共查询到19条相似文献,搜索用时 62 毫秒
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利用高分辨电镜研究了变质岩斜方辉石的超微结构,其中的单斜辉石多型是偶数倍0.9m宽度,并发现(001)90°和180°畴结构,它表明样品曾受到较强的挤压作用。 相似文献
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煤基石墨微结构的高分辨电镜研究 总被引:3,自引:0,他引:3
煤体经热变质作用形成的石墨叫煤基石墨。湖南省鲁塘地区煤基石墨,经与之共生的红柱石的相图分析,它属于低压相系矿物,在200—800℃和5.5×10~5Pa以下条件下形成。它的高分辨电子显微象显示,煤基石墨按其石墨化程度有四种类型微结构。因而。将煤基石墨划分为相继的四个石墨化阶段。同时有四种石墨产物,它们是:前石墨化阶段——芳层石墨;初石墨化阶段——微柱石墨;中石墨化阶段——柔绉石墨;高石墨化阶段——平直石墨 相似文献
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围压作用下冻结砂土微结构变化的电镜分析 总被引:7,自引:7,他引:7
利用扫描电子显微镜,对饱水冻结兰州砂土在-5℃和围压(0-22MPa)下进行结构观测,结合围压对强度影响的宏观特征分析发现:当O≤σ〈8MPa时,结构以压密为主,强化作用占优势,强度随围压的增大而增大;当8≤σ〈16MPa时,颗粒出现破碎现象,某些颗粒接触点处的冰发生融化,粒间摩擦减少,致使强度随围压的增大而缓慢降低,当σ≥16MPa时,颗粒破碎程度加剧,某些团粒中出现大的裂隙,结构联结破坏,导致 相似文献
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浙江青田单斜晶系叶腊石微结构的高分辨透射电镜研究 总被引:2,自引:2,他引:0
采用X射线粉晶衍射(XRD)、高分辨透射电镜(HR-TEM)及X射线荧光光谱(XRF)对青田叶腊石的矿物学特征进行了较为系统的研究。结果表明:叶腊石矿物颗粒微结构中最基本的构成单元为纳米板片,且该板片多呈聚集态,单层板片面积大小不一,厚度为(8±2)nm。XRF分析结果表明青田叶腊石原矿混合物中SiO2与Al2O3的分子个数比为6.2,明显高于纯叶腊石中SiO2与Al2O3的分子个数比4.0。HR-TEM对叶腊石晶体结构的研究证实青田叶腊石具有典型的单斜晶系特征,该结论与叶腊石XRD结论一致;且XRD分析结果证实其伴生矿为石英,该结论与XRF所获得的青田叶腊石的"富硅"特征吻合。此外,叶腊石微结构中存在着较明显的晶体缺陷。在高能电子束辐照作用下,叶腊石晶体结构发生明显的破坏,并最终转变为非晶态结构。 相似文献
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叶腊石微结构及其晶体结构缺陷的高分辨透射电镜分析 总被引:2,自引:0,他引:2
采用场发射扫描电镜(FE-SEM)、高分辨透射电镜(HRTEM)结合选区电子衍射(SAED)、X射线粉晶衍射(XRD)及X射线荧光光谱(XRF)等对浙江青田叶腊石的微结构特征进行较系统的研究。结果表明:①粉晶X射线衍射证实青田叶腊石具有典型的单斜晶系特征,该结论与叶腊石粉体选区电子衍射结果吻合,且其伴生矿为石英。②叶腊石微晶体呈"复式板片"构型,且"复式"板片中薄片厚度约为8±2 nm。③在高能电子束辐照下,叶腊石矿物颗粒形貌及晶格结构发生明显的改变,且由此产生晶格膨胀,并最终形成非晶态。 相似文献
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在对湖南湘潭锰矿次生氧化带中天然锰钾矿鉴定的基础上.采用HRTEM对该地区结晶程度差、呈隐晶质集合体的天然锰钾矿微结构进行研究.结果表明:Mn,K,O为样品的主要元素.还含少量Cu,Si.Al,Mg,Fe等杂质元素;锰钾矿表现出一维针状的纳米晶,大多数纳米晶的宽度〈100nm;对选区电子衍射(SAED)计算d值并指标化.确定是锰钾矿,而电子衍射所表现出的弥散环、衍射斑点圆弧化和拉长,均表明该地区样品结晶度差、具有超结构和一定择优取向的特征,这与锰钾矿呈一维针状纳米晶的特征相一致。在锰钾矿的晶格像中,普遍存在晶格畸变、位错缺陷和超结构现象。因此,结晶度较差、颗粒细小至纳米级、结构的有序度较低等是该地区锰钾矿的主要特点。 相似文献
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The microstructure of palygorskite from Longwang Mountain of Xuyu County, Jiangsu Province, was studied by energy dispersive X-ray analysis (EDX), selected-area electron diffraction (SAED) and high-resolution transmission electron microscopy (HRTEM). The average composition of the palygorskite studied is (Si7.38A10.62) (A10.96Fe^3+ 0.62Mg2.86 0.56)Ca0.03K0.06O20(OH)2(OH2)4, which is rich in Mg. Several SAED patterns from a single crystal of palygorskite were obtained with different zone axes. The polymorphs (monoclinic and orthorhombic) are unequivocally distinguished by distant interplanar angles, even though they possess similar sets of d-values. High-resolution images of three principal zones ([010], [100] and [110]) were obtained. The lattice fringes on HRTEM images along [010] have spacings of 0.319 nm. These fringes are interpreted as periodic alterations of two tetrahedral (T) sheets and one octahedral (O) sheet (-TT-O-TT-O-). We have directly observed trioctahedral and dioctahedral individual palygorskite particles along [100]. They are all presented as dark lines along [001], but the width of dark lines corresponding to trioctahedral crystals (0.913 nm) is twice that of the dioctahedral ones (0.456 nm). This is because the trans.sites are occupied by cations in trioctahedral palygorskite. The width of dark lines along [110] is 1.024 nm, a bit thinner than the theoretical spacing (1.044 nm). This is because water molecules quickly leave the structure upon the irradiation by the electron beam. 相似文献
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珍珠显微结构及纳米矿物的电镜分析 总被引:1,自引:1,他引:1
采用SEM(扫描电子显微镜)和HRTEM(高分辨透射电子显微镜)技术,系统地研究了珍珠层及其微结构.发现珍珠质层是由有机质胶结的文石组成片状晶层,文石大量为六边形、不规则多边形和近圆形,并与有机质层交互平行叠置.在棱柱层的柱状晶体周围也有纤维状、胶状有机质.同时,在棱柱状和片状文石晶体的截面上,含有大量纳米级的圆形、椭圆形等形状的有机质、气液包裹体或孔洞.其中许多部位的有机基质中不同程度地显现出晶格条纹像,均为纳米矿物所致.以上结果均表明珍珠层具有有序、精细、多层次、整体性好等优良的结构特点.这一结论对于探讨珍珠的成因、机械强度及医药保健性能等方面均具有重要的意义. 相似文献
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Kerogen plays an important role in shale gas adsorption, desorption and diffusion. Therefore, it is necessary to characterize the molecular structure of kerogen. In this study, four kerogen samples were isolated from the organic-rich shale of the Longmaxi Formation. Raman spectroscopy was used to determine the maturity of these kerogen samples. High-resolution transmission electron microscopy (HRTEM), 13C nuclear magnetic resonance (13C NMR) , X-ray diffraction (XRD) and Fourier transform infrared (FT-IR) spectroscopy were conducted to characterize the molecular structure of the shale samples. The results demonstrate that VReqv of these kerogen samples vary from 2.3% to 2.8%, suggesting that all the kerogen samples are in the dry gas window. The macromolecular carbon skeleton of the Longmaxi Formation kerogen is mainly aromatic (fa’=0.56). In addition, the aromatic structural units are mainly composed of naphthalene (23%), anthracene (23%) and phenanthrene (29%). However, the aliphatic structure of the kerogen macromolecules is relatively low (fal*+falH=0.08), which is presumed to be distributed in the form of methyl and short aliphatic chains at the edge of the aromatic units. The oxygen-containing functional groups in the macromolecules are mainly present in the form of carbonyl groups (fac=0.23) and hydroxyl groups or ether groups (falO=0.13). The crystallite structural parameters of kerogen, including the stacking height (Lc=22.84 ?), average lateral size (La=29.29 ?) and interlayer spacing (d002=3.43 ?), are close to the aromatic structural parameters of anthracite or overmature kerogen. High-resolution transmission electron microscopy reveals that the aromatic structure is well oriented, and more than 65% of the diffractive aromatic layers are concentrated in the main direction. Due to the continuous deep burial, the longer aliphatic chains and oxygen-containing functional groups in the kerogen are substantially depleted. However, the ductility and stacking degree of the aromatic structure increases during thermal evolution. This study provides quantitative information on the molecular structure of kerogen samples based on multiple research methods, which may contribute to an improved understanding of the organic pores in black shale. 相似文献
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在宏观变形分析的基础上,重点论述仙女山断层带的微观变形特征。估算了断层带发育过程中两个主要变形阶段的温度、应力和应变速率,探讨了微观变形机制和变形环境。 相似文献
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粘性土微观结构的定向性是影响粘性土工程地质性质一个十分重要因素。本文介绍了两种粘性土微观结构定量测试新技术,即D/MAX Ⅲ A型全自动组构测角仪和Videolab图像分析系统;系统地提出了四种评价粘性土微观结构定向性的定量表示方法,即各向异性率、概率熵、粘土矿物定向频率分布函数(F(ф))和粘性土团粒定向频率分布函数(Q(α))。最后对江苏淮阴粘土、粉质粘土和粉土三类重塑固结土的微观结构定向性进行了系统分析。研究结果表明,在相同的固结和制样条件下,由于三类粘性土的粒度和成分不同,其定向性有明显差别,同一试样中,片状粘土矿物的定向性与粘性土团粒的定向性常常是不一致的;选取何种定向频率分布函数评价粘性土的各向异性,应视具体的研究内容和土性来决定。研究成果对于建立各向异性粘性土微观力学模型是必不可少的,具有重要意义。 相似文献
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