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1.
Optically stimulated luminescence (OSL) dating of polymineral fine-grained loess samples collected from the southern Loess Plateau of China was conducted using the single-aliquot regenerative-dose (SAR) protocol. A ‘Double-SAR’ procedure in which aliquots are subjected to both infrared (IR) and blue stimulations was used, and two sets of equivalent dose (D e ) determinations were produced. These doses are assumed to be predominantly related to the feldspathic and quartz fine grain populations, respectively. The results revealed that the OSL ages estimated by infrared stimulated luminescence (IRSL) signals and those estimated by [post-IR] stimulated luminescence ([post-IR] OSL) signals disagreed. Specifically, the ages estimated using the IRSL signals were smaller than those estimated using [post-IR] OSL signals. The results of an anomalous fading test of the two types of OSL signals revealed that the [post-IR] OSL signals from the etched sub-sample (by H2SiF6 and HF) and the un-etched sub-sample did not fade significantly. However, the IRSL signals from the un-etched sub-sample showed obvious signs of fading. These findings indicate that the lower age estimated by IRSL is due to the anomalous fading of feldspar IR signals in the polymineral fine grains. For samples collected from greater than 100 cm, the estimates of their OSL ages using two types of luminescence signals generally agreed with their pre-estimated ages, especially those of the [post-IR] OSL signals. However, for the three samples that were collected from a depth of less than 100 cm, their OSL ages were remarkably underestimated, possibly due to the enhanced human activity (such as soil cultivation) that has occurred in the region since 3000 a B.P.  相似文献   

2.
A study was made of the applicability of three different techniques for equivalent dose (De) determination in the optical dating of quartz: the single‐aliquot regenerative‐dose technique (SAR), the single‐aliquot additive‐dose technique (SAAD) and the multiple‐aliquot additive‐dose technique (MAAD). For this purpose, quartz grains were extracted from a sequence of Upper Pleniglacial to Late‐glacial coversands exposed at the locality of Ossendrecht in the southwestern Netherlands, a site for which both radiocarbon and earlier luminescence dates are available, providing independent age control. Upon testing the different assumptions underlying each of the three OSL techniques investigated, the SAR protocol was found to be the technique of choice. The optical ages obtained with this protocol were in good agreement with the chronostratigraphical position of the sediments investigated and with the available chronostratigraphical information on the same and equivalent deposits. This confirms the suitability of the SAR technique for dating coversands. Furthermore, a small laboratory intercomparison of SAR‐based De determinations yielded results that were in fair overall agreement. Copyright © 2004 John Wiley & Sons, Ltd.  相似文献   

3.
从湖南省北部赤山岛枫树嘴旧石器遗址剖面第2、第3和第4考古层位采集的3个沉积物样品中提取的细粒混合矿物,尝试对其红外释光(IRSL)信号进行研究。实验表明,虽然长石IRSL信号很弱,但仍可以测得信噪比足够高的红外激发后高温红外激发释光(post-IR IRSL)信号。与此同时,样品存在明显的红外激发后蓝光释光(post-IR OSL)信号,并且样品的IRSL与post-IR OSL信号均以快组分为主,这为该地区沉积物利用长石光释光信号定年提供了新的可能。鉴于长石IRSL信号较弱,根据剂量恢复实验结果,本研究采用post-IR IRSL SAR法(50℃红外激发后270℃高温红外激发,pIRIR270℃)进行等效剂量测量,同时也应用post-IR OSL SAR法定年进行比较。实验结果表明,细粒混合矿物的pIRIR270℃等效剂量分别为418.8±13.2 Gy、562.3±18.2 Gy和694.8±17.9 Gy,相对应的post-IR OSL SAR等效剂量结果为345.0±29.4 Gy、409.6±33.7 Gy和424.7±32.2 Gy。假设强烈化学风化未对沉积物的剂量率造成很大影响,基于长石pIRIR270℃信号的释光年龄为89±6 ka、118±8 ka和152±9 ka,比前人所得的石英OSL SAR法年龄老30%~55%(约20~55 ka)。通过对比不同测量条件下获得的等效剂量值来评估长石IRSL信号是否存在晒退问题,没有发现长石post-IR IRSL信号存在晒退不完全的证据。根据本研究post-IR IRSL SAR法测年结果,赤山岛枫树嘴旧石器遗址似阿舍利技术类型的石器出现在倒数第二次冰期(MIS 6)后期至末次间冰期(MIS 5)前期,比湖南道县福岩洞现代人类牙齿化石年龄(80~120 ka)稍老。作为似阿舍利技术石器制造者的赤山岛古人与福岩洞现代人的关系将是我国旧石器时代考古学和古人类学研究的一个重要课题。  相似文献   

4.
The loess–palaeosol sequence of Batajnica (Vojvodina region, Serbia) is considered as one of the most complete and thickest terrestrial palaeoclimate archives for the Middle and Late Pleistocene. In order to achieve a numerical chronology for this profile, four sets of ages were obtained on 18 individual samples. Equivalent doses were determined using the SAR protocol on fine (4–11 μm) and coarse (63–90 μm) quartz fractions, as well as on polymineral fine grains by using two elevated temperature infrared stimulation methods, pIRIR290 and pIRIR225. We show that the upper age limit of coarse quartz OSL and polymineral pIRIR290 and pIRIR225 techniques is restricted to the Last Glacial/Interglacial cycle due to the field saturation of the natural signals. Luminescence ages on coarse quartz, pIRIR225 and pIRIR290 polymineral fine grains are in general agreement. Fine quartz ages are systematically lower than the coarse quartz and pIRIR ages, the degree of underestimation increasing with age. Comparison between natural and laboratory dose response curves indicate the age range over which each protocol provides reliable ages. For fine and coarse quartz, the natural and laboratory dose response curves overlap up to ~150 and ~250 Gy, respectively, suggesting that the SAR protocol provides reliable ages up to c. 50 ka on fine quartz and c. 100 ka on coarse quartz. Using the pIRIR225 and pIRIR290 protocols, equivalent doses up to ~400 Gy can be determined, beyond which in the case of the former the natural dose response curve slightly overestimates the laboratory dose response curve. Our results suggest that the choice of the mineral and luminescence technique to be used for dating loess sediments should take into consideration the reported limited reliability.  相似文献   

5.
We report direct luminescence ages for the culture‐bearing sediments of the Kebaran site of Nahal Hadera V (NHV) in the coastal plain of Israel. Although the site contains, in addition to rich lithic deposits, plentiful mammalian bone, it has proved to be undatable using radiocarbon dating, in spite of the fact that the cultural context places the time of occupation well within the range of radiocarbon dating. In contrast, luminescence dating of the site sediments proved successful. Luminescence ages were determined using the single aliquot additive‐dose (SAA) method, applied to sand‐sized quartz extracts to determine past equivalent doses (De). Dose rates (R) were calculated using thick source alpha counting for the uranium (U) and thorium (Th) concentrations and x‐ray fluorescence analysis for the potassium (K20) concentration. Of the five samples collected at the site, four represent cultural and subcultural deposits and the fifth represents the geological substrate for the archaeological deposit, a quartz‐rich, carbonate‐cemented dune sand known as aeolianite or kurkar. The luminescence age of the kurkar is 42.7 ± 6.3 ka. Human occupation of the site occurred between 21.3 ka and 14.0 ka ago, during the Last Glacial Maximum. © 2003 Wiley Periodicals, Inc.  相似文献   

6.
湖泊沉积物的14 C和光释光测年* ——以固城湖为例   总被引:3,自引:0,他引:3  
富含有机质的湖泊沉积物被认为是14 C测年建立古环境记录年代标尺的理想材料,光释光测年方法近年开始应用于水成沉积物的定年。应用14 C和光释光两种方法对江苏固城湖湖心钻孔岩芯进行了年龄测定,结果表明全样有机质的14 C年龄与石英的光释光年龄存在系统差异,后者较前者年轻约2000年。系统光释光测年研究排除了光释光年龄低估的可能性,所以,二者的差异可能是湖泊沉积物碳库效应的反映。  相似文献   

7.
The infrared stimulated luminescence (IRSL) dating method is applied to alkali feldspar coarse grains from the two distinct Middle Pleistocene interglacial estuarine deposits of Tourville, located along the Seine Valley. The upper deposit (unit D), previously dated at 200 ka by ESR on in situ shells and correlated with a stage 7 high sea-level stand (186–245 ka), yields a measured IRSL age of 176 ± 21 ka. The lower deposit (unit B) assigned to a distinctly older high sea-level event (stage 9: 303–339 ka) yields a measured IRSL age of 273 ± 28 ka. The nearby stage 7 raised beach of Sangatte, in Northwestern France, previously dated by TL on quartz (229 ± 18 ka) yields a measured IRSL age of 186 ± 19 ka. These IRSL age estimates systematically underestimate the expected geological ages. This could be due to the long-term fading or instability of the luminescence signal in alkali feldspars. The correction for long-term fading has been tested on these samples. At Tourville, it yields corrected IRSL ages of 196 ± 23ka and 314 ± 32ka, for the upper and lower units respectively and, at Sangatte, a corrected IRSL age of 206 ± 20 ka. These corrected IRSL age estimates are in better agreement with the expected geological ages. This study demonstrates the potential of the feldspar luminescence dating method to provide chronological information on Middle Pleistocene interglacial estuarine sediments within the North Sea-English Channel Basin.  相似文献   

8.
Buylaert, J.‐P., Huot, S., Murray, A.S. & Van den haute, P.: Infrared stimulated luminescence dating of an Eemian (MIS 5e) site in Denmark using K‐feldspar. Boreas, 10.1111/j.1502‐3885.2010.00156.x. ISSN 0300‐9483. Infrared stimulated luminescence (IRSL) dating of K‐feldspars may be an alternative to quartz optically stimulated luminescence (OSL) dating when the quartz OSL signal is too close to saturation or when the quartz luminescence characteristics are unsuitable. In this paper, Eemian (MIS 5e) coastal marine sands exposed in a cliff section on the coast of southern Jutland (Denmark) are used to test the accuracy and precision of IRSL dating using K‐feldspars. This material has been used previously to test quartz OSL dating ( Murray & Funder 2003 ): a small systematic underestimation of <10% compared to the expected age of ~130 ka was reported. In our study, a single‐aliquot regenerative‐dose (SAR) IRSL protocol is used to determine values of equivalent dose (De) and the corresponding fading rates (g values). A significant age underestimation (of up to ~35%) is observed; this is attributed to anomalous fading. Using a single site‐average fading rate of 3.66 ± 0.09%/decade to correct the IRSL ages for all samples provides good agreement between the average fading‐corrected K‐feldspar age (119 ± 6 ka) and the independent age control (132–125 ka). This is despite the reservations of Huntley & Lamothe (2001) that their fading correction method is not expected to work on samples older than ~20–50 ka. This fading‐corrected feldspar result is not significantly different from the overall revised quartz age (114 ± 7 ka) also presented here. We conclude that fading‐corrected IRSL ages measured using K‐feldspar may be both precise and accurate over a greater age range than might be otherwise expected.  相似文献   

9.
使用钾长石进行释光测年时,由于长石的释光信号存在异常衰减,会导致沉积事件年龄的低估。对中国北方4个全新世样品分别使用石英和钾长石矿物组分释光测年,通过测量钾长石的衰退系数(g值)对钾长石使用再生剂量法获得的表征年龄进行了校正。发现对于本文所研究的年轻样品钾长石表征年龄与石英年龄相比系统偏小约2%~9%,钾长石校正年龄与石英年龄相比则严重偏大约16%~40%,表明使用g值无法校正年轻样品的钾长石年龄。对于年轻样品,钾长石IRSL信号异常衰减现象对测年结果的影响是可以忽略的。  相似文献   

10.
对洛川末次冰期的黄土细颗粒混合矿物红外释光(IRSL)信号异常衰减行为的初步研究结果表明: 1)预加热只能部分消除异常衰减对等效剂量测定的影响,不能完全消除这种影响,IRSL异常衰减过程也许存在着热效应和非热效应两种组分; 2)对16个已知年龄的马兰黄土(15~70ka)样品细颗粒混合矿物天然IRSL信号的ED值与期望ED值的比较初步显示,马兰黄土细颗粒混合矿物IRSL信号异常衰减不断发生,导致混合矿物IRSL的年龄测定值可能被低估达20 % 以上。  相似文献   

11.
Luminescence dating is used extensively to provide absolute chronologies for Late Pleistocene sediments. Nowadays, most optical dates are based on quartz optically stimulated luminescence (OSL). However, the application of this signal is usually limited to the last ~100 ka because of saturation of the quartz luminescence signal with dose. In contrast, the feldspar infrared stimulated luminescence (IRSL) dose–response curve grows to much higher doses; this has the potential to extend the datable age range by a factor of 4–5 compared with quartz OSL. However, it has been known for several decades that this IRSL signal is unstable, and this instability often gives rise to significant age underestimation. Here we test against independent age control the recently developed feldspar post‐IR IRSL approach to the dating of sediments, which appears to avoid signal instability. A physical model explaining our observations is discussed, and the method is shown to be accurate back to 600 ka. The post‐IR IRSL signal is reduced by exposure to daylight more slowly than that from quartz and low‐temperature IRSL, preventing its general application to young (e.g. Holocene) sediments. Nevertheless, this new approach is widely applicable (feldspar of appropriate luminescence behaviour is even more ubiquitous than quartz). These characteristics make this a method of great importance for the dating of Middle and Late Pleistocene deposits.  相似文献   

12.
Radiocarbon dating of bulk organic matter is the most commonly used method for establishing chronologies of lake sediments for palaeoclimate reconstructions on the Tibetan Plateau. However, this method is likely to be problematic because the dated material often suffers from old carbon contamination. Recently, advances in luminescence‐based chronological techniques have provided new options for dating lacustrine sediments. In the current study, we tested for the first time the applicability of a new post‐IR IRSL (pIRIR) measurement protocol for dating fine‐grained polymineral material from a deep‐lake sediment core from the central part of Tangra Yumco, on the southern Tibetan Plateau. Our results show that: (i) radioactive disequilibria in the uranium decay chain were observed in the studied lake sediments, and thus taken into account for dose rate calculation by using a dynamic modelling approach; (ii) the suitability and robustness of the pIRIR protocol measured at 150°C (pIRIR150) for our samples are confirmed by a set of luminescence characteristic tests as well as the agreement with an independent age control; (iii) turbidite deposition partly caused an insufficient resetting of luminescence signals and thus apparent overestimation in luminescence dating; (iv) compared with the luminescence‐based age‐depth model, the 14C ages of bulk organic matter from the studied core generally yielded an age difference of ~2 ka, which is attributed to hardwater reservoir effects in Tangra Yumco. This study highlights the need for multi‐dating approaches of lake sedimentary archives on the Tibetan Plateau.  相似文献   

13.
We report the discovery of the oldest evidence for human presence in the southeastern Baltic Sea region. This paper presents an overview of the Riadino‐5 archaeological site in the lower course of the Šešupė River (Kaliningrad Oblast of Russia) and direct infrared stimulated luminescence (IRSL) ages for the culture‐bearing sediments from the site, which place the time of occupation well within the range of Marine Isotope Stage (MIS) 3 (ca 57–26 ka). Luminescence ages were determined using the multiple‐aliquot additive‐dose technique, applied to sand‐sized potassium feldspar. Four of the six IRSL samples from the site come from the cultural deposits, while two are from the surrounding sediments. The luminescence age of the deposits implies that human occupation of the southeastern Baltic Sea region occurred at least between 50 ka and 44 ka during the first half of MIS 3 and the Middle‐Upper Paleolithic.  相似文献   

14.
This study evaluates the accuracy of optically stimulated luminescence to date well-preserved strandline sequences at Manistique/Thompson bay (Lake Michigan), and Tahquamenon and Grand Traverse Bays (Lake Superior) that span the past ∼4500 yr. The single aliquot regeneration (SAR) method is applied to produce absolute ages for littoral and eolian sediments. SAR ages are compared against AMS and conventional 14C ages on swale organics. Modern littoral and eolian sediments yield SAR ages <100 yr indicating near, if not complete, solar resetting of luminescence prior to deposition. Beach ridges that yield SAR ages <2000 yr show general agreement with corresponding 14C ages on swale organics. Significant variability in 14C ages >2000 cal yr B.P. complicates comparison to SAR ages at all sites. However, a SAR age of 4280 ± 390 yr (UIC913) on ridge77 at Tahquamenon Bay is consistent with regional regression from the high lake level of the Nipissing II phase ca. 4500 cal yr B.P. SAR ages indicate a decrease in ridge formation rate after ∼1500 yr ago, likely reflecting separation of Lake Superior from lakes Huron and Michigan. This study shows that SAR is a credible alternative to 14C methods for dating littoral and eolian landforms in Great Lakes and other coastal strandplains where 14C methods prove problematic.  相似文献   

15.
The alternation of terrestrial and marine deposits is an indicator of past environmental and sea‐level changes. The age of deposition is usually dated by means of radiocarbon. However, radiocarbon dates of molluscan shells from coastal areas may be complicated by various sources of carbon, and problematic for deposits of 40–50 ka or older. Herein, we apply the Optically Stimulated Luminescence (OSL) dating method to date samples from terrestrial and marine/coastal sediments extracted from three cores in the south Bohai Sea, China. Multiple‐ and single‐aliquot regenerative‐dose procedures using OSL signals from fine‐silt (4–11 μm), coarse‐silt (38–63 μm) and fine‐sand (63–90 or 90–125 μm) quartz were employed to determine the equivalent dose (D e). The results showed that: (i) OSL ages from quartz of different grain sizes and different protocols are consistent with each other; (ii) for Holocene samples, most of the radiocarbon dates agree well with OSL ages; (iii) for pre‐Holocene samples, radiocarbon dates cluster at 40–50 14 C ka BP, whereas OSL ages are in stratigraphic order from 11 ka to 176 ka. Because of the self‐consistency of the quartz OSL ages, the stratigraphic agreement in the three cores, and the clustering of the radiocarbon dates, we suggest that the quartz OSL ages are more reliable with respect to dating the samples from the south Bohai Sea. Finally, the four marine strata identified in the south Bohai Sea are likely to have formed during the Holocene, Marine Isotopic Stage (MIS) 3–5, MIS 6 and probably MIS 7, respectively.  相似文献   

16.
《Quaternary Science Reviews》2003,22(8-9):925-941
We summarize the results of a test on the potential of optical dating for the age assessment of Late Quaternary deep-sea sediments. Our approach combines a single aliquot regeneration (SAR) protocol for equivalent dose (De) estimation on fine silt-sized quartz with a time-dependent evaluation of supported and unsupported long-lived radioisotopes within the deposited sediment matrix. For this purpose nine samples from two independently dated deep-sea cores from the Indian Ocean were obtained. The SAR analysis resulted in mean De estimates with precisions ranging from 0.9% to 3.7%. Combination of these data with measured radioisotope concentrations resulted in stratigraphically sensible ages ranging from ca 7 to 120 ka. These ages exhibit good agreement with existing chronologies for the cores based on radiocarbon age determinations and correlation of key volcanic, palaeoecological and isotopic events. Optical dating may provide an important additional dating method for Late Quaternary deep-sea sediments.  相似文献   

17.
采用热释光和红外光释光测年技术获取了采自朝鲜半岛西南部和顺支石墓遗址剖面中的陶片和沉积物的年龄.古陶片的热释光年龄分别是(3100±210)a和(3680±320)a,相应文化层中支石墓墓葬层位的红外光释光年龄分别是(2200±190)a和(2900±310)a.古陶片的热释光年龄老于地层的红外光释光年龄,代表着支石墓...  相似文献   

18.
Excavations at the Wenas Creek Mammoth Site yielded mammoth, bison, and two possible artifacts in a single colluvial stratum, with radiocarbon bone dates ∼17 ka. Eight infrared‐stimulated luminescence (IRSL) samples were collected to establish general ages of site strata, returning multi‐grain estimates consistent with stratigraphic integrity and the radiocarbon dates. Four additional IRSL samples were collected to estimate the depositional age of one artifact found in place. These produced a pooled total of 94 single‐grain estimates from near the artifact, 80% averaging 16.8 ± 0.9 ka, and 20% averaging 5.1 ± 0.5 ka. These results could be interpreted to demonstrate pre‐Clovis age artifact deposition consistent with the bone dates, or a mid to late Holocene intrusion into older deposits, possibly by bioturbation. The single‐grain IRSL dates do not provide proof of pre‐Clovis presence beyond reasonable doubt at this site, but do show that this technique is valuable in assessing the stratigraphic integrity needed for any such claim.  相似文献   

19.
A 10.5 m core from Changeable Lake in the Severnaya Zemlya Archipelago just north of the Taymyr Peninsula intersects ca. 30 cm of diamicton at its base, interpreted as a basal till. Because the upper 10.13 m of this core consists of non‐glacial sediments, a maximum numeric age for these non‐glacial sediments would provide a clear lower limit to the timing of the last glaciation in the area of Changeable Lake. Radiocarbon (14C) dating of several materials from this core yielded widely scattered results. Consequently we applied photonic dating to sediments above the diamicton. The experimental single‐aliquot‐regenerative (SAR) dose fine‐grain method was applied to two samples, using the ‘double SAR’ approach. With one exception, these fine‐grain SAR results and the results of application of the SAR method to sand‐sized quartz grains from two samples, at ca. 9.95 m and ca. 10.05 m depth, are discrepant with age estimates from the multi‐aliquot infrared‐photon‐stimulated luminescence (IR‐PSL) method applied to fine grains. Multi‐aliquot IR‐PSL dating of 10 samples produces ages increasing monotonically from ca. 4 ka at 2 m to 53 ± 4 ka at 9.97 m. These self‐consistent multi‐aliquot IR‐PSL ages, along with limiting 14C ages of >47 ka at ca. 10 m, provide direct evidence that glacial ice did not advance over this lake basin during the Last Glacial Maximum, and thus delimit the northeastern margin of the Barents–Kara Sea ice‐sheet to somewhere west of this archipelago. The last regional glaciation probably occurred during marine isotope stage (MIS) 4 or earlier. Copyright © 2004 John Wiley & Sons, Ltd.  相似文献   

20.
北美五大湖区的安大略湖北岸Don Valley Brickyard、Scarborough Bluffs、Bowmanville Bluffs剖面共同构成了北美东北部最长也是最厚的陆地第四纪沉积记录, 较完整地记录了晚更新世劳伦泰德冰盖(the Laurentide Ice Sheet)的演化. 晚更新世劳伦泰德冰盖演化的重建有赖于这些经典剖面中重要沉积地层单元的准确年代学控制. 传统的地层年代学主要是依靠少量14C年代, 将主要的混杂堆积单元(diamicton)解释为气候变冷环境下的冰川扩张, 并与指示全球冰量变化的深海氧同位素曲线一一比对建立起来的. 这样建立起来的年代学存在很大的不确定性. 20世纪80-90年代的少量热释光年代也不相吻合, 最近的13个长石红外释光定年则只集中于Bowmanville Bluffs的一个分层, 并未建立整个剖面的地层年代学, 使这些经典沉积剖面的年代学一直没有得到系统的建立. 应用石英光释光SAR-SGC法测试了Bowmanville Bluffs剖面Glaciofluvial Sand单元的2个冰水沉积样品, 年代结果分别为(41.6±3.8) ka、(48.1±4.4) ka, 分析表明这一年代结果偏老, 石英颗粒可能晒褪不完全. 由于大测片无法识别晒褪不完全的颗粒, 因此, 测试更多的剖面序列的光释光年代并尝试采用粗颗粒小测片或单颗粒技术解决样品颗粒晒褪不完全的问题将是必要的.  相似文献   

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