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1.
Arnold, L. J. & Roberts, R. G. 2011: Paper I – Optically stimulated luminescence (OSL) dating of perennially frozen deposits in north?central Siberia: OSL characteristics of quartz grains and methodological considerations regarding their suitability for dating. Boreas, Vol. 40, pp. 389–416. 10.1111/j.1502‐3885.2011.00209.x. ISSN 0300?9483. Optically stimulated luminescence (OSL) dating of coarse‐grained quartz is increasingly being used as the main chronological tool in late Quaternary palaeoenvironmental reconstructions of Siberia. However, relatively little information has been published on the suitability of OSL dating for the various types of perennially frozen sediments found in this region. Here we provide a systematic examination of the quartz luminescence characteristics of 21 perennially frozen samples from the Taimyr Peninsula and adjacent coastal lowlands of north‐central Siberia, and discuss their implications for the reliability of single‐grain and multi‐grain OSL chronologies in such contexts. The results of this study suggest that the quartz luminescence characteristics of these samples are, in principle, favourable for OSL dating but, in practice, require that a series of validation checks are made of the chosen experimental conditions. If these tests are satisfied, then reliable OSL chronologies should be obtained for sedimentary deposits in this region. Importantly, however, the single‐grain and multi‐grain aliquot equivalent dose (De) distribution characteristics for our samples reveal that there are advantages in targeting certain types of depositional settings for OSL dating studies of Siberian sediments. We also show that samples from the same depositional settings, and even from the same sites, do not necessarily display similar De distribution characteristics. The latter complication favours the use of single‐grain analysis to unravel the bleaching and burial histories of young (mid‐ to late Holocene) sediments in these Arctic environments.  相似文献   

2.
The alternation of terrestrial and marine deposits is an indicator of past environmental and sea‐level changes. The age of deposition is usually dated by means of radiocarbon. However, radiocarbon dates of molluscan shells from coastal areas may be complicated by various sources of carbon, and problematic for deposits of 40–50 ka or older. Herein, we apply the Optically Stimulated Luminescence (OSL) dating method to date samples from terrestrial and marine/coastal sediments extracted from three cores in the south Bohai Sea, China. Multiple‐ and single‐aliquot regenerative‐dose procedures using OSL signals from fine‐silt (4–11 μm), coarse‐silt (38–63 μm) and fine‐sand (63–90 or 90–125 μm) quartz were employed to determine the equivalent dose (D e). The results showed that: (i) OSL ages from quartz of different grain sizes and different protocols are consistent with each other; (ii) for Holocene samples, most of the radiocarbon dates agree well with OSL ages; (iii) for pre‐Holocene samples, radiocarbon dates cluster at 40–50 14 C ka BP, whereas OSL ages are in stratigraphic order from 11 ka to 176 ka. Because of the self‐consistency of the quartz OSL ages, the stratigraphic agreement in the three cores, and the clustering of the radiocarbon dates, we suggest that the quartz OSL ages are more reliable with respect to dating the samples from the south Bohai Sea. Finally, the four marine strata identified in the south Bohai Sea are likely to have formed during the Holocene, Marine Isotopic Stage (MIS) 3–5, MIS 6 and probably MIS 7, respectively.  相似文献   

3.
Acequias (irrigation channels and ditches) were used by Spanish settlers, their descendants, and Native Americans in New Mexico. Several such features were recently excavated in Santa Fe, but material for numeric dating was difficult to find. Therefore, for this high‐energy‐deposition irrigation‐feature setting we applied optically stimulated luminescence (OSL) sediment dating methods to determine the timing of last filling of some of these acequias. We report multigrain single‐aliquot quartz (MGSAQ) OSL dating results and the first single‐grain quartz (SGQ) OSL dating results for irrigation features. One sample yielded an average age of 96 ± 13 yr, consistent with the maximum expected age of 127 yr (before 2007). An OSL age of 175 ± 15 yr for another sample delimits a sedimentation event since the first construction of that feature ca. 300 yr ago. A sample known to be younger than 400–450 yr but predating the mid‐19th century gave an SGQ age of 376 ±31 yr. These results indicate that: (1) Regional quartz in New Mexico is highly favorable to OSL dating; (2) in this setting, SGQ OSL dating is preferred to MGSAQ dating; and (3) for the last 500–600 yr, SGQ OSL dating in such settings is preferred to 14C dating because OSL dating lacks those ambiguities inherent in converting 14C ages to calendar years. © 2009 Wiley Periodicals, Inc.  相似文献   

4.
The burial age of an alluvially deposited cobble pavement at the Tapada do Montinho archaeological site (east‐central Portugal) is investigated using optically stimulated luminescence (OSL) dating. Measurements on the cobbles (quartzite clasts) were carried out on intact slices and large aliquots (~8 mm) of quartz grains (63–300 μm), both recovered from the outer 1.5‐mm surface of the cobbles. The recycling ratio, recuperation and dose‐recovery tests show that the single‐aliquot regenerative‐dose (SAR) protocol is applicable to both rock slices and quartz grains; both have similar luminescence characteristics. The variation in the natural OSL signal with depth below the cobble surface using intact slices from two different cobbles shows that both were bleached to a depth of at least ~2 mm before deposition. A model of the variation of dose with depth fitted to data from one of the cobbles gives a burial age of ~19 ka and also predicts the dose‐depth variation at the time of deposition. Ages based on rock slices suggest that one cobble surface, and the inner parts of two other cobbles experienced a resetting event at ~45 ka, consistent with the age control. However, the surfaces of the other cobbles all record light‐exposure events in the range 26 to 14 ka, suggesting that some of the cobbles were exposed to daylight perhaps more than once in this period. Given the shallow burial depth and unexpectedly young ages of the surrounding and overlying finer‐grained sediment, it is suggested that phases of light exposure following surficial erosion are probably responsible for this underestimate. Nevertheless, it is remarkable that we can identify and quantify four events (two light exposures of different durations and two sequential burial periods) in the dose record contained within a single clast, and this suggests that the luminescence dating of rock surfaces may prove, in the future, to be at least as important as sand/silt sediment dating.  相似文献   

5.
释光技术在水成沉积物测年中的应用进展   总被引:1,自引:0,他引:1  
准确获得水成沉积物的年龄是第四纪年代学重要的前沿问题之一。随着释光技术的发展,水成沉积物释光测年在如下方面有新的进展:具体释光技术的选择、释光测量方法、测年矿物的种类、矿物的粒级和获得等效剂量的统计方法等。线性调整光释光技术能够提取光释光信号中衰退快的组分;单片再生法应用广泛;单颗粒技术在挑选沉积时晒退充分的颗粒方面具有一定的优势;水成沉积物中的石英比长石更易晒退;较多的实验表明水成沉积物中的粗颗粒比细颗粒更易晒退;获得等效剂量的统计模型很多,但尚无一种统计模型适用于所有样品。在此基础上探讨了水成沉积物释光测年在气候、构造运动、冰川进退历史和人类活动主导的土壤侵蚀量变化研究中的意义及今后的研究方向,为全面了解该领域的最新研究进展提供参考。  相似文献   

6.
The thermoluminescence (TL) and optically stimulated luminescence (OSL) sensitivities of quartz grains from deserts and loess–red clay sequences are used to trace eolian provenances in northern China. Our results indicate that the 110°C TL peak and OSL sensitivities of quartz grains show differences among Chinese deserts, which can be subdivided into four groups according to the spatial variations of luminescence sensitivities. Such differences are related mostly to the regional difference in rock types of mountains surrounding or adjacent to the deserts. We also examine the possible provenance changes between the Quaternary loess and the Tertiary eolian red clay, and the results indicate that the luminescence sensitivity of Tertiary red clay is higher than that of Quaternary loess (L1, L15, and L33), implying source materials of the eolian deposits changed relative to those of the Quaternary.  相似文献   

7.
In this study we present optically stimulated luminescence (OSL) dating results obtained at one of the most important open‐air Middle Palaeolithic sites in the Sierra de Atapuerca foothills – Hotel California. We also assess the possibility of obtaining extended‐range OSL chronologies for a nearby Middle Pleistocene fluvial deposit using several novel methods, namely OSL dating of individual quartz ‘supergrains’, multi‐grain aliquot thermally transferred OSL (TT‐OSL) dating and the first application of a single‐grain TT‐OSL dating procedure. Four single‐grain OSL ages constrain the Middle Palaeolithic occupation of Hotel California to between 71±6 and 48±3 ka. The Hotel California single‐grain equivalent dose (De) distributions are highly overdispersed and contain several dose populations, which are probably attributable to post‐depositional sediment mixing, partial bleaching and intrinsic scatter. The reliability of multi‐grain aliquot OSL dating is compromised by the complex underlying De dispersion affecting these samples, as well as by biasing multi‐grain averaging effects. Extended‐range OSL and TT‐OSL chronologies for the nearby Pico River terrace are consistent with each other and with broad independent age control. These experimental approaches yield a weighted average age of 348±16 ka for terrace TA9 of the Arlanzón River sequence. Our results highlight the benefits of comparing ages obtained using several OSL methodologies to improve the robustness of luminescence chronologies. They also demonstrate the potential that single‐grain OSL techniques offer for establishing improved age constraints on the many other Middle Palaeolithic sites found at Atapuerca and elsewhere across north‐central Spain.  相似文献   

8.
Auto-regenerative dating of zircon grains from fired materials has been shown to be a very powerful technique. The high internal dose rate in zircon gives a measurable auto-regenerated TL signal a few months after the natural TL measurement, allowing the determination of age without dosimetry. The technique has been extended to zircon grains from sediments, using optically stimulated luminescence (OSL) techniques to measure the natural signal. The auto-regenerated signal is only a few hundred photons and cannot be measured above background using present OSL techniques, so it is counted using the highly sensitive TL reader developed for fired zircon grains. Preliminary measurements on fired zircons are in good accord with TL dating and the known ages, but precision becomes poor for samples <1 ka in age. Possible improvements using auto-regenerative phototransfer TL dating are discussed.  相似文献   

9.
High-resolution loess deposits are widely distributed in Arid Central Asia (ACA) and provide important records associated with dust transportation, paleoenvironmental and paleoclimatic evolution. The chronology is the foundation of the research into loess deposits as an environmental archive. In recent decades, the gradually developed optical dating method has been increasingly matured and become an important approach to establishing the loess-paleosol sequences. Here, we summarized and discussed previous work on loess chronology mainly based on optical dating approach in ACA. The following understandings have been listed: ① In comparison with optical dating method, the suitable material for 14C dating is uncommon in ACA. However, the dating range of luminescence dating is more extensive, and the dating materials are accessible. Thus, the optical dating is widely applicable in the establishment of loess framework in this area. ② Until now, the quartz Single Aliquot Regeneration (SAR) method can be applied to the establishment of loess-paleosol sequence since last glacial period. But several issues remain unaddressed. For example, the Optically Stimulated Luminescence (OSL) signal sensitivity of quartz grains are low in some areas. Furthermore, the results of OSL dating of different grain sizes within a single sample are inconsistent in some areas. The solution of these problems still requires more methodological research. ③ The post-IR IRSL (pIRIR) and multiple elevated temperature stimulation (MET-pIRIR) protoCols of feldspar have basically overcome the anomalous fading issue in the traditional IRSL dating process. In ACA, the framework since MIS 7 can be established with K-feldspar luminescence dating method. Compared with quartz luminescence characteristics, the K-feldspar luminescence signals are more sensitive and exhibit a high saturation level. In specific applications, it is necessary to establish the age frame according to the luminescence sensitivity, the age of samples or other factors.  相似文献   

10.
Optical stimulated luminescence (OSL) study on sand and fossil soils from Hulun Buir Dunefield in Eastern China is reported in this paper. Aeolian dune sequences responded to the climate change by alternations of aeolian sand and dark sandy soils, which corresponded to arid and humid conditions, respectively. Optical dating using the single aliquot regeneration technique with quartz was applied to the deposits. The results indicate that the soils and underlying aeolian sand correspond to the Holocene optimum (HO) and the last late glacial, respectively. Combined with studies of OSL dating of 13 profiles and grain-size, magnetic susceptibility, total organic carbon, sediment color and scanning electron microscopy measurements for two representative sections, indicate the expansion in the last late glacial sand was 10 times that of today. The dune field was not totally stabilized by vegetation cover until HO (10–5 ka BP).  相似文献   

11.
The Dolní Věstonice loess section in the Czech Republic is well known for its high‐resolution loess–palaeosol sequence of the last interglacial–glacial climatic cycle (Upper Pleistocene). The loess section is situated in a climatic transition zone between oceanic and continental climates and is therefore of great value in reconstructing past regional climate conditions and their interaction with climate systems, in particular that of the North Atlantic. Based on a combination of optically stimulated luminescence (OSL) ages, stratigraphic field observations and magnetic susceptibility measurements, a chrono‐climatic interpretation of the Dolní Věstonice loess section is presented. To establish a reliable Upper Pleistocene chronology, a quartz OSL approach was applied for equivalent dose (De) determination. Monomineralic quartz extracts of three distinct grain sizes, fine (4–11 μm), middle (38–63 μm) and coarse (90–200 μm), were used and compared. Within error limits, the calculated OSL ages are the same for the different grain sizes, and the OSL ages are in stratigraphic order. The established OSL chronology is in agreement with a Weichselian litho‐ and pedostratigraphy. The Dolní Věstonice loess section is characterized by four pedosedimentary subsequences. At the base of the profile, subsequence I is characterized by a distinct Early Glacial soil complex, OSL‐dated to c. 110 to 70 ka, representing one of the most complete records of environmental change in the European loess belt. Subsequence II is allocated to the Lower Pleniglacial and is characterized by laminated sandy loess. Middle Pleniglacial subsequence III is represented by a brown soil complex, and is followed by the uppermost subsequence IV, characterized by a thick body of laminated sandy loess, indicating strong wind activity and a high sedimentation rate of more than ~1 mm a?1 during the Upper Pleniglacial. According to the OSL chronology, as well as to the sedimentological and palaeopedological investigations, it is likely that the sequence at Dolní Věstonice has recorded most of the climatic events expressed in the NGRIP δ18O reference record between 110 and 70 ka.  相似文献   

12.
甘肃玉门地区第四纪晚期构造阶地的红外释光测年   总被引:4,自引:0,他引:4  
光释光(OSL)测年是近几年从热释光(TL)测年基础工起来的测定第四纪沉积物年龄的一种新技术,其原理与TL测年类似。不同的是:OSL是单色光束激发品体中储存的电离辐射能使其以光的形式释放出来。当用近红外线束作为激光光源时称之为红外释光测年。与TL测年相比,ISL测年可以不考虑残留的OSL信号,而且测量具有简便,迅速且准确等优点。本文用细颗粒红外释放技术对玉门地区的构造阶地进行了年龄测定,初步结果表  相似文献   

13.
A detailed study is presented of a 15.3-m-thick Pleistocene coastal terrace located on the Cantabrian coast (northern Spain). Stratigraphic, sedimentological, topographic and micropalaeontological information is combined with a chronology based on luminescence dating to characterize the deposits. The sedimentary succession records: (i) a basal transgressive system, consisting of a wave-cut surface covered by a lower layer of beach gravels and upper beach pebbly sands; and (ii) a thicker upper highstand system (aggrading), comprising medium to very fine aeolian sands interbedded with thin palustrine muds. Luminescence dating involved a detailed sampling strategy (36 samples and two modern analogues) and the use of both quartz optically stimulated luminescence (OSL) and feldspar post-infrared infrared stimulated luminescence single aliquot regeneration protocols; feldspar results were used to confirm the completeness of bleaching of the quartz OSL signal. The quartz OSL luminescence age–depth relationship shows significant dispersion, but nevertheless two rapid phases of deposition can be clearly identified: one at ~130 ka [Marine Oxygen Isotope Stage (MIS) 5] and one at ~100 ka (MIS 5c). The top of the succession is dated to ~70 ka. The MIS 5e marine maximum flooding surface is identified at an elevation of 6.85 m above mean seal level. This elevation provides evidence of a regional sea-level highstand for this sector of the Cantabrian coast.  相似文献   

14.
Optically stimulated luminescence (OSL) dating was applied to proglacial deposits from the Klettgau Valley in northern Switzerland, which is understood to record several phases of glaciation prior to the Last Interglacial. The aim was to provide an independent chronology for the different sedimentary units to understand better the complex depositional history of the region. This time range requires care when assessing the reliability of the luminescence protocols applied. Equivalent doses for fine‐ and coarse‐grain quartz remained below 300 Gy, while dose response curves for both fractions continued to display growth above 500 Gy. Dose recovery tests confirmed the ability of the single aliquot regenerative (SAR) protocol to recover laboratory doses of a similar size to burial doses, and isothermal decay measurements confirmed the stability of the quartz signal. Having passed rigorous testing criteria, quartz OSL ages of up to ~200 ka were considered reliable but significantly underestimated expected ages and prompt a reconsideration of earlier interpretations of the stratigraphy for this site. Rather than representing three separate glaciations, quartz luminescence ages instead suggest that these deposits record up to four independent ice advances during Marine Isotope Stage 6. For both single grain and single aliquot feldspar dating, it was not possible to separate the conflicting influences of anomalous fading and partial bleaching. However, uncorrected feldspar central age model ages were found to be in reasonable agreement with quartz age estimates, and suggest that feldspar ages may still offer useful additional information in this region.  相似文献   

15.
Buylaert, J.‐P., Huot, S., Murray, A.S. & Van den haute, P.: Infrared stimulated luminescence dating of an Eemian (MIS 5e) site in Denmark using K‐feldspar. Boreas, 10.1111/j.1502‐3885.2010.00156.x. ISSN 0300‐9483. Infrared stimulated luminescence (IRSL) dating of K‐feldspars may be an alternative to quartz optically stimulated luminescence (OSL) dating when the quartz OSL signal is too close to saturation or when the quartz luminescence characteristics are unsuitable. In this paper, Eemian (MIS 5e) coastal marine sands exposed in a cliff section on the coast of southern Jutland (Denmark) are used to test the accuracy and precision of IRSL dating using K‐feldspars. This material has been used previously to test quartz OSL dating ( Murray & Funder 2003 ): a small systematic underestimation of <10% compared to the expected age of ~130 ka was reported. In our study, a single‐aliquot regenerative‐dose (SAR) IRSL protocol is used to determine values of equivalent dose (De) and the corresponding fading rates (g values). A significant age underestimation (of up to ~35%) is observed; this is attributed to anomalous fading. Using a single site‐average fading rate of 3.66 ± 0.09%/decade to correct the IRSL ages for all samples provides good agreement between the average fading‐corrected K‐feldspar age (119 ± 6 ka) and the independent age control (132–125 ka). This is despite the reservations of Huntley & Lamothe (2001) that their fading correction method is not expected to work on samples older than ~20–50 ka. This fading‐corrected feldspar result is not significantly different from the overall revised quartz age (114 ± 7 ka) also presented here. We conclude that fading‐corrected IRSL ages measured using K‐feldspar may be both precise and accurate over a greater age range than might be otherwise expected.  相似文献   

16.
Optically stimulated luminescence (OSL) dating is widely applied to sediments in paleoenvironmental sciences. However, there are only limited examples determining the age of archaeological stone structures by OSL using dust deposits. The age of dust deposits associated with ancient buildings may be used to date the onset of settlement (sediment below structures), settlement activity (occupation layer), or the time after a settlement had been abandoned or destroyed (sediment between collapsed roofs and walls). In this study, OSL dating is applied to establish numerical dates for settlement structures situated in the Negev Highlands, Israel. Two archaeological sites are investigated to identify their occupation history, by dating nine samples of aeolian dust trapped within the remains of ancient buildings. The OSL dating technique is applied using coarse grain quartz and a standard single‐aliquot regenerative‐dose (SAR) protocol. It was possible to date the onset of sedimentation in a later phase of the human occupation or shortly after the sites were abandoned, to 3.7 ± 0.3 ka (Intermediate Bronze Age) at the central site and to 2.7 ± 0.2 ka (Iron Age) at the ephemeral site. These results are supported by archaeological evidence gained from pottery finds and the architecture of the ancient buildings.  相似文献   

17.
北美五大湖区的安大略湖北岸Don Valley Brickyard、Scarborough Bluffs、Bowmanville Bluffs剖面共同构成了北美东北部最长也是最厚的陆地第四纪沉积记录, 较完整地记录了晚更新世劳伦泰德冰盖(the Laurentide Ice Sheet)的演化. 晚更新世劳伦泰德冰盖演化的重建有赖于这些经典剖面中重要沉积地层单元的准确年代学控制. 传统的地层年代学主要是依靠少量14C年代, 将主要的混杂堆积单元(diamicton)解释为气候变冷环境下的冰川扩张, 并与指示全球冰量变化的深海氧同位素曲线一一比对建立起来的. 这样建立起来的年代学存在很大的不确定性. 20世纪80-90年代的少量热释光年代也不相吻合, 最近的13个长石红外释光定年则只集中于Bowmanville Bluffs的一个分层, 并未建立整个剖面的地层年代学, 使这些经典沉积剖面的年代学一直没有得到系统的建立. 应用石英光释光SAR-SGC法测试了Bowmanville Bluffs剖面Glaciofluvial Sand单元的2个冰水沉积样品, 年代结果分别为(41.6±3.8) ka、(48.1±4.4) ka, 分析表明这一年代结果偏老, 石英颗粒可能晒褪不完全. 由于大测片无法识别晒褪不完全的颗粒, 因此, 测试更多的剖面序列的光释光年代并尝试采用粗颗粒小测片或单颗粒技术解决样品颗粒晒褪不完全的问题将是必要的.  相似文献   

18.
A study was made of the applicability of three different techniques for equivalent dose (De) determination in the optical dating of quartz: the single‐aliquot regenerative‐dose technique (SAR), the single‐aliquot additive‐dose technique (SAAD) and the multiple‐aliquot additive‐dose technique (MAAD). For this purpose, quartz grains were extracted from a sequence of Upper Pleniglacial to Late‐glacial coversands exposed at the locality of Ossendrecht in the southwestern Netherlands, a site for which both radiocarbon and earlier luminescence dates are available, providing independent age control. Upon testing the different assumptions underlying each of the three OSL techniques investigated, the SAR protocol was found to be the technique of choice. The optical ages obtained with this protocol were in good agreement with the chronostratigraphical position of the sediments investigated and with the available chronostratigraphical information on the same and equivalent deposits. This confirms the suitability of the SAR technique for dating coversands. Furthermore, a small laboratory intercomparison of SAR‐based De determinations yielded results that were in fair overall agreement. Copyright © 2004 John Wiley & Sons, Ltd.  相似文献   

19.
The sensitivity of optically stimulated luminescence (OSL) of quartz grains has been applied to trace the provenances of sediments in various environments. Here, we studied the OSL sensitivity of quartz grains in four sections (Jingyuan, Huanxian, Xifeng and Luochuan) along a west–east transect on the Chinese Loess Plateau (CLP). The quartz OSL sensitivity in the palaeosol units is higher overall than that in the loess units, and it shows an increasing trend from the west CLP to the east CLP. In palaeosol units, it increases by a factor of ~20 along the west–east transect; while in loess units it increases by a smaller degree of 3–5. The change of provenances and the change of distances between the provenances and the loess sections cannot fully account for the large degree of sensitivity variation between the loess and palaeosol units in the central and eastern CLP. We propose that wildfires may have played an important role in enhancing the quartz OSL sensitivity in the palaeosol units in the central and eastern CLP. Quartz OSL sensitivity has the potential to be used as a proxy for palaeowildfires.  相似文献   

20.
龙山文化末期泾河特大洪水事件光释光测年研究   总被引:6,自引:5,他引:6       下载免费PDF全文
通过对泾河流域深入的野外考察,在其中游基岩峡谷内发现了含有龙山文化末期文化层和古洪水滞流沉积单元的全新世黄土土壤剖面。利用光释光的单片测年技术,确定古洪水滞流沉积层覆盖着的黑垆土层的OSL年龄为 4078±382aB.P. 和4111±450aB.P.。结合其中所含龙山文化遗址的考古年代,揭示出泾河流域在4100~4000aB.P.之间出现一个古洪水多发时期。这组古洪水滞流沉积单元包含5个单层,记录了4100~4000aB.P.之间泾河流域曾经发生的5次特大古洪水事件。这个洪水期对应着我国北方在4000aB.P.前后,由全新世大暖期向着全新世晚期干旱期转折过程中的气候剧烈变化。这些史前洪水事件可能对我国龙山文化的衰落和古代华夏文明的诞生具有重大的影响。  相似文献   

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