热处理饱水致密砂岩的水相自吸与返排

致密砂岩气藏在开发过程中由于水相的侵入或滞留会在近井带或水力裂缝面造成水相圈闭损害,严重影响开发效益.储层高温热处理作为一种新型储层改造技术,已应用于解除近井地带水相圈闭损害.选取鄂尔多斯盆地典型致密砂岩岩样,分别采用干岩样、饱和蒸馏水、饱和3%KCl溶液以及饱和地层水的岩心开展了100～600℃的热处理实验;进行了超过阈值温度的高温热处理前后的岩心自吸、返排实验,并对热处理前后岩心的水相圈闭损害程度进行评价.研究表明,饱和蒸馏水和饱和3%KCl溶液的岩样在热处理后的增渗率明显大于干岩样和饱和地层水的岩样,且岩样热致裂的阈值温度明显降低,从干岩样时500℃降低到300℃;高温热处理增加致密砂岩孔隙度与渗透率,不仅使水相自吸量与自吸速率明显提高,而且岩心渗透率恢复率显著提升.致密岩石热致裂阈值温度可以降低,热增渗后不仅解除水相圈闭损害,而且可以预防后期作业储层水相圈闭损害.     

致密砂岩衰减岩石物理图板分析:储层微裂隙预测

致密砂岩储层普遍具有孔隙度低、微裂隙发育的特点,岩石内部常含有强烈的结构非均质性.致密砂岩发育的微裂隙使储层具有良好的连通性,促成高饱和气的天然气成藏.针对川西某探区须家河组高含气饱和度致密砂岩,本文选取致密砂岩岩心样本,进行了不同围压下的超声波实验测量.考虑储层完全饱气情况下的粒间孔隙、微裂隙双重孔隙结构,采用Biot-Rayleigh双重孔隙方程,构建致密砂岩岩石物理模型,进而分析了裂隙含量对纵波频散和衰减的影响.基于地震波衰减,构建了致密砂岩多尺度岩石物理图板.采用谱比法和改进频移法估算致密砂岩样本及储层衰减,对超声和地震频带下的图板进行校正.将校正后的图板应用到研究工区,选取二维测线和三维区块,进行储层孔隙度和裂隙含量的定量预测.对比实际资料进行分析,结果显示,本文预测的孔隙度和裂隙含量与三口测井的孔隙度曲线和实际产气情况基本吻合,基于孔隙-裂隙衰减岩石物理模型有效地预测了优质储层的分布区域.     

基于岩石物理相约束的致密砂岩气储层渗透率解释建模

充分利用岩心、薄片和钻测井等资料,对四川盆地JQ区块须家河组须二段致密砂岩气储层的沉积微相、成岩相和裂缝相特征进行了研究.结果表明,须二段沉积以辫状河三角洲前缘为主,发育水下分流河道、河口坝和分流间湾等微相;根据成岩作用类型、强度、成岩矿物及其对储层物性的影响将储层划分为压实致密、碳酸盐岩胶结、伊蒙混层充填和不稳定组分溶蚀4种成岩相;裂缝相则以局部层段发育的近水平缝为主.通过三者的叠加与复合对储层岩石物理相进行分类命名,划分出了河口坝-不稳定组分溶蚀-近水平缝相等多种岩石物理相.然后按照岩石物理相对储层物性的建设与破坏作用对其进行聚类分析,归纳出了PF1～PF4四大类岩石物理相.通过建立每一类岩石物理相的孔隙度-渗透率关系表明,基于岩石物理相约束而建立的储层渗透率解释模型具有更高的精度.岩石物理相是揭示致密砂岩气储层成因机理并提高其物性参数测井解释精度的有效途径.     

基于岩石物理模型的页岩油储层各向异性研究（英文）

针对沾化凹陷罗家地区泥页岩进行岩石物理建模,在Backus平均理论中引入粘土矿物压实指数,考虑粘土定向排列引起的各向异性,由Chapman多尺度理论考虑裂缝系统引起的各向异性。根据储层物性特征,以水平缝为主控因素开发基于模型的反演算法,计算裂缝密度和各向异性参数。结果表明,反演的水平裂缝密度与岩心实测的水平渗透率有很好的正相关性,说明裂缝密度可作为渗透率的有效指示参数,同时也表明研究层段泥页岩的裂缝密度与粘土和石英等陆源碎屑含量呈负相关,而与碳酸盐岩含量呈正相关。同时,裂缝的存在使得纵波各向异性大于横波各向异性,裂缝密度与纵波各向异性参数呈明显正相关,而粘土含量与横波各向异性具有明显正相关性。这充分证明了岩石物理建模方法与裂缝反演技术的有效性。     

致密砂岩储层抗拉强度评价方法研究

致密砂岩储层抗拉强度直接影响压裂过程中裂缝起裂、水力裂缝扩展以及水力裂缝与天然裂缝的沟通能力.基于巴西劈裂实验圆盘测定了 14组致密砂岩抗拉强度,同时在围压条件下测定了相同取心位置的14块岩心的纵横波波速和密度.基于上述实验结果,并与岩心所处井深测井数据对比分析,建立了基于地球物理测井数据(声波时差测井和密度测井)的致密砂岩抗拉强度的预测模型,模型相关系数大于0.93.由预测模型可知,抗拉强度与岩样密度和纵波波速呈正比(与声波时差呈反比).利用所建立的抗拉强度评价方法在鄂尔多斯盆地M16井致密砂岩储层进行了应用分析.得到了全井段抗拉强度,并基于抗拉强度预测了储层断裂韧性,其评价结果与压裂后产能监测数据相一致.本研究可为压裂设计、可压裂性评价及工程"甜点"选择提供支撑.     

致密砂岩气藏裂隙-孔隙型弹性岩石物理模板研究:以川西坳陷A区为例

相对于常规砂岩,致密砂岩在岩石物理性质、力学性质等方面具有明显差异,并呈现出很强的非均质性.岩石物理模型能将储层参数与地震特性信息联系起来,因此可以作为致密砂岩储层参数与地震特性信息转换的桥梁.常规的岩石物理模型通常只考虑单一因素(例如非均匀性,单一孔隙,单一尺度等),建立的岩石物理模板并不适用于致密砂岩.本文针对高饱和气、微裂隙发育、非均质性强的致密砂岩储层,利用Voigt-Reuss-Hill模型计算混合矿物的弹性模量,采用微分等效介质(DEM)模型描述含裂隙、孔隙岩石的骨架弹性模量,基于Biot-Rayleigh波动方程构建了岩石物理弹性模板,给出了致密砂岩储层弹性参数与物性的关系.基于测井数据和实验数据对岩石物理弹性模板进行校正,并将校正后的岩石物理弹性模板结合叠前地震资料应用于川西地区储层孔隙度与裂隙含量预测.结果显示,反演裂隙含量、孔隙度与储层试气报告、测井孔隙度基本吻合,表明该模板能够较合理地应用于致密砂岩储层孔隙度及裂隙含量解释中.     

受孔隙形态影响的碳酸盐岩孔隙度反演

深层碳酸盐岩往往具有孔隙度低,孔隙形态复杂的特点.传统孔隙度反演方法仅考虑孔隙空间大小对地层岩石物性的影响,未考虑孔隙形态对岩石弹性特征的作用,在反演深层碳酸盐岩孔隙度时往往存在偏差.孔隙形态的影响可以利用含有孔隙纵横比的等效介质模型表示;通过引入DEM模型对声波孔隙度方程进行改进,定量体现孔隙形态的影响.将改进的声波反演与中子反演、密度反演相结合,得到井区受孔隙形态影响的地层孔隙度.首先利用中子、密度和纵波时差反演得到地层孔隙度初值;进而通过DEM公式获得孔隙纵横比初值;最后综合利用中子测井、密度测井和声波测井数据,实现受孔隙纵横比影响的地层孔隙度反演.应用该方法反演了西南某地MX19井深层白云岩储层的孔隙度,通过与岩心孔隙度测量数据进行对比,验证了反演结果的准确性.     

基于沉积过程的数字岩石建模方法研究

本文提出模拟地层沉积及成岩过程的矿物沉积算法,建立数字岩石模型,并通过对比Micro-CT扫描图像和数值模型的局部孔隙度及平均渗流概率函数分布特征,评价建模的准确性.结果表明,由二维扫描提取的粒径信息作为输入参数,模拟矿物沉积过程建模得到的三维数字岩石模型,能够准确重构原始岩心的非均质性及渗流特性,成功应用于泥质砂岩、碳酸盐岩、页岩等存在多矿物或多尺度孔隙的数字岩石建模中.数字岩石物理是正在兴起的重要技术.数字岩石采用超高分辨率先进成像装备,采集和表征微纳尺度岩石结构,在岩石弹性、电性、核磁、渗流特性等数值计算中发挥重要作用.但是,由于三维直接成像在有限视域内难以表征足够的岩石非均质性,提取二维结构统计特征,利用统计或地质过程法重构具有代表性的三维岩石结构成为十分有价值的研究课题,而且,对业界大量存在的岩石薄片及电镜高清二维图像的深度开发应用也具有重要的现实意义.本文发展的新方法,复原沉积过程,较好地解决了孔隙尺度岩石物理定量研究中数值建模与理论计算的技术瓶颈.     

致密砂岩储层CO2驱油特征的核磁共振实验研究

利用核磁共振技术对致密砂岩储层不同渗透率级别基质岩心和裂缝基质岩心不同驱替压力下CO2驱油特征进行了研究,简述核磁共振原理及实验方法。表明:致密砂岩储层特低、超低渗透基质岩心在初始CO2驱替压力下,岩心毛细孔隙和微毛细孔隙区间的油不同程度被采出,随着CO2驱替压力增大,特低、超低渗透基质岩心毛细孔隙区间油的采出程度不断增加且累积采出程度不同。裂缝致密砂岩储层岩心,裂缝和毛细孔隙区间的油在初始CO2驱替压力下,岩心裂缝中的油及毛细孔隙中的部分油被驱替出来,CO2驱替压力提高毛细孔隙、微毛细区间油的采出程度和累积采收程度较小。致密砂岩储层特低、超低渗透基质岩心和裂缝致密砂岩储层岩心,随着CO2驱替压力增大毛细孔隙区间的部分剩余油成正比增加进入到微毛细孔隙区间改变储层剩余油分布。核磁共振技术能够深入研究致密砂岩储层CO2不同驱替压力阶段,岩心裂缝、毛细孔隙区间、微毛细孔隙区间油的采出程度和剩余油分布情况,对于研究致密砂岩储层微观驱油机理具有较重要的价值。      

含流体致密砂岩的纵波频散及衰减:基于双重双重孔隙结构模型描述的特征分析

致密砂岩普遍具有低孔、低渗及微裂缝发育的地质特征,并且呈现出很强的非均匀性.致密砂岩储层与常规砂岩储层比较,具有明显的岩石物理性质、渗流力学性质方面的差异.致密砂岩内部的非均匀性对弹性波频散、衰减有显著影响,其中包括孔隙结构的非均匀性,即岩石内部孔隙参数的不均一性,以及孔隙内部不相混溶流体的非均匀分布;此外,非均匀性的尺度也决定了波出现显著频散与衰减的频段.综合考虑致密砂岩孔隙结构非均匀性及流体斑块状饱和的非均匀性,本文采用双双重孔隙介质结构模拟了致密砂岩的弹性波响应,分析了同时具备两类非均质性岩石中的波传播特征.调查分析了两组分别来自中国鄂尔多斯盆地苏里格气田及四川盆地广安气田的不同类型致密砂岩储层的岩芯超声波实验数据,给出了岩石样本的弹性波速度频散与衰减曲线.结果显示理论模型预测结果与完全饱和、部分饱和岩石的实验数据吻合良好.对两个地区致密砂岩岩芯数据进行对比分析,苏里格致密砂岩样本总体上比广安致密砂岩渗透率高,在各孔隙度范围内,特征模拟显示苏里格样本的裂隙尺寸明显大于广安样本.广安致密砂岩在低孔隙度范围内发育了更多、更小的颗粒裂隙/接触.致密砂岩的速度频散与衰减结果受流体黏度、晶体破裂及流体斑块状饱和的共同影响.此外,孔隙度越大,部分饱和岩石中斑块状饱和机制对总衰减的贡献越低,与之相对,结构非均质性所占的比重则有所增强.     

Controlling of cements and physical property of sandstone by fault as observed in well Xia503 of Huimin sag, Linnan sub-depression

Cement content of carbonate in tight sandstone near section is much higher than that of the normal sandstones far away from the fault of well Xia503,in the Huimin sag in Linnan sub-depression.In order to understand the origin and its impact on fault sealing,analyses of the whole-rock minerals,casting thin sections,cathodoluminescence,isotope and physical properties are conducted on cores from well Xia503.It is found that 13C varies from 0.1‰to 0.6‰with the average value of 0.42‰,18O varies from 13.5‰to 12.3‰with the average of 13.1‰,and C–O isotope plotting points are distributed in the low to moderate temperature area of the hydrothermal dolomite.According to the occupied relationship,cathodoluminescence,and C–O isotope feature,the carbonate cementation could be divided into four stages:calcites,dolomite,ankerite,and ferrocalcite.It is discovered that the carbonate cementation is negatively related to reservoir physical property,with the porosity of 4.8%,permeability of 0.37 mD,and displacement pressure of 1.97 MPa in the tight sandstone,which have increased by almost one order of magnitude compared to the porosity of 14.3%,permeability of 3.73 mD,and displacement pressure of 0.27 MPa in the normal sandstone,which is far away from the fault.Regardless of the lithology of the counterpart wall of the fault,only the displacement pressure difference caused by carbonate cementation between the tight sandstone and the normal sandstone could seal 41 m high oil column.     

含流体砂岩地震波频散实验研究

为了研究孔隙流体对不同渗透率岩石地震波速度的影响,在实验室利用跨频带岩石弹性参数测试系统得到了应变幅值10-6的2~2000Hz频段下的地震波速度和1 MHz频率下的超声波速度,利用差分共振声谱法得到了频率600Hz岩石干燥和完全饱水情况下岩石声学参数.实验表明,在低饱和度下,致密砂岩在地震和超声频段下没有明显的频散;在高饱和度下纵波速度的频散变得明显.从干燥到完全水饱和条件,不同频率测量的致密砂岩的体积模量随岩石孔隙度增高而降低,且体积模量的变化量受岩石微观孔隙结构的影响较大.高孔、高渗砂岩无论在低含水度下还是在高含水饱和度下频散微弱,并且在地震频段下围压对于岩石纵横波速度的影响要大于频率的影响.高孔、高渗砂岩和致密砂岩不同含水饱和度下的频散差异可应用于储层预测,油气检测等方面,同时该研究可以更好地帮助理解岩石的黏弹性行为,促进岩石物理频散理论的发展,提高地震解释的精度.     

Porosity, permeability, and fluid flow in the Yellowstone geothermal system, Wyoming

Cores from two of 13 U.S. Geological Survey research holes at Yellowstone National Park (Y-5 and Y-8) were evaluated to characterize lithology, texture, alteration, and the degree and nature of fracturing and veining. Porosity and matrix permeability measurements and petrographic examination of the cores were used to evaluate the effects of lithology and hydrothermal alteration on porosity and permeability. The intervals studied in these two core holes span the conductive zone and the upper portion of the convective geothermal reservoir. Variations in porosity and matrix permeability observed in the Y-5 and Y-8 cores are primarily controlled by lithology. Y-8 intersects three distinct lithologies: volcaniclastic sandstone, perlitic rhyolitic lava, and non-welded pumiceous ash-flow tuff. The sandstone typically has high permeability and porosity, and the tuff has very high porosity and moderate permeability, while the perlitic lava has very low porosity and is essentially impermeable. Hydrothermal self-sealing appears to have generated localized permeability barriers within the reservoir. Changes in pressure and temperature in Y-8 correspond to a zone of silicification in the volcaniclastic sandstone just above the contact with the perlitic rhyolite; this silicification has significantly reduced porosity and permeability. In rocks with inherently low matrix permeability (such as densely welded ash-flow tuff), fluid flow is controlled by the fracture network. The Y-5 core hole penetrates a thick intracaldera section of the 0.6-Ma Lava Creek ash-flow tuff. In this core, the degree of welding appears to be responsible for most of the variations in porosity, matrix permeability, and the frequency of fractures and veins. Fractures are most abundant within the more densely welded sections of the tuff. However, the most prominent zones of fracturing and mineralization are associated with hydrothermal breccias within densely welded portions of the tuff. These breccia zones represent transient conduits of high fluid flow that formed by the explosive release of overpressure in the underlying geothermal reservoir and that were subsequently sealed by supersaturated geothermal fluids. In addition to this fracture sealing, hydrothermal alteration at Yellowstone appears generally to reduce matrix permeability and focus flow along fractures, where multiple pulses of fluid flow and self-sealing have occurred.     

Experimental of the influence of mineral composition and normal stress on the frictional slip of shale

Natural fractures are widely distributed in shale reservoirs. During the hydraulic fracturing process, frictional slip occurring on natural fractures can increase the reservoir permeability and is of great significance to improve the efficiency of reservoir stimulation. Shale contains a large amount of clay and organic matter, and its frictional behavior is different from that of other previously studied lithologies. In this paper, the frictional behavior of shale is analyzed, and the results show that the frictional behavior is controlled by the content of clay and organic matter. As the content of clay and organic matter increases, the micro support type transforms from the particle support mode by hard quartz mineral to matrix support mode by plastic clay and organic matter. Accordingly, the shear strength and friction coefficient of shale both decrease, and the shear type transforms from brittle to plastic.When the content of clay and organic matter is low, the asperity of friction surfaces will break in a brittle manner and the wear degree of surfaces is low. Therefore, fractures are still featured by moderate apertures after friction.The lower the content of clay and organic matter is, the easier the asperity of crack surfaces supports themselves,and the higher the fracture residual permeability is. Thus, promoting shear slip is the main measure of reservoir stimulation. However, when the content of clay and organic matter is high, the remaining post-slip fracture aperture is small. It is difficult to increase reservoir permeability through the frictional slip of natural fractures,and in this situation, the proppant support efficiency needs to be improved.     

不同围压和流体饱和状态下致密砂岩弹性各向异性特征

为研究致密砂岩声波速度及其各向异性随围压的变化规律以及不同流体饱和状态下的弹性各向异性特征,钻取了不同方向的岩心并在实验室超声波频率下对致密砂岩的声学特性进行了测量,分别给出干燥和饱和水状态下,不同方向样品纵横波速度、刚性系数以及各向异性系数随围压的变化规律,并对实验结果进行了分析讨论.实验结果表明致密砂岩纵横波速度、纵横波速度比以及刚性系数均随围压增加而增加,但其在不同饱和状态下的变化率却截然不同;纵横波速度比、各向异性系数在饱和水状态下变化规律不明显,表明孔隙流体的存在对于岩石物理性质有着非常重要的影响.这方面的实验工作不但对于考察不同流体性质对致密岩石弹性各向异性影响是必要的,而且有助于致密砂岩油水和气层的识别.     

Influence of Bedding and Mineral Composition on Mechanical Properties and Its Implication for Hydraulic Fracturing of Shale Oil Reservoirs

The premise of hydraulic fracturing is to have an accurate and detailed understanding of the rock mechanical properties and fracture propagation law of shale reservoirs. In this paper, a comprehensive evaluation of the mechanical properties of the shale oil reservoir in the south of Songliao Basin is carried out. Based on the experiments and the in-situ stress analysis, the fracture propagation law of three types of shale reservoirs is obtained, and the suggestions for fracturing are put forward. The results have shown that the fracture propagation of pure shale and low mature reservoir is easy to open along the bedding plane under compression loading, which is greatly influenced by the bedding. Sand-bearing shale is slightly better, the fractures of which are not easy to open along the bedding plane. The mechanical experimental results show that all the samples have the characteristics of low compressive strength, low Young''s modulus and strong anisotropy, indicating that the shale oil reservoir is certain plastic, which is related to its high clay mineral content and controlled by the bedding development. Compared with pure shale and low mature shale, the sand-bearing shale has less clay content and less developed bedding, which maybe the main reason for its slightly better brittleness. Overall, the expansion of hydraulic fracture is controlled by in-situ stress and bedding. Because of the development of bedding, it is easy to form horizontal fractures. Thus it is not suitable for horizontal well fracturing. Because of the high content of clay minerals, the applicability of conventional slick hydraulic fracturing fluid is poor. It is suggested to use vertical well or directional well to carry out volume fracturing. In this way, the effect of bedding can be effectively used to open and connect the bedding and form a larger fracture network.     

泥质砂岩液相渗透率计算新方法

液相渗透率描述了岩石的渗流特性,是评价储层与预测油气产能的重要参数.液相渗透率是指盐水溶液在岩石孔隙中流动且与岩石孔隙表面黏土矿物发生物理化学作用时所测得的渗透率;液相渗透率的实验测量条件更加接近实际地层泥质砂岩的条件,使得液相渗透率更能反映地层条件下泥质砂岩的渗流特性;然而,现有的液相渗透率评价模型较少,且模型未能揭示液相渗透率与溶液矿化度之间的关系.基于此,开展了液相渗透模型推导与计算方法研究;文中首先将岩石等效为毛管束模型,推导建立了液相渗透率与比表面、喉道曲折度、总孔隙度、黏土束缚水孔隙度等参数之间的关系;其次,根据岩石物理体积模型,推导建立了黏土束缚水孔隙度与阳离子交换容量、溶液矿化度等参数的关系;最终,将黏土束缚水孔隙度引入液相渗透率计算公式,建立了基于总孔隙度、阳离子交换容量、溶液矿化度、比表面、喉道曲折度等参数的液相渗透率理论计算模型.液相渗透率计算模型与两组实验数据均表明,液相渗透率随阳离子交换容量的增大而降低,随溶液矿化度的增大而增大.然而,液相渗透率理论计算模型的实际应用中喉道曲折度、比表面等参数求取困难,直接利用理论模型计算液相渗透率受到限制.在分析液相渗透率与孔隙渗透率模型的基础上,建立了液相渗透率与空气渗透率之间的转换模型,形成了利用转化模型计算液相渗透率的新方法.为进一步验证液相渗透率与空气渗透率转化模型的准确性,基于两组实验数据,利用转换模型计算了液相渗透率;液相渗透率计算结果与岩心测量液相渗透率实验结果对比显示,液相渗透率计算结果与实际岩心测量结果吻合较好,文中建立的液相渗透率与空气渗透率转化模型合理可靠.     

四川盆地侏罗系致密砂岩弹性特征及岩石物理建模

近年来围绕四川盆地侏罗系陆相致密砂岩已取得了勘探突破,其中川中—川西过渡带具备形成大气田的地质条件,但对该套致密砂岩弹性性质变化规律的研究还较少,致使利用地震方法进行"甜点"储层预测的精度不高.本文利用四川盆地侏罗系沙溪庙组32块样品开展了系统的声学测量,在此基础上,分析了样品弹性性质的变化规律.结合X射线衍射矿物组分分析、扫描电镜、铸体薄片和岩石薄片特征确定了不同成岩作用对岩石储集性能的影响.研究结果表明,研究区致密砂岩储层表现为孔隙型储层,受差异性成岩作用影响,黏土含量、钙质含量和硅质含量的差异以及它们分布特征之间的差异对岩石弹性性质造成了很大的影响.在研究区对岩石物性及弹性性质有明显影响的成岩作用包括早期的钙质胶结作用、压实作用和溶蚀作用,因此针对不同时期的成岩作用对岩石弹性及物性的影响,利用接触-胶结模型、微分等效模量模型和临界孔隙度校正的Hashin-Shtrikman上限模型建立了研究区致密砂岩的岩石物理模型.     

Quantitative characterization of reservoir space in the Lower Silurian Longmaxi Shale,southern Sichuan,China

Based on the drilling data of the Upper Ordovician Wufeng Shale and the Lower Silurian Longmaxi Shale in southern Sichuan Basin,the construction of matrix pores and the development condition of fractures in a marine organic-rich shale are quantitatively evaluated through the establishment of the reservoir petrophysical models and porosity mathematical models.Our studies show that there are four major characteristics of the Longmaxi Shale confirmed by the quantitative characterization:(1)the pore volume of per unit mass is the highest in organic matter,followed in clay minerals,finally in brittle minerals;(2)the porosity of the effective shale reservoir is moderate and equal to that of the Barnett Shale,and the main parts of the shale reservoir spaces are interlayer pores of clay minerals and organic pores;(3)the porosity of the organic-rich shale is closely related to TOC and brittle mineral/clay mineral ratio,and mainly increases with TOC and clay mineral content;(4)fractures are developed in this black shale,and are mainly micro ones and medium-large ones.In the Longmaxi Shale,the fracture density increases from top to bottom,reflecting the characteristics with high brittle mineral content,high Young’s modulus,low Poisson's ratio and high brittleness at its bottom.