made during the Middle and Upper Pleistocene in the Paris Basin.     

Re-evaluation of the chronology of the palaeolithic site at Jeongokri,Korea, using OSL and TT-OSL signals from quartz

Seven samples were collected from sediments at the Palaeolithic site of Jeongokri, Korea, known for the first discovery of Acheulian-like handaxes in East Asia. Optically stimulated luminescence (OSL) ages obtained from chemically purified quartz from the upper five samples are in stratigraphic order, but the ages of the lower samples are not. The OSL signal of the oldest samples occurs well above the saturation level of the exponential part of the dose response curve; however, the OSL signal has an additional component that grows linearly at high doses, making it possible to calculate a D_e value and thus an age. However the reliability of calculating D_e using this linear component is not clear. In contrast, the thermally transferred OSL (TT-OSL) signal grows linearly with dose up to at least 1600 Gy, thus permitting its use for dating. The TT-OSL ages are in agreement with those from the OSL for the four uppermost samples, but give older ages for the lower three samples. Ages obtained using TT-OSL are in stratigraphic order and indicate that the oldest artefacts have an age of ～195 ka.     

Validating a Swedish varve chronology using radiocarbon,palaeomagnetic secular variation,lead pollution history and statistical correlation

We use statistical correlation of palaeomagnetic secular variation (PSV) curves from a varved Holocene lake sediment sequence in west central Sweden (Lake Kälksjön) against those of a Fennoscandian master stack (FENNOSTACK) to correct for an apparent error in the varve chronology. Additional correlation between a lead pollution-derived chronology for the last 2000 years corroborates the PSV results. Use of the FENNOSTACK palaeomagnetic master curve reveals no significant difference in duration between large-scale features from ～2500 to ～8000 cal. yrs BP. Statistical correlation, however, implies that 270 years are missing from the younger part (<1000 cal. yrs BP) of the varve chronology, and that there is an overestimation by approximately 230 years in the number of varves counted in the early Holocene (>8000 cal. yrs BP). A similar comparison between the PSV-determined ages and calibrated bulk radiocarbon ages suggests that the sediments of mid-Holocene age contain substantial amounts of old carbon, probably of soil origin, which causes bulk sediment-calibrated mean ¹⁴C ages to be up to 850 years older than the corrected varve chronology, which extends to 9193 ± 186 cal. yrs BP. This study highlights both the use of statistical correlation as a technique for detecting errors between chronologies, and the importance of validating incremental chronologies with more than one independent method.