磁组构的分离与岩石构造变形分析

目前实验条件下获得的AMS（磁化率各向异性）是岩石内所有磁性矿物磁化率各向异性叠加的综合响应,详细的岩石磁学和构造地质学的综合分析表明常规AMS测试结果通常无法揭示岩石复杂的构造变形过程.本文综述了运用非磁滞剩磁各向异性（AARM）、低温AMS（LT-AMS）和高场AMS（HF-AMS）等实验方法对岩石AMS组分进行分离,可以定量获取不同磁性矿物的磁组构贡献,进而解释其不同的变形特征.在此基础上阐述了近年来针对不同磁性矿物组合的AMS分离方法的理论技术创新和进展及其在岩石构造变形特征分析中的应用前景,讨论了常见磁性矿物单晶的岩石磁学性质及各向异性度（P_j）与形状因子（T）在揭示岩石变形特征中的复杂性与局限性,最后举例并分析了磁组构分离技术在造山带岩石构造变形分析中的应用.

     

Correlation of strain with anisotropy of magnetic susceptibility (AMS)

Existing correlations between strain and anisotropy of low-field magnetic susceptibility (AMS) have been re-assessed using a single parameter to express both anisotropies. TheP parameter (Hrouda, 1982) shows potential as a powerful single expression of the intensity of strain and of AMS. Previous correlations are improved by use of this parameter. Cautious optimism is justified for correlations between strain and susceptibility in a certain strain window between a lower limit (excluding the incomplete overprint of predeformation anisotropy) and an upper limit (excluding the effects of saturation anisotropy). For successful correlations the influence of stress-controlled recrystallisation should be minimal and the mineralogical sources of susceptibility must predate deformation.     

Microstructure and magnetic fabric in the Shuanghe pluton: A synkinematic granite in Eastern Dabie Mountains,China

Strain analyses for the Shuanghe pluton show that the main strain planes suffered distinct deformation. The main strain value (XZ) is up to 1.59-2.18, and the value of Flinn index (K) ranges from 0.11 to 0.82. Anisotropy of magnetic susceptibility (AMS) measurements reveal that the orientations of the magnetic foliation and lineation gently dip SE, consistent with the macroscopic foliation of the pluton. The value of anisotropy degree (P) ranges from 1.109 to 1.639, and the shape parameter (7) from 0.079 to 0.534. These studies prove that the pluton was deformed under strong compression. Quartz c-axis textures, defined by monoclinic or triclinic asymmetry, usually developed the high maxima paralleling the b-axis, which is defined by the developed in the high-ultrahigh pressure rocks (UHP) which were captured in the pluton or country rocks. It is concluded that the Shuanghe pluton emplaced under regional compression slightly after the formation of UHP, and it is characterized by synkinematic granitic deformation.     

Origin of layering in cumulate gabbros in the Oman ophiolite: Insights from magnetic susceptibility measurements in the Wadi Sadm area

Abstract   Magnetic susceptibility and the anisotropy of magnetic susceptibility were measured on an 800-cm-thick succession of cumulate gabbro in the Sadm area of the Oman ophiolite. The section contained three distinct cumulate units. The susceptibility tends to decrease upward in each from a melanocratic layer (several tens of centimeters thick) to a leucocratic layer (a few meters thick). The susceptibility decreases in accordance with the decreasing number of magnetite grains, which are the alteration product mainly of olivine minerals. This suggests the cyclic downward accumulation of olivine in the cumulate gabbro. The apparent strain deduced from the patterns of magnetic and grain fabrics was the result mostly of simple shear, so that the layering of gabbro is understood to be formed primarily by a crystal cumulus process followed by simple shear deformation.     

Magnetic fabric of bulgarian loess sediments derived by using various sampling techniques

Summary The anistropy of low field magnetic susceptibility has been studied for seven outcrops of loess sediments in North-Eastern Bulgaria. Different sampling methods were applied in order to choose the best technique for obtaining the primary magnetic fabric of such unconsolidated sediments. AMS results show significant changes in the petrofabric of samples collected by the first technique which disturbs the original sedimentary fabric. The second applied technique does not cause such a strong deformation but some disturbance of the magnetic fabric is probable. Typical sedimentary fabric is obtained from hand samples and it is therefore concluded that this represents the best method for obtaining reliable AMS results from soft sediments.     

High magnetic susceptibility produced by thermal decomposition of core samples from the Chelungpu fault in Taiwan

We carried out thermomagnetic susceptibility analyses of fault rocks from core samples from Hole B of the Taiwan Chelungpu Fault Drilling Project (TCDP) to investigate the cause of high magnetic susceptibilities in the fault core. Test samples were thermally and mechanically treated by heating to different maximum temperatures of up to 900 °C and by high-velocity frictional tests before magnetic analyses. Thermomagnetic susceptibility analyses of natural fault rocks revealed that magnetization increased at maximum heating temperatures above 400 °C in the heating cycle, and showed three step increases, at 600 to 550 °C and at 300 °C during the cooling cycle. These behaviors are consistent with the presence of pyrite, siderite and chlorite, suggesting that TCDP gouge originally included these minerals, which contributed to the generation the magnetic susceptibility by thermomechanical reactions. The change in magnetic susceptibility due to heating of siderite was 20 times that obtained by heating pyrite and chlorite, so that only a small fraction of siderite decomposition is enough to cause the slight increase of the susceptibility observed in the fault core. Color measurement results indicate that thermal decomposition by frictional heating took place under low-oxygen conditions at depth, which prevented the minerals from oxidizing to reddish hematite. This finding supports the inference that a mechanically driven chemical reaction partly accounts for the high magnetic susceptibility. A kinetic model analysis confirmed that frictional heating can cause thermal decomposition of siderite and pyrite. Our results show that decomposition of pyrite to pyrrhotite, siderite and, to some extent, chlorite to magnetite is the probable mechanism explaining the magnetic anomaly within the Chelungpu fault zone.     

Magma flow revealed by magnetic fabric in the Okavango giant dyke swarm, Karoo igneous province, northern Botswana

To determine the magma flow direction of the giant, 179 Ma Okavango dyke swarm of northern Botswana, we measured the anisotropy of magnetic susceptibility (AMS) of 23 dykes. Dykes are located in two sections (Shashe and Thune Rivers), which are about 300 km and 400 km from the presumed magma source respectively; the Nuanetsi triple point. We collected samples from the margins of the dykes in order to use the imbrication of magnetic foliation to determine magma flow direction. About half of the magnetic fabric in the dykes is inverse, i.e. with the magnetic foliation perpendicular to the dyke plane. Lateral flow to the west and vertical flow is in evidence in the Shashe section. However, the overall analysis of normal and inverse magnetic fabric data supports that lateral flow to the west was dominant in the Shashe section. Across the Thune section, a poorly defined imbricated magnetic foliation also suggests lateral flow to the west.     

Post-emplacement tilting of lava flows inferred from magnetic fabric study: the example of Oligocene lavas in the Jeanne d’Arc Peninsula (Kerguelen Islands)

Statistical analysis of the magnetic fabric of samples from several successive lava flows emplaced under similar conditions can allow determination of the mean flow direction when magnetic fabric data from individual flows do not lead to reliable results. A difference between the obtained flow direction and the present dip direction indicates that the flows were tilted after emplacement. For 2 successive series of flows on the Jeanne d’Arc Peninsula presently NNW dipping, this method shows lava emplacement along a SSW–NNE direction. This indicates a gentle tilting acquired during a period of weak deformation in the whole archipelago. Additionally, the magnetic fabric data allow the reconstruction of the different conditions of emplacement of these two series of lava flows and of formation of the local thick conglomerate interbedded between these series.     

Low-field variation of magnetic susceptibility measured by the KLY-4S Kappabridge and KLF-4A magnetic susceptibility meter: Accuracy and interpretational programme

The KLY-4S Kappabridge and KLF-4A Magnetic Susceptibility Meter enable automated measurement of susceptibility variation with field in the ranges of 2–450 A/m and 5–300 A/m (in effective values), respectively. Unfortunately, the measurement accuracy decreases with decreasing field and it is not easy to decide whether the susceptibility variation at the lowest fields is natural phenomenon or results from measuring errors. To overcome this problem, the accuracies of both the above instruments were investigated experimentally using artificial specimens (mixture of pure magnetite and plaster of Paris) with variable susceptibilities ranging from 1 × 10⁻⁵ to 5 × 10⁻². The complete curve of the field variation of susceptibility of each specimen was measured 10 times and the relative error was calculated for each field. In the KLY-4S Kappabridge, in specimens with susceptibilities higher than 100 × 10⁻⁶, the relative errors are lower than 3% in all fields and lower than 1% in the fields stronger than 10 A/m. In the KLF-4A Magnetic Susceptibility Meter, in relatively strongly magnetic specimens with susceptibilities 5 × 10⁻⁴ to 5 × 10⁻², the relative error is less than 1.5% in the entire field range. While the former instrument is convenient for investigating almost all rock types, the latter instrument is convenient for measuring moderately and strongly magnetic specimens. To facilitate work with field variation of susceptibility curves, showing variable accuracies with field, the programme FieldVar was written. One of its options is plotting the measured data with corresponding field-variable error bars. In this way, a tool is offered for interpreting such susceptibility changes that are sound and reasonable from the point of view of measuring accuracy.     

磁组构与构造变形

磁组构通常指磁化率各向异性,即AMS（Anisotropy of Magnetic Susceptibility）,是一种重要的岩石组构,是弱变形沉积岩地区灵敏的应变指示计.近年来,AMS在造山带及前陆地区的广泛应用为构造变形研究提供了极大的帮助,同时提升了该方法的理论认识.本文在研读最新相关文献与著作的基础上,结合笔者及研究团队在龙门山地区获得的磁组构研究成果,综述了磁组构在沉积岩地区构造变形研究中的应用进展,并基于现有的研究认识对关键问题进行讨论,提出以下几点认识：（1）磁性矿物分析是AMS研究的关键,应结合多种岩石磁学实验及光学与电子显微构造研究手段展开详细的磁性矿物学分析;（2）磁化率椭球与应变椭球的对应主轴在绝大多数情况下相互平行,但在不同期次、不同种类复杂的磁性矿物组成,或者多期次构造变形的影响下,AMS与应变的关系相对复杂,应比对高场和低温AMS及非磁滞剩磁各向异性（AARM）测试结果,获得不同矿物的优选定向特征,并对获得的组构进行分期;（3）AMS可以揭示造山带及其前陆地区的构造演化历史,并且是分析断层相关褶皱的有限应变特征和变形机制的重要方法,同时也是厘定断裂带变形性状和期次及运动学分析的有效手段;（4）磁组构形成于成岩作用早期或构造变形的最早阶段,能很好地记录褶皱和逆冲作用之前的平行层缩短变形,因此可以揭示同沉积阶段的古构造应力方向.后期足够强烈的构造变形能局部改造或彻底掩盖先存AMS记录,构造流体有关的同构造期结晶矿物或先存矿物的重结晶导致的再定向被认为是其根本原因;（5）斜交磁线理是一种特殊的磁组构类型,反映了区域构造叠加或多期构造变形作用或隐伏斜向逆冲等可能的构造过程,有必要结合多方面的地质证据对其成因作出合理解释.

     

南海北部陆区岩石磁化率的矿物学研究

基于2517套现场测量资料,245块岩石样品的体积磁化率测量和详细的岩矿鉴定及硅酸盐全分析结果,结合单矿物磁化率特征及各岩石之间的对比研究,发现岩石磁化率主要受组成岩石的矿物磁化率控制.即岩石磁化率(κr)与组成岩石各个矿物磁化率(κi)及其体积含量(Ci)成正比.例如侵入岩磁化率,κr= -5.68×102Cq +2.86×102Cf +3.28×102Ca +1.18×104Cb +1.27×104Cam +5.35×105Cm;其中多项式各项的系数是与该矿物磁化率值成正比的常数,C为该矿物在该岩石中的体积含量,依次为石英q(κ=-1.3)、斜长石f(κ=0.01)、碱性长石a(κ=0.01)、黑云母b(κ=100)、角闪石am(κ=80)和磁铁矿m(κ=100000).对区内火山岩、侵入岩、沉积岩和变质岩磁化率研究发现,其他三类岩石磁化率与其组成矿物磁化率的关系和侵入岩的情况相同,矿物对岩石磁化率的贡献顺序为铁磁性矿物>顺磁性矿物>逆磁性矿物.其中,火成岩磁化率变化大,主要取决于岩石中磁铁矿、角闪石和黑云母的含量;沉积岩多为无磁性、弱磁性,其磁化率主要由黑云母、碱性长石及岩屑提供;变质岩的磁性变化较大,从无磁性到极强磁性,主要决定于其原岩的类型,副变质岩(沉积原岩)磁化率类似于沉积岩类,正变质岩(火成原岩)类似于火成岩类;石英岩和碳酸盐岩是所有岩石中磁性最弱的.岩石蚀变会对其磁化率产生显著性影响,通常,黑云母、角闪石等铁镁硅酸盐矿物经蚀变会因形成含铁质氧化物而使岩石的磁化率升高;长石等弱顺磁矿物的粘土矿化、绢云母化会升高磁化率而碳酸盐化、高岭土化作用会使磁化率降低;岩石的绿泥石化会增加磁化率;含铁磁性矿物的岩石风化时会因高磁性组分破碎、流失而致使岩石的磁化率降低.从岩石磁化率与其组成矿物的磁化率之间的关系,推测地质体的总磁化率与构成地质体各个岩石的磁化率-体积含量之间也应存在类似关系.     

巴基斯坦Bahawalpur黄土岩石磁学特征及磁化率变化机制研究

风成黄土是陆地上分布最广泛的沉积物之一,记载了各种古气候演化信息.目前巴基斯坦的黄土研究甚少,磁化率与气候对应的变化机制研究尚未开展.本文对位于巴基斯坦印度河平原Bahawalpur地区新发现的黄土-古土壤剖面进行系统的岩石磁学研究,结合粒度和漫反射光谱(DRS)数据,讨论巴基斯坦黄土的磁化率变化机制.实验结果显示：Bahawalpur (BH)剖面黄土层主要的载磁矿物为磁铁矿,同时含有少量磁赤铁矿和针铁矿,磁性颗粒以原生的MD和PSD颗粒为主.相对于黄土层,古土壤层则是以针铁矿为主,含有顺磁性矿物和少量磁铁矿.BH剖面磁化率与成土作用关系和中国黄土高原典型剖面相反,磁化率的变化可能存在一个阈值12.8×10^-8m³·kg^-1,在阈值之上,强磁性矿物(磁铁矿、磁赤铁矿)占主导;阈值之下,以弱磁性矿物(主要是针铁矿)为主,这种磁性矿物的转变可能导致磁化率降低.本文可为今后利用磁化率解读该地区地层蕴含的古气候信息提供新线索.

     

The anisotropy of magnetic susceptibility of lava flows: an experimental approach

Measurements of the anisotropy of magnetic susceptibility (AMS) of natural lavas have shown that AMS varies with depth within a lava flow. We have investigated the reasons for such variation by studying the effects of temperature and strain rate on the AMS of recent lava in the laboratory. Samples of lava from Kilauea were melted and subjected to a range of strain rate and cooling histories. The results show that the degree of anisotropy is a function of both the thermal and shearing history of a sample. High degrees of anisotropy were found only in samples that were deformed at temperatures close to those encountered during eruption and then rapidly quenched. Lavas subjected to similar shear stresses at high temperatures had low degrees of anisotropy if allowed to cool down slowly without further deformation. Additionally, lava subjected to complex shearing yield a lower degree of anisotropy even when high strain rates were imposed on it. These results lead to the conclusion that only the last phase of deformation is detectable using AMS and that high strain rates will not result in high degrees of anisotropy if either deformation ends while lava is still fluid or if the orientation of the maximum shear stress varies with time. The relation between the orientation of the principal susceptibilities and that of shear is less sensitive to variation on shear with time. Consequently, flow directions can be inferred confidently with this type of measurements.     

Determining flow patterns and emplacement dynamics from tsunami deposits with no visible sedimentary structure

In the absence of eyewitness reports or clear sedimentary structures, it can be difficult to interpret tsunami deposits or reconstruct tsunami inundation patterns. The emplacement dynamics of two historical tsunami deposits were investigated at seven transects in Okains Bay, New Zealand, using a combined geospatial, geomagnetic and sedimentological approach. The tsunami deposits are present as layers of sand and silt intercalated between soils and become finer and thinner with distance inland. The deposits are attributed to the 1960 and possibly the 1868 tsunamis, based on radiometric dating and correlation with historical records. Measurements of Magnetic Fabric (MF: Anisotropy of Magnetic Susceptibility) and particle size were used to reconstruct the evolution of flow dynamics laterally and vertically. A combination of statistical methods, including spatial autocorrelation testing, Spearman's rank order correlation, Principal Component Analysis (PCA) and K‐means cluster analysis, was applied to examine relationships between MF parameters and sediment texture, and infer depositional hydrodynamics. Flow patterns deduced from MF show the estuary channel acted as a conduit for inundation, with flow commonly aligned sub‐perpendicular to the estuary bed. MF and sediment data suggest deposition occurred from settling during laminar flow. Evidence of both uprush and backwash deposition, as well as wave reflection from infrastructure, was found. Statistical analysis of data showed significant relationships between grain size parameters and MF parameters associated with flow speed and magnetic fabric type. PCA and cluster analysis differentiated samples into two primary hydrodynamic groups: (1) samples deposited from laminar flow; and (2) samples deposited close to the limit of inundation, which includes samples deposited further inland, those affected by flow convergence, and those in the upper part of tsunami deposits. This approach has potential as a tool for reconstructing hydrodynamic conditions for palaeotsunamis and by combining spatial and statistical analyses, large‐scale investigations can be more easily performed. Copyright © 2016 John Wiley & Sons, Ltd.     

Pressure Instability of Magnetic Susceptibility of Pyrrhotite Bearing Rocks from the KTB Borehole

Experimental results of pressure-induced changes in mean magnetic susceptibility of rock samples from the main KTB borehole are reported. It was found that susceptibility values of rocks from depths between 5200 and 7000 m show unstable behaviour upon application of pressure, showing an increase in susceptibility of between 20 and 120%. This unstable behaviour was only detected in samples from the above mentioned depth interval, which contain both ferrimagnetic and antiferromagnetic phases of pyrrhotite. On the basis of thermomagnetic analysis, magnetic field treatment, optical microscopy and domain observations of undeformed and deformed samples, reasons for this instability are discussed and interpreted in relation to redistribution of internal stresses within the ferrimagnetic phase, resulting in changes in domain wall mobility.     

冀鲁豫交界区岩石圈磁场异常分布与磁化率结构分析

利用重磁反演软件,对2017年8月冀鲁豫交界区流动地磁总强度数据进行处理并解析延拓,研究该区岩石圈磁场及其深部、浅表磁场异常分布特征与地下介质磁化率结构的性质。结果表明:冀鲁豫交界区岩石圈磁场异常分布是岩石圈浅表与深部磁异常综合叠加的结果,岩石圈地下介质的浅表与深部磁化率结构具有一定差异性,且受断裂控制呈分段性特征,可能与该区域复杂的岩石圈磁化率结构及地质构造有关。     

Multiple origins and interpretations of the magnetic susceptibility signal in Chinese wind-blown sediments

In most Chinese loess–paleosol sequences, high magnetic susceptibility values are found in the soil horizons, with low values in the loess layers. The susceptibility signal has been widely used as a proxy climatic indicator. However, both the causes and mechanisms which control susceptibility still remain controversial. Our recent studies challenge some earlier interpretations of the magnetic susceptibility signal in Chinese wind-blown sediments. First, the prevailing hypothesis of pedogenic origin cannot totally account for the susceptibility variations in many sections. Second, in some cases, the principal carrier of the magnetization seems not to be the ultrafine pedogenic minerals, rather coarse lithogenic magnetic minerals derived from local sources can also contribute significantly to the susceptibility signal. Finally, not all the Chinese soils have higher susceptibility values than that of loess or sand layers, opposite relationships do exist. It is concluded that the source and causes of susceptibility may be different from site to site or even at different times at a given site. Any single hypothesis cannot completely account for the susceptibility variations in the Chinese Loess Plateau and its surrounding regions. Besides the previous explanations of carbonate leaching, pedogenic processes and organic decomposition, the contribution of source materials to magnetic susceptibility must also be taken into account.     

Alteration induced changes of magnetic fabric as exemplified by dykes of the Koolau volcanic range

We studied 93 samples from 8 basaltic dykes of the Koolau volcanic range on the island of Oahu,Hawaii,USA,to determine the influence of hydrothermal alteration on the magnetic fabric as determined by anisotropy of magnetic susceptibility (AMS) measurements. Rock magnetic as well as microscopic investigations show that only ≈25% of the samples have retained their original magnetomineralogical composition of unaltered Ti-poor titanomagnetite. The remaining samples have undergone hydrothermal alteration which transformed the primary magnetic phase into a granular intergrowth of titanomagnetite, titanomaghemite and hematite. In both sample groups,this magnetic phase occurs in coarse (tens of microns),irregularly shaped particles as well as interstitial clusters of smaller (< 5 μm) grains. Our investigations show that hydrothermal alteration does change the bulk susceptibility and the degree of anisotropy but not the directions of principal axes of the AMS ellipsoid which are predominantly corresponding to normal magnetic fabric. The stability of AMS directions, regardless of the degree of alteration, points towards the model of distribution anisotropy as the controlling factor for the observed magnetic fabric.     

空间波数混合域三维各向异性强磁性介质磁场数值模拟

各向异性普遍存在于强磁性体矿物中,为研究各向异性强磁性体磁场响应特征,本文提出一种空间波数混合域三维各向异性磁场数值模拟方法.该方法首先将各向异性强磁性体磁位满足的三维偏微分方程进行水平方向二维傅里叶变换,将其降为不同波数之间相互独立的一维常微分方程;然后加载准确的上下边界条件,采用二次插值有限单元法计算一维常微分方程,得到五对角方程,采用追赶法进行高效求解;最后采用迭代法求解场分量,引入紧算子保证迭代稳定收敛;综合傅里叶变换的高效性、一维方程求解的快速性和迭代算法的稳定性,实现各向异性强磁性体磁场的三维高效、高精度数值模拟.设计各向异性椭球模型验证算法的正确性,并分析紧算子对不同各向异性磁化率模型的迭代收敛性;与COMSOL Multiphysics软件对比计算效率,表明相同节点下本文算法效率优于常规三维有限元方法,且计算节点总数越多优势越明显.重点研究各向异性参数改变对VTI、HTI、TTI强磁介质异常场响应的影响.最后采用某磁铁矿DEM高程数据模拟起伏地形对各向异性强磁性体磁异常场幅值和形态的影响,体现出本文算法对各向异性强磁性体大规模复杂地形的适应性.

     

Anisotropy of magnetic remanence: A brief review of mineralogical sources,physical origins,and geological applications,and comparison with susceptibility anisotropy

The magnetic fabric of rocks and sediments is most commonly characterized in terms of the anisotropy of low-field magnetic susceptibility (AMS). However, alternative methods based on remanent magnetization (measured in the absence of a magnetic field) rather than induced magnetization (measured in the applied field) have distinct advantages for certain geological applications. This is particularly true for; (1) adjunct studies in paleomagnetism, in order to assess the fidelity with which a natural remanence records the paleofield orientation; (2) studies of weakly magnetic or weakly deformed rocks, for which susceptibility anisotropy is very difficult to measure precisely; and (3) quantitative applications such as strain estimation. The fundamental differences between susceptibility and remanence (and their respective anisotropies) are due to several factors: (1) susceptibility arises from all of the minerals present in a sample, whereas remanence is carried exclusively by a relatively small number of ferromagnetic minerals; (2) ferromagnetic minerals are generally more anisotropic than para- and diamagnetic minerals; (3) for ferromagnetic minerals, remanence is inevitably more anisotropic than susceptibility; and (4) a number of common minerals, including single-domain magnetites, possess an inverse anisotropy of susceptibility, i.e., they tend to have minimum susceptibility parallel to the long axis of an individual particle; remanence is immune to this phenomenon. As a consequence of all these factors, remanence anisotropy may generally provide a better quantitative estimate of the actual distribution of particle orientations in a rock sample.Contribution number 9102 of the Institute for Rock Magnetism, University of Minnesota.